提出一种自支撑通孔有序氧化铝膜(AAM)的阴极电解制备方法.在中性氯化钾水溶液中,以AAM/Al为阴极,石墨为阳极,电压为-4～-5V,电解3～10min即可把氧化铝膜从铝基底上剥离,同时去除背面阻挡层,获得自支撑通孔氧化铝膜.讨论了通孔氧化铝膜电解制备方法的剥膜、通孔的机理.
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