{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"为了进一步研究气/<span style=\"color:red\">液</span>界面上的Richt myer-Meshkov (RM)不稳定性现象,在水平激波管中进行了激波与单、双排<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>相互作用的实验.通过使用驱动气体为氮气、被驱动气体为空气,获得了马赫数为1.10与1.25的激波;通过更换不同尺寸的试件获得了初始直径不同的<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>.使用高速摄影仪记录了激波作用之后<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>失稳变形的详细过程,测量分析了不稳定性发展过程中,尖钉高度、气泡深度及混合区域宽度随时间的发展规律,并与理论分析中的公式进行了比较.","authors":[{"authorName":"施红辉","id":"ea28a99f-fce4-4649-a6d5-b398bcb45b2a","originalAuthorName":"施红辉"},{"authorName":"肖毅","id":"5bb7d0ed-9f40-4789-b0a8-62a244d66724","originalAuthorName":"肖毅"},{"authorName":"吴宇","id":"cbbb9a34-7a52-4de5-a702-25d5ba3b08fe","originalAuthorName":"吴宇"},{"authorName":"章利特","id":"ba142a7d-0b36-4f6a-8e4e-7b184e29ef3a","originalAuthorName":"章利特"},{"authorName":"王超","id":"52c8b82b-d5eb-4d63-99c9-7e57cd9c5daf","originalAuthorName":"王超"},{"authorName":"董若凌","id":"3831763c-6d3d-460f-aaf7-81d2bc243476","originalAuthorName":"董若凌"}],"doi":"","fpage":"1775","id":"f0a5f57a-3fa8-4ecb-b251-ebf05495cce5","issue":"9","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"c615b433-97a0-49ed-a463-fbb0c3a33bd5","keyword":"Richtmyer-Meshkov不稳定性","originalKeyword":"Richtmyer-Meshkov不稳定性"},{"id":"88938481-f687-4737-aeec-cbbb7c7319c8","keyword":"激波与激波管","originalKeyword":"激波与激波管"},{"id":"fefcc55f-3d21-44d8-a8ce-81a41b6235b4","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>","originalKeyword":"液柱"},{"id":"39dad059-4f50-493c-bdef-dc2e83f3c370","keyword":"尖钉和气泡的增长","originalKeyword":"尖钉和气泡的增长"}],"language":"zh","publisherId":"gcrwlxb201409021","title":"激波诱导的<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>气<span style=\"color:red\">液</span>界面RM不稳定性的研究","volume":"35","year":"2014"},{"abstractinfo":"制备<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>柱头筛板的选择直接影响到样品在柱头的分配情况及色谱<span style=\"color:red\">柱</span><span style=\"color:red\">柱</span>效的高低.利用<span style=\"color:red\">柱</span>后可见-紫外检测,比较了采用多孔聚四氟乙烯材料和多孔烧结不锈钢材料作为台锥形制备<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>柱头筛板材料时的<span style=\"color:red\">柱</span>效;用<span style=\"color:red\">柱</span>上可视化方法研究了柱头筛板的直径对流型的影响.结果表明,多孔聚四氟乙烯的变形使得采用该材料做<span style=\"color:red\">柱</span>间筛板的色谱<span style=\"color:red\">柱</span><span style=\"color:red\">柱</span>效比使用多孔不锈钢筛板的色谱<span style=\"color:red\">柱</span><span style=\"color:red\">柱</span>效低约40%;样品流经直径小于<span style=\"color:red\">柱</span>入口内径的筛板导致样品在柱头分配不均,而流经直径与<span style=\"color:red\">柱</span>入口内径相同的筛板时因受到的阻力相同,可以实现柱塞状进样.还观察到不同直径的筛板导致不同的流型.使用直径与色谱<span style=\"color:red\">柱</span>入口内径相同的筛板可以提高<span style=\"color:red\">柱</span>效约20%.","authors":[{"authorName":"马继平","id":"06b43e54-a80d-41d6-b3b6-0a7b3a12b69f","originalAuthorName":"马继平"},{"authorName":"陈令新","id":"0505b4bd-be9f-4b51-a8f4-f56a6ee5bf2d","originalAuthorName":"陈令新"},{"authorName":"朱道乾","id":"15775e42-14fe-43d6-b1bb-64af47d9322a","originalAuthorName":"朱道乾"},{"authorName":"关亚风","id":"0ea5660e-f26b-44cf-b6e1-59b6534187ed","originalAuthorName":"关亚风"}],"doi":"10.3321/j.issn:1000-8713.2003.04.034","fpage":"430","id":"7413a35c-e0c7-4666-b21f-2d7132fc057a","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"f008b9f0-15ea-43bb-a3b1-1685771a34df","keyword":"制备<span style=\"color:red\">液</span>相色谱","originalKeyword":"制备液相色谱"},{"id":"e05ff710-bc13-4fe5-86a6-9449afbce98d","keyword":"筛板","originalKeyword":"筛板"},{"id":"e93727b6-df8e-4306-85b1-dd9b6d191c57","keyword":"样品分配","originalKeyword":"样品分配"},{"id":"a35ed332-bd93-4a46-9581-4fa4252cae2f","keyword":"流型","originalKeyword":"流型"},{"id":"66e3efa2-4c33-4156-9cd4-b7402334b223","keyword":"台锥形<span style=\"color:red\">柱</span>","originalKeyword":"台锥形柱"}],"language":"zh","publisherId":"sp200304034","title":"筛板对台锥形制备<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>流型和<span style=\"color:red\">柱</span>效的影响","volume":"21","year":"2003"},{"abstractinfo":"设计并评价了尾锥形填充毛细管<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>,与粘结型<span style=\"color:red\">柱</span>尾比较,前者<span style=\"color:red\">柱</span>效高且van Deemter曲线高流速部分的流速-<span style=\"color:red\">柱</span>效关系明显改善.在折合流速为10～15时,前者的<span style=\"color:red\">柱</span>效比后者高出30%～50%.谱带的抛物线状的流形在尾锥形<span style=\"color:red\">柱</span>内得到改善,使色谱峰的对称性有明显提高.比较了两种结构的色谱<span style=\"color:red\">柱</span>在芳烃快速分析中的分离效果,结果是尾锥形<span style=\"color:red\">柱</span>的分离性能优于粘结型<span style=\"color:red\">柱</span>.","authors":[{"authorName":"朱翠茹","id":"d6e316be-f1fd-4dec-be54-5ef366f52ede","originalAuthorName":"朱翠茹"},{"authorName":"关亚风","id":"12048f02-4b4c-48e1-b139-02925d945fe4","originalAuthorName":"关亚风"},{"authorName":"吴建强","id":"2cf78081-9f21-4214-867a-da1ada927c5b","originalAuthorName":"吴建强"}],"doi":"10.3321/j.issn:1000-8713.2000.05.002","fpage":"383","id":"590faf93-bcf1-485e-9686-cbbb4145e656","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"d2b7a50d-57f2-42c1-91f3-86a12c372df4","keyword":"尾锥形<span style=\"color:red\">柱</span>","originalKeyword":"尾锥形柱"},{"id":"63cf80c4-c38b-4d24-b2a5-36a8a7dbd8cf","keyword":"填充毛细管<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>","originalKeyword":"填充毛细管液相色谱柱"},{"id":"dc77d40a-0988-4742-aff9-b4a5b13c3691","keyword":"<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>结构","originalKeyword":"液相色谱柱结构"},{"id":"b4826631-0d1f-443d-9147-6811d37ab549","keyword":"快速分析","originalKeyword":"快速分析"}],"language":"zh","publisherId":"sp200005002","title":"宽口径填充毛细管<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span><span style=\"color:red\">柱</span>尾结构的改进","volume":"18","year":"2000"},{"abstractinfo":"湿法<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>烟气脱硫技术是基于简易湿法石灰-石膏烟气法开发的新型湿法脱硫技术,本套设备在2000～2001年间进行了工业级示范实验运行,得到了湿法<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>脱硫反应的一些基本数据与规律.本文主要探讨了湿法<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>脱硫系统中<span style=\"color:red\">液</span>气比、吸收塔浆液pH值、烟气温度和烟气中SO2含量等工艺参数对系统脱硫效率的影响规律,并进行了初步的机理分析,为进一步的改进湿法<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>烟气脱硫系统的工艺奠定了基础.","authors":[{"authorName":"杨小勇","id":"ed1868d0-4d72-4ca3-97d6-044f0f5cd287","originalAuthorName":"杨小勇"},{"authorName":"李彦","id":"7683479e-0d33-4e30-b564-800e601575cd","originalAuthorName":"李彦"},{"authorName":"项光明","id":"718eedd9-deaf-4e39-8503-6e63bc426175","originalAuthorName":"项光明"},{"authorName":"李定凯","id":"8d77440a-f38b-4114-9bdd-9ef2205c0117","originalAuthorName":"李定凯"},{"authorName":"陈昌和","id":"59da4a3f-5dcb-4dbe-97cc-d383273c3298","originalAuthorName":"陈昌和"},{"authorName":"徐旭常","id":"34304a63-4df1-4e5b-9674-b24dce2a00cb","originalAuthorName":"徐旭常"}],"doi":"","fpage":"167","id":"71389a89-bd38-4737-8870-4f5ccb8d712f","issue":"1","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"2c5b0525-fa19-4b97-8896-ca92ef447390","keyword":"湿法烟气脱硫","originalKeyword":"湿法烟气脱硫"},{"id":"5b1d70a6-9cff-4068-8463-c7b928a1d0e9","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>脱硫塔","originalKeyword":"液柱脱硫塔"},{"id":"81a04115-32b6-453b-acf0-b9e73554c828","keyword":"<span style=\"color:red\">液</span>气比","originalKeyword":"液气比"},{"id":"e1950293-14af-486d-a1bb-494e62166759","keyword":"浆液pH值","originalKeyword":"浆液pH值"}],"language":"zh","publisherId":"gcrwlxb200601052","title":"湿法<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>喷射烟气脱硫反应的实验研究","volume":"27","year":"2006"},{"abstractinfo":"本文提出了一种<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>冲击式湿法脱硫装置,对该装置的吸收段阻力特性和脱硫特性进行了试验研究,对试验结果进行了分析.分析发现了在塔内风速为2 m/s～2.9 m/s范围内,脱硫效率随塔内风速的增大而增加这一不同于其它装置的特点,得到了在塔内风速2.6 m/s,喷<span style=\"color:red\">液</span>量30 m3/h时脱硫效率高、阻力低这个比较经济的工况点.","authors":[{"authorName":"孔华","id":"50046482-fe1b-45f2-8fcb-9c9234c9db3a","originalAuthorName":"孔华"},{"authorName":"高翔","id":"9cf332c0-de4e-4e6a-b18a-c793599ce30b","originalAuthorName":"高翔"},{"authorName":"吕同波","id":"32e3d012-2877-49bf-9c03-16f0d995d810","originalAuthorName":"吕同波"},{"authorName":"方航宇","id":"34451638-c63f-4f66-bb7a-892183f84ac5","originalAuthorName":"方航宇"},{"authorName":"骆仲泱","id":"6869ae93-3d85-485d-b7d4-693899d36a8f","originalAuthorName":"骆仲泱"},{"authorName":"岑可法","id":"b52a04db-c2e4-473e-a341-edc40f90e5f2","originalAuthorName":"岑可法"}],"doi":"","fpage":"649","id":"4adf3116-93de-40d6-93a6-5dfb37e781f8","issue":"5","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"d050fdcd-7011-4f91-9e4e-4e36cce6dc0f","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>冲击","originalKeyword":"液柱冲击"},{"id":"2ad698e4-6178-478b-9968-d6b2025235bb","keyword":"阻力","originalKeyword":"阻力"},{"id":"cec15f84-6e60-4510-8aaa-5829b6c89eae","keyword":"脱硫效率","originalKeyword":"脱硫效率"}],"language":"zh","publisherId":"gcrwlxb200105035","title":"<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>冲击式湿法脱硫装置的试验研究","volume":"22","year":"2001"},{"abstractinfo":"综述了动态轴向压缩技术装填<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>的原理、装置及装置设计的发展状况,对动态轴向压缩装填过程和<span style=\"color:red\">柱</span>性能的影响因素如<span style=\"color:red\">柱</span>长、填料和调浆溶剂的性质、压缩压力进行了分析,讨论了<span style=\"color:red\">柱</span>内密度分布不均、<span style=\"color:red\">柱</span>壁效应两种现象和解决的办法,评价了这种技术的优缺点,介绍了其应用、发展现状与前景.引用文献50篇.","authors":[{"authorName":"韩金玉","id":"f068b8d8-03e5-4da1-a7b8-00302e5e0328","originalAuthorName":"韩金玉"},{"authorName":"魏文英","id":"8c08847e-cd89-476f-af55-e68863bc32e5","originalAuthorName":"魏文英"},{"authorName":"常贺英","id":"0df02da2-8723-4d3f-8a1d-aa4e54470c85","originalAuthorName":"常贺英"},{"authorName":"王华","id":"03f36d8e-abc4-4b30-a1f6-be98048e739c","originalAuthorName":"王华"}],"doi":"10.3321/j.issn:1000-8713.2004.04.028","fpage":"403","id":"15cbe6e8-7e4a-4071-9c58-58e06ca4c476","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"ab422393-4c70-4ad0-bac2-427b173ecf6c","keyword":"制备<span style=\"color:red\">液</span>相色谱","originalKeyword":"制备液相色谱"},{"id":"81e8e13d-f57a-48eb-baab-a80e3937726e","keyword":"动态轴向压缩","originalKeyword":"动态轴向压缩"},{"id":"e229ef00-723c-4c49-9f80-bfff1ddc953d","keyword":"<span style=\"color:red\">柱</span>装填","originalKeyword":"柱装填"}],"language":"zh","publisherId":"sp200404028","title":"制备型<span style=\"color:red\">液</span>相色谱动态轴向压缩<span style=\"color:red\">柱</span>技术和应用","volume":"22","year":"2004"},{"abstractinfo":"设计了一种零死体积的二通式<span style=\"color:red\">柱</span>尾结构和一种使匀浆填料均匀进入色谱<span style=\"color:red\">柱</span>管内的储料池，研究了制备内径在0.5 mm～1.0 mm的不锈钢宽口径填充毛细管<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>的方法。详述了以不同牌号、规格的反相ODS类固定相制备的不同<span style=\"color:red\">柱</span>长的色谱<span style=\"color:red\">柱</span>的性能。通过折合板高/折合流速关系和不对称因子对<span style=\"color:red\">柱</span>性能进行了评价，结果表明，该方法制备的色谱<span style=\"color:red\">柱</span><span style=\"color:red\">柱</span>效达到理论值的75%以上、RSD为6%，稳定性也很好。将其应用于抗癫痫药物和氯苯类化合物的分析，结果令人满意。","authors":[{"authorName":"唐意红","id":"bf985b88-d58c-420a-9a5c-81c04e586f55","originalAuthorName":"唐意红"},{"authorName":"朱道乾","id":"dca0b396-bcc3-46f0-9456-25b7597d1deb","originalAuthorName":"朱道乾"},{"authorName":"关亚风","id":"e93acd63-4ec9-4562-9281-80a164d784be","originalAuthorName":"关亚风"}],"doi":"10.3321/j.issn:1000-8713.2001.04.001","fpage":"289","id":"09af51d9-36e3-4835-bfa8-ad787991639d","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"ed545f34-96e2-4a9a-832f-be83fc55743d","keyword":"填充毛细管<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>","originalKeyword":"填充毛细管液相色谱柱"},{"id":"d38b8e7d-4750-49c2-9954-26d3f40622a2","keyword":"<span style=\"color:red\">柱</span>制备","originalKeyword":"柱制备"},{"id":"b9a3601b-e375-40e7-9a88-dbf6ca078480","keyword":"<span style=\"color:red\">柱</span>尾结构","originalKeyword":"柱尾结构"},{"id":"3d5c6d9a-6b60-406e-880a-e41f45a392e7","keyword":"储料池","originalKeyword":"储料池"}],"language":"zh","publisherId":"sp200104001","title":"不锈钢宽口径填充毛细管<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>","volume":"19","year":"2001"},{"abstractinfo":"电磁铸造的<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>成形性控制是工艺成败及获得合理形状铸锭的关键，稳定、合适的<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>高度反映了各种工艺参数间的良好配合.采用基于模糊理论的神经网络预测方法，通过对铸造系统电信号的跟踪，进行模糊模式识别，预测<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>高度.结果表明，基于模糊神经网络的控制系统使得铸造过程中<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>高度更加稳定，有利于电磁铸造工艺过程的顺利进行，使铸锭的表面质量得到改善.","authors":[{"authorName":"李朝霞","id":"f6ee7e09-88cc-4c23-b6f2-bf6053513908","originalAuthorName":"李朝霞"},{"authorName":"郑贤淑","id":"90df9d32-0fab-4121-8f75-e4ea31bc8650","originalAuthorName":"郑贤淑"}],"doi":"10.3969/j.issn.1005-0299.2000.04.025","fpage":"108","id":"8331d465-8d6a-41e9-b018-d3ded68ae231","issue":"4","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"1f41733a-e8ea-435c-a4e5-4b5c127bae04","keyword":"电磁铸造","originalKeyword":"电磁铸造"},{"id":"b49545c4-fe62-4ccb-bb46-fcf64d7b2ca4","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>成形性","originalKeyword":"液柱成形性"},{"id":"8db80cfe-f5d3-46d6-93e6-54eedc3f9c4a","keyword":"模糊神经网络","originalKeyword":"模糊神经网络"},{"id":"06037156-865b-4731-a3d1-6f274888d427","keyword":"模式识别","originalKeyword":"模式识别"}],"language":"zh","publisherId":"clkxygy200004025","title":"模糊神经网络在电磁铸造<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>成形控制中的应用","volume":"8","year":"2000"},{"abstractinfo":"为了更好地研究水平管外降膜蒸发时的降膜流动规律及其影响因素,本文利用VOF方法建立了液体在水平管外降膜流动的计算模型,并对<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>在管束间的偏移特性进行了数值模拟研究;将数值模拟的计算结果与对应的实验结果相比较,数值解与实验值吻合程度较好;结合实验结果与数值计算结果,推导出了适应性较广的计算<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>偏移量的无量纲关系式.利用所推导的关联式对水蒸气流作用下的<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>偏移量进行预测,为海水淡化工程设计提供参考.","authors":[{"authorName":"雷贤良","id":"b575d900-1849-4ca7-a86a-91ac0df14116","originalAuthorName":"雷贤良"},{"authorName":"李会雄","id":"4b578580-4ef1-449d-b051-d55d78935e9b","originalAuthorName":"李会雄"},{"authorName":"颜利波","id":"2aaf5263-9516-4ed7-a399-0d78d9fcf8ef","originalAuthorName":"颜利波"},{"authorName":"郭斌","id":"96bf1400-f989-4a85-99fd-5e2771017ed2","originalAuthorName":"郭斌"}],"doi":"","fpage":"1875","id":"8b04a71e-7f68-4e85-8fa3-a69988dd7e3a","issue":"11","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"4a63a439-f5bc-484d-87ff-8377ef9370f6","keyword":"气<span style=\"color:red\">液</span>两相流","originalKeyword":"气液两相流"},{"id":"4914e9f4-3f43-4005-86a9-42a4eb8f1de5","keyword":"偏移","originalKeyword":"偏移"},{"id":"6aae91ce-8230-495b-83e5-be7f40779267","keyword":"VOF","originalKeyword":"VOF"},{"id":"f5874999-e15b-4c16-ab8b-6754d8fea29f","keyword":"数值模拟","originalKeyword":"数值模拟"},{"id":"e903fa7e-9cf5-4840-899f-1d07fc1b67bd","keyword":"无因次分析","originalKeyword":"无因次分析"}],"language":"zh","publisherId":"gcrwlxb201011019","title":"气流作用下水平管外<span style=\"color:red\">液</span><span style=\"color:red\">柱</span>偏移特性的数值模拟研究","volume":"31","year":"2010"},{"abstractinfo":"采用高效<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>后衍生法测定蜂王浆中的链霉素.样品用庚烷磺酸钠的酸性溶液进行提取,通过LC-18<span style=\"color:red\">柱</span>和WCX<span style=\"color:red\">柱</span>两次固相萃取达到净化的目的.该方法采用反相C8<span style=\"color:red\">柱</span>,以0.01 mol/L的庚烷磺酸钠溶液和乙腈为流动相,在碱性条件下以1,2-萘醌-4-磺酸钠溶液为<span style=\"color:red\">柱</span>后衍生化试剂,用荧光检测器检测.该方法的线性范围为0.02～0.5 mg/L,相关系数为 0.995 8,方法的检出限和定量限分别为为0.005 mg/kg和0.01 mg/kg,回收率范围为84.0% ～104.0% ,相对标准偏差不大于7.9% .结果表明,该方法能有效地减少蜂王浆中链霉素检测的假阳性结果,符合目前检测工作的需要.","authors":[{"authorName":"张晓燕","id":"c548f1ff-217a-41ff-8235-847b948d1a0f","originalAuthorName":"张晓燕"},{"authorName":"徐锦忠","id":"a73ec7bf-0296-4829-b87c-6a0587d16b5a","originalAuthorName":"徐锦忠"},{"authorName":"沈崇钰","id":"c040ccfa-6ece-47cf-b8f8-c46949c1ce88","originalAuthorName":"沈崇钰"},{"authorName":"陈惠兰","id":"7ce0aade-7cd6-475c-9536-2051b08f43a5","originalAuthorName":"陈惠兰"},{"authorName":"吴斌","id":"75c2047d-1a12-42c2-917d-ec1a596039c3","originalAuthorName":"吴斌"}],"doi":"10.3321/j.issn:1000-8713.2008.03.028","fpage":"395","id":"ea1d1ab6-f51f-44b4-ac9f-0cb368ca8795","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"79581318-30e1-4028-bf3b-2a29eb7deecd","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"85b5fbff-8c92-45bd-8243-618ce9e9eb66","keyword":"<span style=\"color:red\">柱</span>后衍生","originalKeyword":"柱后衍生"},{"id":"6f45549a-b3f7-44fb-9edc-57fe91408038","keyword":"链霉素","originalKeyword":"链霉素"},{"id":"9f0a8bf6-ecba-423f-bd24-76b58043e00f","keyword":"蜂王浆","originalKeyword":"蜂王浆"}],"language":"zh","publisherId":"sp200803028","title":"高效<span style=\"color:red\">液</span>相色谱<span style=\"color:red\">柱</span>后衍生法测定蜂王浆中的链霉素","volume":"26","year":"2008"}],"totalpage":2089,"totalrecord":20889}