以Sn(OEt)2为起始原料,采用水热晶化法合成了分散性良好的金红石结构的SnO2纳米颗粒.采用X射线衍射对其进行了表征,表明SnO2纳米颗粒的结晶性良好,颗粒尺寸小于10nm.将合成的SnO2纳米颗粒均匀分散到Sb:SnO2镀膜液中,经陈化后制成镀膜溶胶,以溶胶-凝胶浸渍镀膜工艺制备纳米颗粒掺杂Sb:SnO2薄膜.分别采用范德堡(Van Der Pauw)法、UV/VIS分光光度计和FTIR中红外分析仪测量并分析膜层的导电性能、光学性能及结构特征,研究了导电纳米颗粒添加对Sb:SnO2薄膜电性能、光学性能和结构的影响.
参考文献
| [1] | Chopra K L;Major S;Pandya D K .[J].Thin Solid Films,1983,102:1-46. |
| [2] | Waal H D;Simonis F .[J].Thin Solid Films,1981,77:253-258. |
| [3] | Gowda G;Nguyen D .[J].Thin Solid Films,1986,136:L39-L42. |
| [4] | Putz J;Ganz D;Gasparro G et al.[J].Sol-Gel Science Technol,1998,13:1005-1010. |
| [5] | Burgard D;Goebbert C;Nass R .[J].Sol-Gel Science Technol,1998,13:789-792. |
| [6] | Racheva TM.;Critchlow GW. .SNO2 THIN FILMS PREPARED BY THE SOL-GEL PROCESS[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,1997(1/2):299-302. |
| [7] | Ganz D;Reich A;Aegerter MA .Laser firing of transparent conducting SnO2 sol-gel coatings[J].Journal of Non-Crystalline Solids: A Journal Devoted to Oxide, Halide, Chalcogenide and Metallic Glasses, Amorphous Semiconductors, Non-Crystalline Films, Glass-Ceramics and Glassy Composites,1997(0):242-246. |
| [8] | Wooten F.Optical Properties of Solids[M].New York:Academic Press,1981:123-134. |
| [9] | Orel B;Lavrencic-Stangar U;Crnjak-Orel Z;Bukovec P et al.[J].Journal of Non-Crystalline Solids,1994,167:272-288. |
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