{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以柠檬酸与硝酸盐为原料通过溶胶自燃烧法制备出纳米Mn0.5Zn0.5Fe2O4和BaZn2Fe16O27粉体.采用XRD、TG-DSC、TEM、AA、BET及VSM等方法对产物进行了表征,结果表明,在1000℃灼烧后分别得到了单相尖晶石型Mn0.5Zn0.5Fe2O4纳米粒子和六角磁铅石型BaZn2Fe16O27纳米粒子,其晶型完整,分散性好.","authors":[{"authorName":"姜炜","id":"8bd31770-3b31-4b34-8f7d-ffad083f4818","originalAuthorName":"姜炜"},{"authorName":"王英会","id":"033666c8-eb23-40d1-9845-f7723699cc6d","originalAuthorName":"王英会"},{"authorName":"刘建勋","id":"c6a8fffc-c795-4cb6-b2f8-d198a0e51266","originalAuthorName":"刘建勋"},{"authorName":"杨毅","id":"18d85eae-5c7a-483d-b159-18d004567e5e","originalAuthorName":"杨毅"},{"authorName":"李凤生","id":"3eaa67ce-68bf-4ea0-8791-3c9b07058d8b","originalAuthorName":"李凤生"}],"doi":"","fpage":"161","id":"93ef28f6-19da-44a3-8ff8-27138d0976f4","issue":"z2","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"b5f5a36a-76f1-4dcf-bea4-0f1f4c2bbf90","keyword":"溶胶","originalKeyword":"溶胶"},{"id":"daa5b92a-9041-4936-9b94-fc37227e74ff","keyword":"自燃烧法","originalKeyword":"自燃烧法"},{"id":"cf7b26d1-67ba-463f-970b-8b4243ee7615","keyword":"Mn0.5Zn0.5Fe2O4","originalKeyword":"Mn0.5Zn0.5Fe2O4"},{"id":"ca6da977-6067-4ac9-8a7e-e453b67763d0","keyword":"BaZn2Fe16O27","originalKeyword":"BaZn2Fe16O27"}],"language":"zh","publisherId":"cldb2006z2047","title":"溶胶自燃烧法制备纳米Mn0.5Zn0.5Fe2O4和BaZn2Fe16O27粉体","volume":"20","year":"2006"},{"abstractinfo":"溶胶-凝胶自燃烧法兼顾了溶胶-凝胶法与自燃烧法的优点,是一种很有应用前景的制备复合氧化物纳米材料的低温合成方法.介绍了柠檬酸盐凝胶自燃烧法的基本原理、反应配比的理论计算,分析了pH值、加水量、柠檬酸/硝酸盐、反应温度等因素对柠檬酸溶胶、凝胶的影响.综述了溶胶-凝胶自燃烧法在制备材料中的应用现状.","authors":[{"authorName":"苏言杰","id":"16bf80d8-8d45-4dc5-8404-a056a4cf9535","originalAuthorName":"苏言杰"},{"authorName":"张德","id":"e0ef5dfa-5b86-4401-b522-7a8fa99e0285","originalAuthorName":"张德"},{"authorName":"徐建梅","id":"f74ad6de-7d81-43a2-b765-b831b8f60a15","originalAuthorName":"徐建梅"},{"authorName":"王辉","id":"1e9f404b-c35f-421d-9dcd-0ad3d41fffd5","originalAuthorName":"王辉"}],"doi":"","fpage":"142","id":"f10b4026-5eef-4a74-8370-7e2c55e14cec","issue":"z1","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"837cf475-16f6-486a-81ef-a9677e02efdd","keyword":"柠檬酸盐凝胶自燃烧法","originalKeyword":"柠檬酸盐凝胶自燃烧法"},{"id":"796e6263-86b8-40ed-96ce-b9bd413e2f4f","keyword":"超细粉体","originalKeyword":"超细粉体"},{"id":"c84077b6-9b6f-450d-a29e-82d88ab298b4","keyword":"影响因素","originalKeyword":"影响因素"},{"id":"8359493f-55c3-4cc7-a40d-6ed2a48a19ea","keyword":"低温合成","originalKeyword":"低温合成"}],"language":"zh","publisherId":"cldb2006z1046","title":"柠檬酸盐凝胶自燃烧法合成超细粉体","volume":"20","year":"2006"},{"abstractinfo":"稀磁半导体制备方法与磁性起源的研究是当前凝聚态物理的一项热门课题.首先介绍了自燃烧合成法的原理和优点,然后以Co和Mn掺杂ZnO为重点,总结了国内外采用自燃烧法合成的ZnO基稀磁半导体纳米颗粒晶体结构、磁性能相关的研究进展,讨论了所得纳米颗粒磁性能的内在物理机制.通过对自燃烧法合成的更宽掺杂范围ZnO基稀磁半导体纳米颗粒的研究,使我们能够更加系统地了解过渡金属掺杂ZnO材料的结构与磁性能,并探讨所得实验现象的内在物理机制.","authors":[{"authorName":"段利兵","id":"5e7ef68b-475d-4837-95dc-037b5202e56a","originalAuthorName":"段利兵"}],"doi":"","fpage":"16","id":"3c47dd1d-c418-4ad3-a086-86e263c8f558","issue":"9","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"aaf4d73b-fc06-4cc4-8509-5fd14c7cefe5","keyword":"稀磁半导体","originalKeyword":"稀磁半导体"},{"id":"bdd5827c-d6ac-4ee6-897a-10ff56299b7d","keyword":"ZnO","originalKeyword":"ZnO"},{"id":"87fcf9d8-8af7-4fa2-9a16-b10eb0ca8770","keyword":"晶体结构","originalKeyword":"晶体结构"},{"id":"2c6c8834-7a8c-465c-81b0-a2b478864ab8","keyword":"室温铁磁性","originalKeyword":"室温铁磁性"}],"language":"zh","publisherId":"cldb201009004","title":"自燃烧法合成的ZnO基稀磁半导体纳米颗粒研究进展","volume":"24","year":"2010"},{"abstractinfo":"以硝酸锆为锆源,采用溶胶-自燃烧法在700℃的热处理温度下合成出具有单一钙钛矿结构的PZT粉料.采用溶胶-自燃烧法合成的PZT为基料,在1050℃制备出PMZN陶瓷.采用XRD,SEM研究了PMZN陶瓷的结构,并测量了其介电性能和压电性能.结果表明:PMZN陶瓷为四方钙钛矿结构,其主要电学性能指标为:Kp为0.54,Qm为1073,tgδ小于或等于0.001,ε33=1236,d33=454pC/N,f s为136.1kHz.与以常规固相反应法合成PZT为基料的PMZN陶瓷相比,以溶胶-自燃烧法合成PZT为基料的PMZN陶瓷的烧结温度较低,而且综合电学性能更为优良.","authors":[{"authorName":"孙华君","id":"cd32c936-d0b7-4581-8d1d-32d148e566e9","originalAuthorName":"孙华君"},{"authorName":"陈文","id":"c9917f8a-a7df-42b8-8473-dd40dbfda039","originalAuthorName":"陈文"},{"authorName":"徐庆","id":"938a3325-d224-4778-a36c-bc953161f800","originalAuthorName":"徐庆"},{"authorName":"周静","id":"08ffe214-d0ab-484b-8aeb-87a97fea3972","originalAuthorName":"周静"},{"authorName":"刘晓芳","id":"cdb3d14a-ff1c-49d2-a97f-8f75aae945a2","originalAuthorName":"刘晓芳"}],"doi":"10.3969/j.issn.1001-1625.2004.05.025","fpage":"102","id":"dc5c4e6d-adf2-451e-8e12-af46defae8f0","issue":"5","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"fc9da47b-be3b-4575-acdb-25b23185c486","keyword":"溶胶-自燃烧法","originalKeyword":"溶胶-自燃烧法"},{"id":"25925327-f8b8-4dae-9ff3-0be40f17614c","keyword":"PMZN","originalKeyword":"PMZN"},{"id":"2f50fffd-78e7-480c-8d64-31bb9a5b0bfc","keyword":"压电陶瓷","originalKeyword":"压电陶瓷"},{"id":"2b5bcc21-8648-46e0-9b1e-4d05d212db2b","keyword":"居里温度","originalKeyword":"居里温度"}],"language":"zh","publisherId":"gsytb200405025","title":"以溶胶-自燃烧法合成PZT为基制备PMZN压电陶瓷","volume":"23","year":"2004"},{"abstractinfo":"以柠檬酸-硝酸盐溶液为前驱体,采用低温自燃烧法合成了具有K2NiF4结构的中温固体氧化物燃料电池La2NiO4阴极材料.研究了影响溶胶和凝胶的形成以及La2NiO4粉体晶相结构的影响因素,确定了最佳的合成条件.研究结果表明:自燃烧产物经1000 ℃煅烧2 h后,形成了平均粒径约为90 nm的单一La2NiO4相.经1300 ℃烧结的La2NiO4在100~800 ℃范围内平均热膨胀系数为13.9×10-6 K-1,在600~800 ℃范围内测得的总电导率为84.5~96.3 S·cm-1.","authors":[{"authorName":"龚明光","id":"a8319c50-b86c-41c6-a54d-3b901e7b288e","originalAuthorName":"龚明光"},{"authorName":"陆丽华","id":"b0e4c027-0672-4223-b208-552a891a503c","originalAuthorName":"陆丽华"},{"authorName":"金江","id":"6462d70f-802b-423d-91ae-525410b84a01","originalAuthorName":"金江"},{"authorName":"张华","id":"48660d1c-0400-44e3-a5f0-dc9282709031","originalAuthorName":"张华"}],"doi":"","fpage":"38","id":"3a9aef44-74a1-4b0c-a740-5c3f591dba30","issue":"1","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"c7b67b97-96d1-4590-a1d8-1d23af3bfd0d","keyword":"自燃烧","originalKeyword":"自燃烧"},{"id":"a9392ab3-f66c-4be9-9ce7-0ea05eb426e3","keyword":"阴极材料","originalKeyword":"阴极材料"},{"id":"025ce280-956c-4556-a1a6-393b25a8c396","keyword":"La2NiO4","originalKeyword":"La2NiO4"}],"language":"zh","publisherId":"gsytb200901008","title":"低温自燃烧法合成La2NiO4阴极材料及其性能","volume":"28","year":"2009"},{"abstractinfo":"用柠檬酸和乙二醇做络合剂和燃料, 硝酸盐做氧化剂, 用氨水调节溶胶pH值, 通过溶胶凝胶-自燃烧法一步合成了可用于固体氧化物燃料电池(SOFC)的新型固体电解质La9.33Si6O26. 用XRD、TEM等分析方法对合成粉体进行了物相测定与形貌观察, 并初步考察了粉体的烧结性能. 结果表明:通过工艺参数的有效设计, 溶胶-凝胶和自燃烧过程可以在短时间内达到合成所需要的高温, 一步合成粒径约为150~300nm的单相La9.33Si6O26超细粉体, 其烧结温度比固相法制备的粉体的烧结温度约低200℃.","authors":[{"authorName":"田长安","id":"8019ddc9-1f2b-4c0a-9f2f-c06340e77a75","originalAuthorName":"田长安"},{"authorName":"刘俊亮","id":"21903dac-4763-4a5e-acab-d813ad4dbdcb","originalAuthorName":"刘俊亮"},{"authorName":"蔡俊","id":"01e0de1a-c27e-45d8-ba7c-90952745abb8","originalAuthorName":"蔡俊"},{"authorName":"曾燕伟","id":"d5ab1b39-d60b-4b0c-b663-0b3ae277efad","originalAuthorName":"曾燕伟"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2008.00077","fpage":"77","id":"98613fdf-dd2b-4775-8ae0-a5357e125074","issue":"1","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"3d73c366-ef98-4aaa-8828-0bc73fd8eb0d","keyword":"La9.33 Si6 O26","originalKeyword":"La9.33 Si6 O26"},{"id":"52ac3850-81da-4732-b81f-10821f1c193c","keyword":" ultrafine powder","originalKeyword":" ultrafine powder"},{"id":"5426b071-0265-4506-bea3-8d524c25eb9b","keyword":" synthesis by self-combustion","originalKeyword":" synthesis by self-combustion"},{"id":"aa4ac5c3-2111-445b-b5a8-8877033ff255","keyword":" apatite-type electrolyte","originalKeyword":" apatite-type electrolyte"}],"language":"zh","publisherId":"1000-324X_2008_1_11","title":"溶胶凝胶-自燃烧法合成La 9.33Si 6O26超细粉体","volume":"23","year":"2008"},{"abstractinfo":"用柠檬酸和乙二醇做络合剂和燃料,硝酸盐做氧化剂,用氨水调节溶胶pH值,通过溶胶凝胶-自燃烧法一步合成了可用于固体氧化物燃料电池(SOFC)的新型固体电解质La9.33Si6O26.用XRD、TEM等分析方法对合成粉体进行了物相测定与形貌观察,并初步考察了粉体的烧结性能.结果表明:通过工艺参数的有效设计,溶胶-凝胶和自燃烧过程可以在短时间内达到合成所需要的高温,一步合成粒径约为150~300 nm的单相La9.33Si6O26超细粉体,其烧结温度比固相法制备的粉体的烧结温度约低200℃.","authors":[{"authorName":"田长安","id":"f129b3b1-a45b-4727-afd4-948e5ca7504b","originalAuthorName":"田长安"},{"authorName":"刘俊亮","id":"ed427a3b-906a-4853-a3f4-dc354875a39c","originalAuthorName":"刘俊亮"},{"authorName":"蔡俊","id":"51658ea0-147d-4747-9919-258f6bf55a13","originalAuthorName":"蔡俊"},{"authorName":"曾燕伟","id":"9e30fd01-38ae-430c-9504-4dde195a0781","originalAuthorName":"曾燕伟"}],"doi":"10.3321/j.issn:1000-324X.2008.01.015","fpage":"77","id":"a85c69b0-e548-4d42-833d-8c958683f339","issue":"1","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"e753cb90-abdd-49e7-9b08-c77c43c3aa54","keyword":"La9.33Si6O26","originalKeyword":"La9.33Si6O26"},{"id":"55533119-97b0-4a9f-9a4f-8e18815ddc7e","keyword":"超细粉体","originalKeyword":"超细粉体"},{"id":"15884fa6-8235-4392-b2e1-71b5d936efc3","keyword":"自燃烧法合成","originalKeyword":"自燃烧法合成"},{"id":"a5803484-8155-4b47-a067-b3a61981542f","keyword":"磷灰石型电解质","originalKeyword":"磷灰石型电解质"}],"language":"zh","publisherId":"wjclxb200801015","title":"溶胶凝胶-自燃烧法合成La9.33Si6O26超细粉体","volume":"23","year":"2008"},{"abstractinfo":"利用溶胶-凝胶自燃烧法合成了Ni0.25Cu0.25Zn0.5Fe2-xCexO4纳米晶铁氧体.借助DTA和XRD技术,对干凝胶的热分解过程、合成纳米晶的成分及其吸波性能进行了研究.结果表明,由金属硝酸盐和柠檬酸形成的干凝胶具有自燃烧的特性.通过自燃烧反应可以直接获得镍锌铜铁氧体粉末,经900℃热处理后可以转变成单一的尖晶石相,吸波性能测试发现,Ni0.25Cu0.25Zn0.5Fe2-xCexO4的吸波性能在8.2GHz~12.5GHz范围内随x的变化而不同,当x=0.07时,吸波性能最好,最高吸收峰值达到29.634dB.","authors":[{"authorName":"张伟","id":"7820a008-d425-425d-899c-3d6f5e361117","originalAuthorName":"张伟"},{"authorName":"李国栋","id":"ce87aa35-f3f3-4b46-ad89-3119af91a956","originalAuthorName":"李国栋"},{"authorName":"孙银凤","id":"bc8cd36a-7868-48c5-9758-663e5e255f44","originalAuthorName":"孙银凤"}],"doi":"10.3969/j.issn.1004-0277.2007.04.010","fpage":"43","id":"e9703260-42d6-4731-8e74-824a0864152a","issue":"4","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"4590f561-bfba-4556-be92-ffa16841012b","keyword":"溶胶-凝胶","originalKeyword":"溶胶-凝胶"},{"id":"b67aea03-d75c-44d4-b6c9-2bed9d0f4862","keyword":"自燃烧","originalKeyword":"自燃烧"},{"id":"15729e51-3b95-46c1-8b0f-313165c3c198","keyword":"Ni0.25Cu0.25Zn0.5Fe2-xCexO4","originalKeyword":"Ni0.25Cu0.25Zn0.5Fe2-xCexO4"},{"id":"11d085e0-ca41-43d3-82c1-9d78b64309fd","keyword":"吸波性能","originalKeyword":"吸波性能"},{"id":"8ca1947c-58e4-438e-8a5e-c2b48ee608ff","keyword":"稀土","originalKeyword":"稀土"}],"language":"zh","publisherId":"xitu200704010","title":"溶胶-凝胶自燃烧法合成镍铜锌纳米晶铁氧体及其吸波性能的研究","volume":"28","year":"2007"},{"abstractinfo":"本文研究了影响自燃烧工艺的几个工艺条件,如溶液PH值、溶液中水含量、加热温度等因素对凝胶化的影响;利用差热热重分析仪和X射线衍射仪分析了干凝胶的热历程及产物的物相结构.结果表明,自燃烧粉末的晶化峰温为 509℃,在 800℃ 煅烧2h即可得到晶化的一次颗粒<50nm的BaNd2Ti5O14粉末,并分析了产生温度差异的原因。","authors":[{"authorName":"张明福","id":"ff143a7d-c93c-4b0c-ab93-0db2e84aff38","originalAuthorName":"张明福"},{"authorName":"赫晓东","id":"9d8e068f-cbe3-4688-98ba-8631ffc5f7fd","originalAuthorName":"赫晓东"},{"authorName":"韩杰才","id":"f4f8cc3c-727d-48de-a579-d9e045b1fbe6","originalAuthorName":"韩杰才"},{"authorName":"杜善义","id":"01b29847-c75b-4ee5-b495-3f4aa41a0f21","originalAuthorName":"杜善义"}],"categoryName":"|","doi":"","fpage":"879","id":"0c6d1fcd-37a4-4bed-be49-04af090a7407","issue":"5","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"b8d1aeef-7f7e-4773-a8d1-d41c6be1138b","keyword":"凝胶化","originalKeyword":"凝胶化"},{"id":"72e71b6f-2379-4c0c-9b60-7dea35251562","keyword":" autocombustion","originalKeyword":" autocombustion"},{"id":"f949c7e9-dbb4-40ef-b4f3-4babcbac7ca6","keyword":" BaNd2Ti5O14","originalKeyword":" BaNd2Ti5O14"},{"id":"f77e891b-df36-4d6a-b9eb-422e14160a2e","keyword":" crystallize","originalKeyword":" crystallize"}],"language":"zh","publisherId":"1000-324X_2000_5_19","title":"自燃烧法合成BaNd2Ti5O14的凝胶化及热处理研究","volume":"15","year":"2000"},{"abstractinfo":"本文研究了影响自燃烧工艺的几个工艺条件, 如溶液pH值、溶液中水含量、加热温度等因素对凝胶化的影响; 利用差热热重分析仪和X射线衍射仪分析了干凝胶的热历程及产物的物相结构. 结果表明, 自燃烧粉末的晶化峰温为509C, 在800C煅烧2h即可得到晶化的一次颗粒<50nm的BaNd2Ti5O14粉末, 并分析了产生温度差异的原因.","authors":[{"authorName":"张明福","id":"bfe57705-ffea-4cb5-a609-3158cdd1882b","originalAuthorName":"张明福"},{"authorName":"赫晓东","id":"c4a153e2-243e-4452-9f58-f0fd171cca01","originalAuthorName":"赫晓东"},{"authorName":"韩杰才","id":"47ad7d2f-f171-4c5e-92e1-1756e1fd5b78","originalAuthorName":"韩杰才"},{"authorName":"杜善义","id":"2cf2a1d8-d23e-4184-8e4e-6aa1d62c2e74","originalAuthorName":"杜善义"}],"doi":"10.3321/j.issn:1000-324X.2000.05.019","fpage":"879","id":"3d3cc90a-c171-4650-858f-1aad81439689","issue":"5","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"7f741964-1cbf-449b-90e5-496340483d8c","keyword":"凝胶化","originalKeyword":"凝胶化"},{"id":"799a85be-2deb-44dd-b7da-75c6f69ce64a","keyword":"自燃烧","originalKeyword":"自燃烧"},{"id":"3e80b247-b2c2-47c7-882c-1114b373a50d","keyword":"BaNd2Ti5O14","originalKeyword":"BaNd2Ti5O14"},{"id":"91a80319-3fef-4d2d-9fa0-e90275e840ef","keyword":"晶化","originalKeyword":"晶化"}],"language":"zh","publisherId":"wjclxb200005019","title":"自燃烧法合成 BaNd2Ti5O14的凝胶化及热处理研究","volume":"15","year":"2000"}],"totalpage":3587,"totalrecord":35861}