A novel route to prepare nanocomposites was illustrated through preparing overbased calcium petroleum sulfonate lubricating oil detergent, where the rotating packed bed (RPB) was used as reactor in place of conventional reaction vessel. The results showed that the carbonation efficiency is improved, the raw materials consumption is reduced, and the dispersibilities, sizes and morphologies of nano-sized CaCO3 particles in overbased detergent are enhanced. It is deduced reasonably that this route can be extensively applied to nanocomposites preparation in appropriate conditions and would be a platform technology in this field.
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