{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"目前<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>碲的方法主要有苏打粉焙烧法、碱性高压浸出法、硫酸化焙烧法、氧化酸浸法、萃取法、液膜法、微生物法、电解精炼法、真空蒸馏法、区熔精炼法等,其中电解精炼法得到的碲的纯度达到99.99%,真空蒸馏碲的纯度达到99.999%.区熔精炼碲的纯度可达99.999995%,本文综述了以上<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>碲的方法.","authors":[{"authorName":"程琍琍","id":"6486a9d9-1e3e-40f6-a7e6-6432eeda834f","originalAuthorName":"程琍琍"},{"authorName":"李啊林","id":"7a4ac665-a741-41f9-ac31-2ce1c21da1e7","originalAuthorName":"李啊林"}],"doi":"10.3969/j.issn.0258-7076.2008.01.023","fpage":"115","id":"6a9afad4-16c9-4ebf-9e87-d67b6e514956","issue":"1","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"eac6dce4-33c6-4d7e-bbb1-020a022b587e","keyword":"萃取","originalKeyword":"萃取"},{"id":"2a282729-c23c-4fa7-baab-d233ce7b7161","keyword":"液膜法","originalKeyword":"液膜法"},{"id":"63e89e32-bc8c-4c2e-9649-d79d65ac351f","keyword":"电解精炼","originalKeyword":"电解精炼"},{"id":"a58133ce-7a5b-4663-a2d7-bbf592899419","keyword":"真空蒸馏","originalKeyword":"真空蒸馏"},{"id":"bb4e4539-c457-4e45-8d11-8ca930ca6a60","keyword":"区熔精炼","originalKeyword":"区熔精炼"},{"id":"ad29e790-9a3d-4f2f-bfec-378d213739b7","keyword":"碲","originalKeyword":"碲"},{"id":"a7879da1-4523-4500-81f2-652405bc3251","keyword":"<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>","originalKeyword":"分离提纯"}],"language":"zh","publisherId":"xyjs200801023","title":"碲的<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>技术研究进展","volume":"32","year":"2008"},{"abstractinfo":"离子交换法是铂族金属湿法冶金中一项很有应用前景的绿色环保技术，与传统的化学沉淀法和溶剂萃取法相比有很多优势，因此在铂族金属的<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>中得到了广泛的应用。针对铂族金属二次资源回收，介绍了阳离子交换树脂在铂族金属与贱金属<span style=\"color:red\">分离</span>中的工业应用和阴离子交换树脂在铂族金属富集、<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>中的研究及应用；同时也对分子识别技术在铂族金属<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>领域的应用做了简要的介绍。","authors":[{"authorName":"谭明亮","id":"43643ba0-9055-4419-a236-83ea90353403","originalAuthorName":"谭明亮"},{"authorName":"王欢","id":"979250a9-151d-4c0a-ad6c-da3937fe2724","originalAuthorName":"王欢"},{"authorName":"贺小塘","id":"e64a8ca9-390b-467c-9b9f-7d325136e40a","originalAuthorName":"贺小塘"},{"authorName":"郭俊梅","id":"6fa501db-6e0f-4894-9078-96d3f466eec9","originalAuthorName":"郭俊梅"},{"authorName":"韩守礼","id":"041d734f-9ae0-4a81-882c-830ced769fa7","originalAuthorName":"韩守礼"},{"authorName":"李红梅","id":"f4eed825-1320-4f4a-af5b-f26569125639","originalAuthorName":"李红梅"},{"authorName":"赵雨","id":"3aee2c67-969e-4d9f-9b6d-d3330a319f7d","originalAuthorName":"赵雨"},{"authorName":"李勇","id":"14c31e6e-4b67-40cf-823f-07960f02c82e","originalAuthorName":"李勇"},{"authorName":"吴喜龙","id":"cac78b72-59c9-4493-ad12-a6804b898150","originalAuthorName":"吴喜龙"},{"authorName":"余青智","id":"26389804-5b01-4f5b-9dc3-8cc009d94f2c","originalAuthorName":"余青智"}],"doi":"","fpage":"30","id":"a1c09960-457c-4116-8975-1195f99afa6f","issue":"z1","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"af0ce4ad-fc36-4d11-b5a7-c462d19dc8b7","keyword":"冶金技术","originalKeyword":"冶金技术"},{"id":"7f3e2dce-ab2e-4d15-be4a-86715ce28756","keyword":"离子交换","originalKeyword":"离子交换"},{"id":"3130d121-013d-4937-bbb3-3ae30ea7e268","keyword":"铂族金属","originalKeyword":"铂族金属"},{"id":"477a7407-f756-413c-9fab-11a6f5c7bfbd","keyword":"<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>","originalKeyword":"分离提纯"},{"id":"2707d669-3ee1-4958-b6cf-abfaa80405be","keyword":"废催化剂","originalKeyword":"废催化剂"},{"id":"b5330a29-ecb5-41e2-a1a7-bc5441f6a760","keyword":"回收","originalKeyword":"回收"}],"language":"zh","publisherId":"gjs2013z1008","title":"离子交换技术在铂族金属富集、<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>中的应用","volume":"","year":"2013"},{"abstractinfo":"甘蓝型(Brassica oleracea)油菜籽中硫甙混合物用70%甲醇提取后,依次通过酸性氧化铝色谱柱和反相碳十八硅胶柱<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>,得到1-硫[(1Z)-3-羟基-1-[(磺氧基)亚氨基]-4-戊烯基]-1-硫代-β-D-葡萄糖钾盐(progoitrin). 表征了progoitrin的结构,测定了progoitrin的纯度. 并测试了用硫甙混合物及纯化硫甙作为化学抗癌剂的抗肿瘤活性. 实验结果显示,混合硫甙和纯化硫甙的降解产物对小鼠S180实体瘤均具有抑制作用,按60 mg/kg硫甙剂量给药时,抑瘤率分别达到67.3%和59.5%.","authors":[{"authorName":"周锦兰","id":"21a1a7de-d690-46e7-a16d-1ef3044416f9","originalAuthorName":"周锦兰"},{"authorName":"俞开潮","id":"b91d3f97-65a5-4299-9fb5-556aab95a96d","originalAuthorName":"俞开潮"}],"doi":"10.3969/j.issn.1000-0518.2005.10.007","fpage":"1075","id":"fe349ab2-d1e3-4203-a945-44017a4e4b56","issue":"10","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"9ac9eb76-ffba-470b-b1e6-42de5f97308e","keyword":"硫代葡萄糖苷","originalKeyword":"硫代葡萄糖苷"},{"id":"0f033de9-efe0-4080-b5ec-8e5d3bfcd3ae","keyword":"<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>","originalKeyword":"分离提纯"},{"id":"8f0726bc-d06c-48f3-83ac-81573183645a","keyword":"S180","originalKeyword":"S180"},{"id":"0de9cf03-5d65-40fa-a18c-a8df2ece543e","keyword":"抗肿瘤作用","originalKeyword":"抗肿瘤作用"}],"language":"zh","publisherId":"yyhx200510007","title":"油菜籽中主要硫甙的<span style=\"color:red\">提纯</span>与抗肿瘤活性","volume":"22","year":"2005"},{"abstractinfo":"纳米金刚石具有金刚石和纳米材料的双重特性,具有广阔的应用前景.介绍了纳米金刚石的爆轰合成与<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>、纳米金刚石的基本性质与检测表征、纳米金刚石的应用研究领域和最新研究动态.","authors":[{"authorName":"罗立群","id":"541fec2d-9fe4-4881-8f6c-0f9705c659cd","originalAuthorName":"罗立群"},{"authorName":"张泾生","id":"60e695d9-8d4f-4876-8d03-9856a59ba38c","originalAuthorName":"张泾生"},{"authorName":"朱永伟","id":"bf94de56-21c7-494e-8e99-c6b630a9e4eb","originalAuthorName":"朱永伟"}],"doi":"","fpage":"127","id":"85bf4ae6-d005-4656-9051-cecbdfdc416f","issue":"z2","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"ffd5ec81-c1f2-4bbc-8bfa-1208c6db3425","keyword":"纳米金刚石","originalKeyword":"纳米金刚石"},{"id":"d23f5d8f-99bf-4d95-8271-8d349db19a46","keyword":"爆轰合成","originalKeyword":"爆轰合成"},{"id":"3dfcf568-cb49-4e9e-8b72-d116c668bfb8","keyword":"<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>","originalKeyword":"分离提纯"},{"id":"ca4086e9-d2b4-44a3-87db-98c7a3c072ce","keyword":"应用","originalKeyword":"应用"}],"language":"zh","publisherId":"cldb2004z2038","title":"纳米金刚石的研究与应用现状","volume":"18","year":"2004"},{"abstractinfo":"纳米碳管是一种新型的纳米材料,有着独特的结构和性能.本文对纳米碳管的制备方法和<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>技术进行了简要的综述.","authors":[{"authorName":"刘伟良","id":"8460539c-1c7d-4e67-afef-e7cb5b38d5ea","originalAuthorName":"刘伟良"},{"authorName":"梁忠友","id":"dc808f9d-b5bc-4777-ad52-a9d6576b6d20","originalAuthorName":"梁忠友"}],"doi":"10.3969/j.issn.1001-1625.2002.05.006","fpage":"26","id":"d2ffc202-0be2-45cf-ba79-8cd3e9cba687","issue":"5","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"05f62b2a-c23f-41ba-89c5-c2ea1fe92154","keyword":"纳米碳管","originalKeyword":"纳米碳管"},{"id":"82741227-eed8-47b9-aad9-4fcb6661c02b","keyword":"制备方法","originalKeyword":"制备方法"},{"id":"6fde5fce-59bd-4bfd-86a5-becd3bc82937","keyword":"<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>","originalKeyword":"分离提纯"}],"language":"zh","publisherId":"gsytb200205006","title":"纳米碳管的制备和纯化","volume":"21","year":"2002"},{"abstractinfo":"研究了AuPt合金中Au与Pt的<span style=\"color:red\">分离</span>及Pt的<span style=\"color:red\">提纯</span>工艺,拟定了AuPt合金的<span style=\"color:red\">分离</span>和Pt<span style=\"color:red\">提纯</span>的工艺步骤,通过批量生产,获得了满意的结果.在使用还原剂将Au和Pt<span style=\"color:red\">分离</span>后,Au不需再<span style=\"color:red\">提纯</span>,其纯度可达99.9%;将Pt<span style=\"color:red\">提纯</span>后其纯度可迭99.99%;物料总回收率>98.6%.","authors":[{"authorName":"翟步英","id":"46db8b21-d79f-4b46-81f8-42aaee8d97f3","originalAuthorName":"翟步英"},{"authorName":"刘庆宾","id":"83049a16-9f27-4e18-86ea-5be129d4a160","originalAuthorName":"刘庆宾"},{"authorName":"段明江","id":"15e29b9a-c511-4ee2-96b6-2e8e1d05edc5","originalAuthorName":"段明江"}],"doi":"","fpage":"527","id":"9d3622bd-d2b6-4e8a-ac98-c0018c533fae","issue":"3","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"475e7522-3927-4955-9219-04516b49b595","keyword":"AuPt合金","originalKeyword":"AuPt合金"},{"id":"7b0fe69e-cf9d-46d1-b2b4-828f612a5987","keyword":"还原剂","originalKeyword":"还原剂"},{"id":"be8b5022-5237-40dc-bcba-cbc7f091ecdc","keyword":"一次<span style=\"color:red\">分离</span>","originalKeyword":"一次分离"},{"id":"cdf73525-d1e7-41d5-aed5-270ab9521bbe","keyword":"<span style=\"color:red\">提纯</span>","originalKeyword":"提纯"},{"id":"c0a0246a-61be-4497-b940-f5c40d722c0d","keyword":"Pt","originalKeyword":"Pt"}],"language":"zh","publisherId":"gncl200903051","title":"AuPt合金的<span style=\"color:red\">分离</span>及Au、Pt<span style=\"color:red\">提纯</span>的研究","volume":"40","year":"2009"},{"abstractinfo":"用柱色谱方法从甘蓝型油菜籽中<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>了1-硫[(1Z)-3-羟基-1-[(磺酸基)亚氨基]-4-戊烯基]-1-硫代-β-D-葡萄糖钾盐(progoitrin).用甲醇溶液提取菜籽中的硫甙,得到粗提物;粗提物经酸性氧化铝色谱柱与反相C18硅胶柱进一步<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>,得到纯品.对纯品进行紫外光谱、红外光谱、核磁共振氢谱、质谱和元素分析,测得的数据与文献值相符.用高效液相色谱测得硫甙提取物的纯度为99% .该方法操作简便,得到的硫甙样品纯度高,是一种有价值的硫甙提取方法,具有良好的应用前景.","authors":[{"authorName":"周锦兰","id":"d92db10e-10ec-4107-bb8c-0f411746e5b5","originalAuthorName":"周锦兰"},{"authorName":"胡健华","id":"78bc61b7-2174-43de-ba0c-5956ae95c56d","originalAuthorName":"胡健华"},{"authorName":"裘爱泳","id":"98e9d57a-9fa4-4a0a-98c3-cfc171a42565","originalAuthorName":"裘爱泳"}],"doi":"10.3321/j.issn:1000-8713.2005.04.019","fpage":"411","id":"f3959dc1-c8e9-4048-a329-e90c7e3485b8","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"a64e50a8-248e-4638-b4d4-58e6f73b0822","keyword":"柱色谱","originalKeyword":"柱色谱"},{"id":"df339a26-fc55-4ea0-a14f-f7c1b5e96f1f","keyword":"硫甙","originalKeyword":"硫甙"},{"id":"d63e4cea-9719-45bb-9f8e-359dd7d48259","keyword":"<span style=\"color:red\">分离</span>","originalKeyword":"分离"},{"id":"d09397e9-ee75-4f44-a3bc-3ebbb27ef133","keyword":"<span style=\"color:red\">提纯</span>","originalKeyword":"提纯"},{"id":"cff98d1d-fc0f-4734-98dd-72dddaa3b2ef","keyword":"油菜籽","originalKeyword":"油菜籽"}],"language":"zh","publisherId":"sp200504019","title":"油菜籽中主要硫甙的<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>","volume":"23","year":"2005"},{"abstractinfo":"采用水提一超滤法<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>无患子皂苷.实验考察了絮凝剂的用量,超滤时温度、膜面流速、压力、超滤液pH、膜截留分子量等对<span style=\"color:red\">分离</span>纯化效果的影响.结果表明在水提液中加入体积分数为2.0%的壳聚糖一醋酸絮凝剂时,预处理效果较好.正交实验表明,采用截留分子量为20 K-50 K的超滤膜,在温度25℃、膜面流速2.78×10-5 m/s、压力0.08 MPa的条件下,所得无患子总皂苷的纯度可达67.02%;而采用6 K超滤膜所得无患子皂苷的产品纯度可达.72.42%.","authors":[{"authorName":"魏凤玉","id":"31b63d9b-3463-49df-9337-3d39c4ed7c8e","originalAuthorName":"魏凤玉"},{"authorName":"解辉","id":"a42406af-d44a-4544-ac46-36ac5c2f8d85","originalAuthorName":"解辉"},{"authorName":"余锦城","id":"fb059451-a32b-44fb-8453-d567a35fcddf","originalAuthorName":"余锦城"},{"authorName":"吴阳","id":"c6ad9b50-1704-46c3-a739-f53dbc65e458","originalAuthorName":"吴阳"}],"doi":"10.3969/j.issn.1007-8924.2008.02.017","fpage":"85","id":"ecf1680b-6150-491e-87f7-27646db7162e","issue":"2","journal":{"abbrevTitle":"MKXYJS","coverImgSrc":"journal/img/cover/MKXYJS.jpg","id":"54","issnPpub":"1007-8924","publisherId":"MKXYJS","title":"膜科学与技术   "},"keywords":[{"id":"2701caea-516b-47b8-bd8f-686a8cf7d674","keyword":"无患子皂苷","originalKeyword":"无患子皂苷"},{"id":"fb903ebc-b55a-48bc-bf0f-b7c5d4162a53","keyword":"正交实验","originalKeyword":"正交实验"},{"id":"fbf163e4-f61d-4105-9777-68525d595161","keyword":"水提","originalKeyword":"水提"},{"id":"0fbf9349-bc3a-408b-8af2-6ecd1a7e45c9","keyword":"超滤","originalKeyword":"超滤"}],"language":"zh","publisherId":"mkxyjs200802017","title":"超滤法<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>无患子皂苷","volume":"28","year":"2008"},{"abstractinfo":"本文在深入分析含CO2混合气低温相变<span style=\"color:red\">分离</span>法特点与精馏特性的基础上，提出一种新型的CO2<span style=\"color:red\">分离</span>液化<span style=\"color:red\">提纯</span>一体化系统。该系统通过多级压缩，多级冷却与多级<span style=\"color:red\">分离</span>，可将混合气体中绝大部分CO2在较低能耗代价下以液态<span style=\"color:red\">分离</span>出来；同时，通过对<span style=\"color:red\">分离</span>出的粗CO2液体进行高压、近常温条件下的精馏，实现其低能耗<span style=\"color:red\">提纯</span>；最终实现以较低能耗<span style=\"color:red\">分离</span>回收cO2、而<span style=\"color:red\">分离</span>出的CO2纯度可达99．99％。本文研究成果为从具有较高CO2浓度的混合气体中<span style=\"color:red\">分离</span>回收CO2提供了新的思路与途径。","authors":[{"authorName":"徐钢","id":"68f2834f-befb-41e3-8d22-e4ed8234df55","originalAuthorName":"徐钢"},{"authorName":"田龙虎","id":"8c721b03-e0b6-46da-a578-ff1208f1601d","originalAuthorName":"田龙虎"},{"authorName":"杨勇平","id":"09d69c93-a8be-45e4-9878-da2cadc4dffb","originalAuthorName":"杨勇平"},{"authorName":"刘彤","id":"96a8e85c-db53-471b-8597-1a22f918e742","originalAuthorName":"刘彤"},{"authorName":"段立强","id":"716c9aaf-3ea4-4b55-83d2-5de5988033ff","originalAuthorName":"段立强"}],"doi":"","fpage":"1987","id":"b9b0c2bd-c714-4f0b-94d5-e7f5578fd2a1","issue":"12","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"f2cbfc0b-9405-4ac0-aea6-6418be614846","keyword":"CO2回收","originalKeyword":"CO2回收"},{"id":"909741f9-0bc7-4fa3-84e7-ae939c4db121","keyword":"低温<span style=\"color:red\">分离</span>法","originalKeyword":"低温分离法"},{"id":"acd6bcee-48a3-4ba3-af2f-b1225ef24822","keyword":"精馏","originalKeyword":"精馏"},{"id":"64251e47-9636-4c41-9d67-30cfd579c987","keyword":"富氧燃烧","originalKeyword":"富氧燃烧"}],"language":"zh","publisherId":"gcrwlxb201112003","title":"新型CO2<span style=\"color:red\">分离</span>液化<span style=\"color:red\">提纯</span>一体化系统","volume":"32","year":"2011"},{"abstractinfo":"分子识别技术(MRT)具有选择性高、生产周期短、成本低、操作简单、分子识别材料可反复使用等优点.介绍了分子识别的原理和基本工艺,列举了分子识别技术在铂族金属(PGMs)<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>中的商业应用.","authors":[{"authorName":"贺小塘","id":"f709cf31-41be-4d22-a9b9-726abd5054c8","originalAuthorName":"贺小塘"},{"authorName":"韩守礼","id":"73196848-c809-414d-9cbc-598467bf420a","originalAuthorName":"韩守礼"},{"authorName":"吴喜龙","id":"e1bfa43c-b0d5-4885-a8b8-3ca2b789b313","originalAuthorName":"吴喜龙"},{"authorName":"王欢","id":"66d87ed1-d9f9-43b9-ab37-dee3837bc69d","originalAuthorName":"王欢"},{"authorName":"王咏梅","id":"06692f70-394d-447f-b63a-ffb12162cdf6","originalAuthorName":"王咏梅"}],"doi":"10.3969/j.issn.1004-0676.2010.01.013","fpage":"53","id":"e0da952f-1c88-4ae2-9c2c-a9d3a951f576","issue":"1","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"21b3d912-ea1f-4ed9-b643-2839de21210d","keyword":"冶金技术","originalKeyword":"冶金技术"},{"id":"315c4003-a359-46a0-8ecf-2816fde389ed","keyword":"分子识别技术","originalKeyword":"分子识别技术"},{"id":"640f7610-94e5-4926-ac33-90a7a3e6e32c","keyword":"铂族金属","originalKeyword":"铂族金属"},{"id":"4080f9fa-6635-409a-b64f-5eda370936c9","keyword":"<span style=\"color:red\">分离</span>","originalKeyword":"分离"},{"id":"417a81cd-1b82-40bd-9916-8ab695e89c55","keyword":"回收","originalKeyword":"回收"}],"language":"zh","publisherId":"gjs201001013","title":"分子识别技术在铂族金属<span style=\"color:red\">分离</span><span style=\"color:red\">提纯</span>中的应用","volume":"31","year":"2010"}],"totalpage":757,"totalrecord":7563}