欢迎登录材料期刊网

材料期刊网

高级检索

目的:进一步提高电沉积 Fe-ZrO2纳米复合镀层的性能。方法在45#钢基体表面电沉积 Fe-ZrO2纳米复合镀层,并进行激光重熔后处理。通过正交实验分析激光重熔参数对镀层显微硬度、结合力和表面形貌的影响,并优化重熔工艺。结果优化的工艺为:电流150 A,脉宽8 ms,频率15 Hz,扫描速率250 mm/ min,负离焦量2 mm。镀层经激光重熔后,硬度提高,纳米颗粒得到了细化,与基体形成了冶金结合。结论激光重熔可以改善 Fe-ZrO2纳米复合镀层的微观形貌,提高其性能。

Objective To further enhance the properties of Fe-ZrO2 Nanocomposite ceramic coating. Methods The Fe-ZrO2 nanocomposite ceramic coating was prepared on 45 steel surface by electrodeposition and then processed by laser remelting coating. A set of orthogonal experiments were used to analyze the effects of laser remelting parameters on the coating microstructure, hard-ness and binding force and optimize the remelting process. Results The optimized process was drawn as the followings: current 150 A, impulse width 8ms, frequency 15 Hz, scan rate 250 mm/ min, negative defocus amount 2 mm. After the laser remelted, the coating hardness had been improved, nanoparticles had been refined, the metallurgical bond had been formed between the coating and substrate. Conclusion The results show that after the laser remelting, the morphology and properties of Fe-ZrO2 nanocomposite ceramic coating have been improved.

参考文献

[1] 李荣久. 陶瓷-金属复合材料[M]. 北京:冶金工业出版社,2002. LI Rong-jiu. The Ceramic Metal Composite Materials[M]. Beijing:Metallurgical Industry Press,2002.,2002.
[2] ALIREZAEI,MONIRVAGHEFI S M,SALEHI M . Effect of Alumina Content on Surface Morphlogy and Hardness of Ni-P-Al2 O3(a)Electroless Composite Coatings[J].Surface and Coatings Technology,2004,184
[3] YANG X Y,PENG X,CHEN J . Effect of a Small Increase in the Ni Content on the Properties of a Laser Surface Clad Fe-based Alloy[J].Applied Surface Science,2007,253(9):4420-4426.,2007.
[4] 舒绪刚,何湘柱,黄慧民,傅维勤,温立哲,姬文晋.纳米ZrO2在复合镀中的应用[J].机械工程材料,2008(03):1-4,12.
[5] 刘娜娜,吴蒙华,李智,王元刚.磁场作用下电沉积镀层技术的研究进展[J].稀有金属材料与工程,2013(03):649-654.
[6] 苗斌,贾卫平,吴蒙华,杨帆.磁场作用下电沉积镍层织构及表面形貌分析[J].表面技术,2012(05):30-33.
[7] HSIEH Y C,CHANG L C,TSENG Y C . Structural Charac-terizations of PtRu Nano Particles by Galvanostatic Pulse Electrodeposition[J].Journal of Alloys and Compounds,2014,583
[8] 陈维平,杨少锋,韩孟岩.陶瓷/铁基合金复合材料的研究进展[J].中国有色金属学报,2010(02):257-266.
[9] 黄燕滨,邵新海,宋高伟,仲流石.陶瓷涂层性能影响因素及工艺优化研究[J].装备环境工程,2012(01):90-93.
[10] 王东生,田宗军,沈理达,刘志东,黄因慧.激光表面熔覆制备纳米结构涂层的研究进展[J].中国激光,2008(11):1698-1709.
[11] 杨宁,杨帆.激光功率对WO3-V2O5-C镍基熔覆层硬度的影响[J].表面技术,2013(05):39-41.
[12] 李崇桂,于治水,张有凤 . 激光重熔 Al2 O3-TiO2 涂层的界面结合及划痕破坏失效行为[J].材料热处理学报,2013,34:156-162. LI Chong-gui, YU Zhi-shui, ZHANG You-feng. Bonding State and Scratch Failure Behavior of Laser Remelted Al2 O3-TiO2 Coatings [J]. Transactions of Materials and Heat Treatment,2013,34(Supplement):156-162.,2013.
[13] 赵冠琳 .激光熔覆原位反应生成TiC-VC增强铁基熔覆层的研究[D].山东大学,2008.
[14] HU C,BAKER T N . A Semi-empirical Model to Predict the Melt Depth Developed in Overlapping Laser Tracks on a Ti-6Al-4V Alloy[J].Journal of Materials Processing Technolo-gy,1999,94
[15] 毛怀东 .激光熔覆层裂纹控制方法与实践[D].天津大学,2007.
[16] 相珺,李刚,邱玲,况军,邱星武.ZrO2增强镍基激光熔覆层的组织与性能[J].机械工程材料,2009(02):59-62.
[17] 齐勇田,生利英.激光熔覆工艺参数对熔覆层组织的影响[J].应用激光,2011(04):322-326.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%