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以硝酸锶、钛酸四丁酯和氢氧化钾为原料,采用水热法制备了纳米SrTiO3粉体,用XRD、SEM、激光粒度分析仪等研究了制备过程中非离子表面活性剂SPAN80含量对纳米SrTiO3粉体物相、形貌、粒径和极性的影响.结果表明:表面活性剂SPAN80的添加对SrTiO3粉体晶型结构没有影响,且有效减弱了粉体的团聚;在SPAN80最佳添加量10%(体积分数)的条件下,制备得到SrTiO3粉体的颗粒尺寸约为39 nm,并呈球形;极性的SrTiO3粉体被SPAN80包裹后变成了非极性粉体.

参考文献

[1] Wenjun Dong;Xiaoyun Li;Jie Yu;Wanchun Guo;Bingjie Li;Li Tan;Chaorong Li;Jianjun Shi;Ge Wang .Porous SrTiO_3 spheres with enhanced photocatalytic performance[J].Materials Letters,2012(1):131-134.
[2] Chandy N. George;J.K. Thomas;R. Jose .Synthesis and characterization of nanocrystalline strontium titanate through a modified combustion method and its sintering and dielectric properties[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2009(1/2):711-715.
[3] T. Xian;H. Yang;J.F. Dai;Z.Q. Wei;J.Y. Ma;W.J. Feng .Photocatalytic properties of SrTiO_3 nanoparticles prepared by a polyacrylamide gel route[J].Materials Letters,2011(21/22):3254-3257.
[4] Hiroyuki Ishikawa;Kouya Oohira;Tatsuo Nakajima .Combustion synthesis of SrTiO_3 using different raw materials[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2008(1/2):384-388.
[5] Low temperature molten salt synthesis of SrTiO_3 submicron crystallites and nanocrystals in the eutectic NaCl-KCl[J].Materials Letters,2010(3):431.
[6] Y.M.Rangel-Hernandez;J.C.Rendon-Angeles;Z. Matamoros-Veloza .One-step synthesis of fine SrTiO3 particles using SrSO4 ore under alkaline hydrothermal conditions[J].Chemical engineering journal,2009(1/2):483-492.
[7] 方惠会,王开毅,薛松.碳酸铵共沉淀法制备高纯超细钛酸锶粉体[J].功能材料,2000(04):408-409,415.
[8] 徐明霞,郑嘹赢,孙清池,杨义敏,徐廷献.无机盐原料溶胶-凝胶工艺合成高纯超细钛酸锶粉料[J].硅酸盐学报,2000(02):184-186.
[9] 罗昆鹏 .微波水热合成钛酸钡纳米粉体[D].西安科技大学,2009.
[10] K. Byrappa;T. Adschiri .Hydrothermal technology for nanotechnology[J].Progress in Crystal Growth and Characterization of Materials,2007(2):117-166.
[11] 吴建鹏,曹丽云,贺海燕,黄剑锋.纳米材料的颗粒尺寸分析方法[J].热加工工艺,2007(12):72-74.
[12] 付猛,岳艳娟,祝雅娟,陈志刚.水热法制备石墨烯及其表征[J].机械工程材料,2013(06):84-88.
[13] 位莉,苏慧兰,张荻.纳米结构金属氧化物气敏材料的研究进展[J].机械工程材料,2013(01):5-9,80.
[14] 朱丽慧,马学鸣.Fe-Ni系纳米材料马氏体相变的研究进展[J].机械工程材料,2002(12):1-4,34.
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