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以水作为溶剂,将水溶性吡咯衍生物单体(碘化N,N,N-三甲基-(2-吡咯-1-乙基))与V2O5溶胶混合,进行原位插层聚合反应,合成PTPAI/V2O5插层纳米复合材料.采用XRD,FT-IR和SEM对其结构和形貌进行了分析.聚(N,N,N-三甲基-(2-吡咯-1-乙基)/V2O5的doo1面间距从10.7739nm增大到13.5436nm,表明聚吡咯衍生物已插入V2O5干凝胶的层间,其FT-IR光谱说明聚吡咯与V2O5层存在着较强的相互关系,SEM图谱揭示了聚(N,N,N-三甲基-(2-吡咯-1-乙基)在V2O5层间附着的形貌特征.

参考文献

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