采用硫酸盐与氢氧化钠沸腾回流共沉淀法制备的锰锌铁氧体纳米粉体,通过XRD、VSM和激光粒度分析对不同温度预烧粉体进行了物相、磁学性能、粉体粒度的研究,同时研究了这些粉体经过成型,烧结,所得到环形烧结体的磁感应强度和微观结构.结果表明:预烧温度为600℃时,饱和磁化强度为59.36 emu/g,而600℃预烧的粉体经过成型,在1000℃烧结所得到的环形烧结体,室温时饱和磁感应强度Bs为0.417 T,微观结构匀称,缺陷较少,空洞较少,晶粒大小在3 μm左右.
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