以金属盐为原料,将溶胶-凝胶和燃烧法相结合,制备Co0.5Mg05Al2O4复合钴蓝颜料.采用XRD,TG-DTA,UV-Vis,SEM和EDS等测试技术对粉体的形成、形貌、粒径及吸光度等进行表征.结果表明,获得的产物是明显的尖晶石晶体结构,粒度均匀、颜色鲜亮,粒径约为67 nm,较传统的钴蓝颜料成本低,具有更好的应用前景.
参考文献
| [1] | 向勇,谢道华.尖晶石结构功能材料的新进展[J].磁性材料及器件,2001(03):21-25,46. |
| [2] | Chemlal S;Larbotetc A .Materials research bulletin[J].Journal of the European Ceramic Society,2000,35(02):2515-2523. |
| [3] | 杨宗志.钴蓝颜料及其进展[J].涂料工业,1997(04):35-40. |
| [4] | 朱骥良;吴申年.颜料工艺学[M].北京:化学工业出版社,2002:293-296. |
| [5] | 钱逸泰.结晶化学[M].合肥:中国科学技术大学出版社,1987:314-328. |
| [6] | 高向阳.新编仪器分析[M].北京:科学出版社,2004:12-18. |
| [7] | 吴瑶,郭英.钴蓝的制备及改性研究[J].天津科技大学学报,2007(03):44-47. |
| [8] | 李仲谨,魏红,崔胜利.超细CoAl2O4多晶材料的制备与性能研究[J].西北轻工业学院学报,2000(04):27-29. |
| [9] | 闫国杰,程继健,张金朝,春胜利.CoxR1-xAl2O4（R=Zn,Mg）钴蓝颜料反射性能的研究[J].无机材料学报,2000(04):660-664. |
| [10] | 韩云芳,李向堂.均匀沉淀法制备钴蓝颜料的研究[J].天津城市建设学院学报,2002(02):92-95. |
| [11] | 周永强,于方丽,罗宏杰,刘海涛.溶胶-凝胶法制备纳米钴蓝颜料[J].硅酸盐通报,2006(05):31-33. |
| [12] | 杨水彬,刘孝恒,杨绪杰,汪信.纳米铝酸钴的合成与表征[J].河北师范大学学报(自然科学版),2007(01):85-86,98. |
| [13] | Zayat M.;Levy D. .Blue CoAl2O4 particles prepared by the sol-gel and citrate-gel methods[J].Chemistry of Materials,2000(9):2763-2769. |
| [14] | 罗红玉,田熙科,杨超,皮振邦.尖晶石型CoAl2O4纳米粉体的合成及表征[J].地球科学-中国地质大学学报,2005(02):191-194. |
| [15] | Chemlal S.;Persin M.;Sarrazin J.;Sghyar M.;Rafiq M.;Larbot A. .Cobalt spinel CoAl2O4 via sol-gel process: elaboration and surface properties[J].Materials Research Bulletin: An International Journal Reporting Research on Crystal Growth and Materials Preparation and Characterization,2000(14/15):2515-2523. |
| [16] | 曹丽云,邓飞,张新河,朱振峰,黄剑锋.微乳液法制备CoAl2O4天蓝纳米陶瓷颜料[J].玻璃与搪瓷,2005(05):41-44. |
| [17] | Chen Jing;Shi Xiaobo Hanbing .The preparation and characteristics of cobalt blue colored mica titania pearlescent pigment by microemulsions[J].Dyes and Pigments,2007(3):766-769. |
| [18] | Cho W S;Kakihana M .Crystallization of pigment CoAl2O4 nanocrystals from Co-Al metal organic precursor[J].Journal of Alloys and Compounds,1999,287(1/2):87-90. |
| [19] | Chen Zhizhan;Shi Erwei;Li Ywenjun et al.Hydrothermal synthesis and optical property of nanosizod COAl2O4 pigment[J].Materials Letters,2002,55(05):281-289. |
| [20] | Carta G;Casarin M;Habra N E .MOCVD deposition of CoAl2O4 films[J].Electrochimica Acta,2005,50(03):4592-4599. |
| [21] | Weast R C.Handbook of chenistry and physics[M].Boca,Florida,USA:CRCA Pr,INC,1990 |
| [22] | Li Weidong;Li Jiazhi;Guo Jingkun .Synthesis and characterization of nanocrystalline CoAl2O4 spinel powder by low temperature combustion[J].Journal of the European Ceramic Society,2003,23(13):2289-2295. |
| [23] | 苏言杰,张德,徐建梅,王辉.柠檬酸盐凝胶自燃烧法合成超细粉体[J].材料导报,2006(z1):142-144. |
| [24] | Visinescu D;Paraschiv C;Ianculescu A et al.The environmentally benign synthesis of nanosized CoxZn1-Al2O4 blue pigments[J].Dyes and Pigments,2010,87(02):125-131. |
| [25] | Stangar U L;Orel B;Krajnc M .Preparation and spectroscopic characterization of blue CoAl2O4 coatings[J].Journal of Sol-Gel Science and Technology,2003,26:771-775. |
| [26] | Zayat M.;Levy D. .Blue CoAl2O4 particles prepared by the sol-gel and citrate-gel methods[J].Chemistry of Materials,2000(9):2763-2769. |
| [27] | 闫国杰,张金朝,春胜利,程继健.复合型钴蓝颜料的研究[J].硅酸盐通报,2000(03):17-20. |
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