Effect of Preparation Atmosphere on the Structure and Properties of Vanadium Pentoxide Xerogel Films

材料科学技术（英）, 2004, 20(3): 365-367.

^1, , ^2, , ^3, , ^4, , ^5, , ^6,

1.School of Materials Science and Engineering, Wuhan University of Technology, Wuhan,430070, China

2.School of Materials Science and Engineering, Wuhan University of Technology, Wuhan,430070, China

3.School of Materials Science and Engineering, Wuhan University of Technology, Wuhan,430070, China

4.School of Materials Science and Engineering, Wuhan University of Technology, Wuhan,430070, China

5.School of Materials Science and Engineering, Wuhan University of Technology, Wuhan,430070, China

6.School of Materials Science and Engineering, Wuhan University of Technology, Wuhan,430070, China

基金项目: 国家自然科学基金(50172036) 教育部高校优秀青年教师资助计划

Effect of Preparation Atmosphere on the Structure and Properties of Vanadium Pentoxide Xerogel Films

Keywords： Preparation atmosphere

In this article, the vanadium pentoxide sols are synthesized by two different routes (melted and quenched in oxygen atmosphere or in air). The structure and properties of the vanadium pentoxide xerogel films are characterized by XRD, ESR, cyclic voltammograms curves and UV-visible transmittance analysis. The results show that the sample prepared in oxygen has poorer crystallization, lower content of V4+ ions and higher Li+ insertion capacity compared with that prepared in air.

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Effect of Preparation Atmosphere on the Structure and Properties of Vanadium Pentoxide Xerogel Films

参考文献