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孔径及其分布决定了多孔陶瓷的性能及应用,因此对其测定和定量表征非常重要.本文综述了多孔陶瓷孔径及孔径分布的常见测定方法,包括气泡法、压汞法、气体透过法、气体吸附法、气体渗透法、液-液法、悬浮液过滤法、X射线小角度散射法、核磁共振成像法、X射线断层扫描法以及电子显微镜图像分析法.比较了各种测试方法的优缺点,认为电子显微镜图像分析法是最直接有效的测定方法,并对多孔陶瓷的测试表征方法提出了展望.

参考文献

[1] 贺辛亥,王俊勃,苏晓磊,秦辉,杨敏鸽,申明乾.生物形态多孔陶瓷的研究进展[J].硅酸盐通报,2011(01):105-110.
[2] 商景利,戴斌煜,王薇薇.有机泡沫浸渍法制备ZrO2泡沫陶瓷烧结过程研究[J].硅酸盐通报,2011(01):153-157.
[3] Jian Yu;Xiaojuan Hu;Yan Huang .A modification of the bubble-point method to determine the pore-mouth size distribution of porous materials[J].Separation and Purification Technology,2010(3):314-319.
[4] GB/T 1967-1996.GB/T 1967-1996,多孔陶瓷孔道直径试验方法[S].
[5] Elsa Vennat;Christine Bogicevic;Jean-Marie Fleureau;Michel Degrange .Demineralized dentin 3D porosity and pore size distribution using mercury porosimetry[J].Dental materials,2009(6):729-735.
[6] Hyunjung Kim;Yoseop Han;Jaikoo Park .Evaluation of permeable pore sizes of macroporous materials using a modified gas permeation method[J].Materials Characterization,2009(1):14-20.
[7] Miyata T.;Endo A.;Ohmori T.;Akiya T.;Nakaiwa M. .Evaluation of pore size distribution in boundary region of micropore and mesopore using gas adsorption method[J].Journal of Colloid and Interface Science,2003(1):116-125.
[8] A. DEMIR;N. ALTINKOK .Effect of gas pressure infiltration on microstructure and bending strength of porous Al_2O_3/SiC-reinforced aluminium matrix composites[J].Composites science and technology,2004(13/14):2067-2074.
[9] Calvo JI;Bottino A;Capannelli G;Hernandez A .Pore size distribution of ceramic UF membranes by liquid-liquid displacement porosimetry[J].Journal of Membrane Science,2008(1/2):531-538.
[10] Kesting R E.Synthetic polymeric membranes[M].M?graw-Hill,1971:29-40.
[11] Matsushima K;Hirata Y;Matsunaga N et al.Pressure filtration of alumina suspensions under alternating current field[J].Colloids and Surfaces A:Physicochemical and Engineering Aspects,2010,364:138-144.
[12] Gilles Renaud;Remi Lazzari;Frederic Leroy .Probing surface and interface morphology with Grazing Incidence Small Angle X-Ray Scattering[J].Surface Science Reports,2009(8):255-380.
[13] James J;Howard;William E K .Determination of pore size distribution in sedimentary rocks by proton nuclear magnetic resonance[J].Marine and Petroleum Geology,1992,9(02):139-145.
[14] Eric Maire;Paolo Colombo;Jerome Adrien .Characterization of the morphology of cellular ceramics by 3D image processing of X-ray tomography[J].Journal of the European Ceramic Society,2007(1):1973-1981.
[15] 章萍,黄勇理.基于显微观测及图像处理的颗粒检测综述[J].现代测量与实验室管理,2004(02):3-6,11.
[16] 夏凤金,吴晓玲,刘培生.多孔材料孔径及孔径分布的测定方法[J].中国组织工程研究与临床康复,2008(41):8183-8188.
[17] 汤国华,杨俊和,张琢,郑金标.一种定量分析多孔材料孔隙结构的新方法[J].煤炭转化,2004(01):71-75.
[18] 张代林.利用图像分析法测定焦炭气孔结构的研究[J].燃料与化工,2003(04):175-178.
[19] Zhengmin Li;Shuping Zhuo;Hongtao Li;Weijiang Si;Yi Ding .Determination of Ligament Size Distribution of Nanoporous Gold by Scanning Electron Microscopy and Image Analysis[J].Journal of nanoscience and nanotechnology,2009(2):1651-1654.
[20] Ziel R;Haus A;Tulke A .Quantification of the pore size distribution(porosity profiles) in microfiltration membranes by SEM,TEM and computer image analysis[J].Journal of Membrane Science,2008,323(02):241-246.
[21] F. H. She;K. L. Tung;L. X. Kong .Calculation of effective pore diameters in porous filtration membranes with image analysis[J].Robotics and Computer Integrated Manufacturing,2008(3):427-434.
[22] Calvo JI.;Caruana G.;Martinez L.;Hernandez A. .PORE SIZE DISTRIBUTIONS IN MICROPOROUS MEMBRANES .1. SURFACE STUDY OF TRACK-ETCHED FILTERS BY IMAGE ANALYSIS[J].Journal of Colloid and Interface Science,1995(1):138-150.
[23] Sunkyu Park;Richard A.Venditti;Hasan Jameel .Changes in pore size distribution during the drying of cellulose fibers as measured by differential scanning calorimetry[J].Carbohydrate Polymers: Scientific and Technological Aspects of Industrially Important Polysaccharides,2006(1):97-103.
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