采用磁控溅射法制备了可钢化TiO2-Si3 N4-CrNx-Ag-NiCrOx-ZnO-Si3 N4复合玻璃涂层(TSCANZSLow-E玻璃),并对其微观结构和物理性能进行了测试.AFM分析发现,薄膜表面光滑平整,粗糙度Ra为0.323nm;XPS探测到膜层表面存在TiO2和Si3N4;四探针面电阻测试仪测定薄膜方阻Rs为8.81Ω/□,比辐射率值为0.108;光学性能分析显示可见光透过率达81%,在2500nm处的中远红外区反射率达80%;剥落实验证明薄膜与玻璃基底之间具有良好的附着性;钢化测试结果符合国标要求.
参考文献
| [1] | 刘起英,汪建勋,陈华,刘军波,孔繁华,应益明.低辐射镀膜玻璃的现状及展望[J].玻璃,2002(06):9-13. |
| [2] | 周家斌,任毅,付志强,王成彪.低辐射镀膜玻璃的研究开发进展[J].建筑结构学报,2007(04):104-108. |
| [3] | Gunther Beister;Eckhard Dietrich;Christian Schaefer et al.Progress in large-area glass coating by high-rate sputtering[J].Surface and Coatings Technology,1995,76-77:776. |
| [4] | Shaecefer C;Brauer G;Szcybowski J .Low emissivity coatings on architectural glass[J].Surface and Coatings Technology,1997,93:37. |
| [5] | Szczyrbowski J;Braeuer G;Ruske M et al.Temperable low emissivity coating based on twin magnetron sputtered TiO2 and Si3 N4 layers[J].Thin Solid Films,1999,351:141. |
| [6] | Gillery F H;Criss R C et al.Protective overcoat for low emissicity coated article[P].US,4716086,1987-09-29. |
| [7] | Navinsek B;Panjan P .Oxidation of CrNx hard coatings reactively sputtered at low temperature[J].Thin Solid Films,1993,223:4. |
| [8] | GB/T 2680-1994.GB/T 2680-1994.建筑玻璃可见光透过比,太阳光直接透射比、太阳能总透射比、紫外线透射比及有关窗玻璃参数的测定[S].北京:中国标准出版社,1993. |
| [9] | ISO 10292-1994.ISO 10292-1994.Glass in building-Calculation of steady-state U values(thermal transmittance) of multiple glazing[S].Wwitzerland:The International Organization for Standardization,1994. |
| [10] | 田秋波;刘德霖.薄膜科学与技术手册[M].北京:机械工业出版社,1991 |
| [11] | GB/T18915.2-2002.GB/T18915.2-2002.镀膜玻璃第2部分:低辐射镀膜玻璃[S].北京:中国标准出版社,2002. |
| [12] | 孙喜莲,邵建达.铬过渡层对银膜光学性质及附着力的影响[J].中国激光,2006(12):1680-1683. |
| [13] | 谢致薇,蒙继龙,王国庆.物理气相沉积薄膜的界面与附着力[J].真空科学与技术学报,2001(03):203-209,213. |
| [14] | 谢致薇,蒙继龙,王国庆.物理气相沉积薄膜的界面与附着力[J].真空科学与技术学报,2001(03):203-209,213. |
| [15] | GB15763.2-2005.GB15763.2-2005.钢化玻璃国家标准[S].北京:中国标准出版社,2006. |
| [16] | 中弘;Hiroshi Nakashima .Mechanism of radiation energy control by films coated on sheet glass[J].New Glass,1992,7(03):227. |
| [17] | 大规东洋;近江伸;江涛 .节能型低辐射率玻璃[J].红外,1999,9(09):9. |
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