欢迎登录材料期刊网

材料期刊网

高级检索

电解质等离子抛光过程中受抛光产生的金属微粒的干扰,无法使用电导法对抛光液中硫酸铵的含量进行检测,为了解决这一问题,基于实验提出了两种确定硫酸铵含量(质量分数)的方法.一种方法是利用抛光液中硫酸铵的含量低于2.5%以后抛光的电流密度会明显下降的现象,定时检测抛光过程中电流值和抛光液温度,以确定是否需要补充硫酸铵.另一种方法是通过实验得到一定抛光液温度下抛光量与硫酸铵消耗量的关系,再在抛光过程中记录抛光量计算抛光液中硫酸铵含量的方法.研究发现,前一种方法应用更为简便,适用于一般工业生产;后一种方法适用于对抛光效果要求更高的加工.经实验验证两种方法均具有可行性.

Conductometry is not available in detecting the mass fraction of ammonium sulfate in polishing solution in electrolysis and plasma polishing because of the interference of the metallic particles produced in the polishing. To solve the problem, two methods based on experiment to detect the mass fraction of ammonium sulfate are proposed. One method is to measure the current and temperature of the polishing solution to determine whether ammonium sulfate need to be added, as the electric current density drops significantly when the mass fraction is less than 2.5%. The other method is to know correlations between the polishing quantity and the consumption of ammonium sulfate at a certain temperature of the polishing solution by experiments, then the polishing quantity is recorded to work out the mass fraction of ammonium sulfate. The first method is simple to operate, and thus is suitable for general industrial production. The second method applies to the process requiring better polishing effects. The two methods are proved to be effective and feasible.

参考文献

[1] 翁慧燕,李振华.抛光的几种工艺对比[J].机械工程师,2010(06):28-29.
[2] 马云,刘存海,王锦江,田小博.我国抛光处理材料的研发现状[J].新技术新工艺,2003(12):48-50.
[3] 徐文骥,宋金龙,刘新,孙晶,陆遥.大面积超疏水铝表面的电化学加工[J].材料科学与工艺,2012(02):52-60.
[4] 赵兴科,王中,郑玉峰,赵连城.抛光技术的现状[J].表面技术,2000(02):6-7.
[5] 朱荻.国外电解加工的研究进展[J].电加工与模具,2000(01):11-16.
[6] 宋小平.溶液电导率的绝对测量方法[J].化学分析计量,2004(06):88-89.
[7] 郑玉婴,王攀,张通,李宝铭.聚3-戊酰基吡咯/多壁碳纳米管复合材料的制备与电导率研究[J].材料科学与工艺,2012(05):111-115.
[8] 齐德江,杨晓红,马子宁,毕孝国,茹红强.(PEO)_(16)LiClO_4-NaY电解质薄膜的显微组织特征与离子导电性能[J].材料科学与工艺,2011(05):12-16.
[9] WANG Ji;SUO Laichun;GUAN Lili et al.Analytical study on mechanism of electrolysis and plasma polishing[J].Advanced Materials Research,2012,472-475:350-353.
[10] MARIC D;SASIC O;JOVANOVIC J .Ionization coeffi-cients in gas mixtures[J].Radiation Physics and Chemistry,2006,76:551-555.
[11] Meletis EI.;Nie X.;Wang FL.;Jiang JC. .Electrolytic plasma processing for cleaning and metal-coating of steel surfaces[J].Surface & Coatings Technology,2002(2/3):246-256.
[12] 李福刚,王永臣,夏吾勇.碱溶液浓度的自动检测[J].沈阳化工学院学报,1997(01):18.
[13] WANG Ji;SUO Laichun;GUAN Lili et al.Optimiza-tion of processing parameters for electrolysis and plas-ma polishing[J].Applied Mechanics and Materials,2012,217-219:1368-1371.
[14] 李军军,张建涛.回归模型可决系数的可决性研究[J].统计与决策,2005(11):19-20.
[15] 叶卫平;方安平;于本方.Origin7.0科技绘图及数据分析[M].北京:机械工业出版社,2003:146-153.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%