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微波固化相对于传统热固化有着固化效率高、无污染、设备投资小等优势.针对双酚A型环氧树脂聚酰胺固化体系,采用DSC测固化度表征微波固化行为,优化体系成份配比,设计正交试验表考察微波固化工艺参数对固化行为的影响,并对两种不同固化方式产物的玻璃化转变温度进行比较.结果表明:微波固化体系最优配比为环氧E51∶650聚酰胺∶660A活性稀释剂=100∶80∶12;影响该体系固化效率的微波固化工艺参数主次顺序依次为加热时间、输出功率、加热周期、间歇时间;该体系微波固化产物的玻璃化转变温度及弯曲性能较热固化产物有一定程度的降低,分析得出微波场的不均匀性是这一现象产生的重要影响因素.

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