采用柠檬酸络合法制备8YSZ粉体，通过测试发现该粉体常温至600℃的发射率呈现不断降低的规律。对所制备的8YSZ粉体进行高温热处理，结果表明，1400℃处理2 h的粉体发射率最低，在600℃下可降至0.288，可以选作为红外隐身涂层的颜料。通过EDS、XRD、SEM等表征手段，探讨分析了热处理影响8YSZ粉体发射率的机理。
8YSZ powder was prepared by the method of citric acid complexation. It is found that the emissivity of the powder de-creases continuously from room temperature to 600℃. The 8YSZ powder was treated at high temperature. The results show that the powder emissivity reduces to the lowest when heating at 1 400℃for 2 h,and can be reduced to 0.288 at 600℃,which can be chosen as pigment for infrared stealth coating. The effect mechanism of heat treatment on powder emissivity was analysed by EDS,XRD and SEM.
参考文献
| [1] | Zueco, J;Alhama, F .Inverse estimation of temperature dependent emissivity of solid metals[J].Journal of Quantitative Spectroscopy & Radiative Transfer,2006(1):73-86. |
| [2] | 胡传炘.隐身涂层技术[M].北京:化学工业出版社,2004:121. |
| [3] | 吕俊伟,李海燕,朱敏,王永.飞机的红外隐身技术[J].现代防御技术,2006(04):92-95,102. |
| [4] | 曹义,程海峰,郑文伟,才鸿年,成绍军.基于红外热像仪的涂层波段发射率测量[J].红外技术,2007(06):316-319. |
| [5] | 王庭慰,程从亮,张其土.8～14μm波长低红外发射率涂料的研究[J].光学技术,2005(04):598-600. |
| [6] | 张宏元,郭俊杰.红外隐身材料的性能特征述评[J].化工新型材料,2003(01):30-33. |
| [7] | 蒋勇,徐国跃,郭腾超,李泉灵,秦锐.热处理对氧化铈粉体3～5μm波段红外发射率的影响[J].红外技术,2011(12):699-703. |
| [8] | Chevalier S.;Kilo M.;Borchardt G.;Larpin JP. .MOCVD deposition of YSZ on stainless steels[J].Applied Surface Science: A Journal Devoted to the Properties of Interfaces in Relation to the Synthesis and Behaviour of Materials,2003(1/4):188-195. |
| [9] | Aaberg RJ.;Odegard R.;Tunold R. .On the electrochemistry of metal-YSZ single contact electrodes[J].Solid state ionics,2000(Special Issue SI):707-712. |
| [10] | 王德,贺强,裴力,贺天民.甘氨酸-硝酸盐法合成纳米YSZ微粉及其性能[J].吉林大学学报(理学版),2004(02):261-264. |
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