欢迎登录材料期刊网

材料期刊网

高级检索

以W粉和Ti粉为原料,采用真空热压烧结工艺制备了W-10%Ti合金,研究了烧结温度对W-Ti合金的相组成、微观形貌和硬度的影响。结果表明,合金主要由富W固溶体、富Ti固溶体和心部未发生扩散的α-Ti相组成。随烧结温度的升高,W与Ti的相互固溶度增大,α-Ti相的残余量减少,1400℃烧结的W-Ti合金中部分富Ti固溶体发生了共析转变。合金的致密度和维氏硬度均随烧结温度的升高先增大后减小,在1300℃时有最大值,分别达99.4%和6.3 GPa。

W-10%Ti alloy was fabricated by vacuum hot-pressing using W and Ti mixed powders as raw materials.The effect of sintering temperature on phase composition,microstructure and hardness of the alloy was studied.The W-Ti alloy sintered at different temperatures consist of W-rich solid solution phase,Ti-rich solid solution phase and remained α-Ti phase.With increasing the sintering temperature,the solid solubility between W and Ti increases and remained α-Ti phase decreases.A eutectoid phase transformation takes place in Ti-rich solid solution phase with higher amount of W,when the alloy is hot pressed at 1400 ℃.Both the relative density and the Vickers hardness of the alloy increase firstly,and then decrease with increasing sintering temperature,reaching the maximum value of 99.4% and 6.3 GPa at 1300 ℃,respectively.

参考文献

[1] Petrovic S;Bundaleski N;Perusko D;Radovic M;Kovac J;Mitric M;Gakovic B;Rakocevic Z .Surface analysis of the nanostructured W-Ti thin film deposited on silicon[J].Applied Surface Science: A Journal Devoted to the Properties of Interfaces in Relation to the Synthesis and Behaviour of Materials,2007(12):5196-5202.
[2] 张青来,贺继弘.溅射靶材综述[J].上海钢研,2002(04):30-41.
[3] Wickersham C E;Poole Jr J E;Mueller J J .Particle contamination during sputter deposition of W-Ti films[J].Journal of Vacuum Science and Technology A:Vacuum Surfaces and Films,1992,10(04):1713-1717.
[4] 王庆相,接显卓,梁淑华,范志康.机械合金化W-Ti粉末的烧结特性[J].材料热处理学报,2010(01):67-73.
[5] 王庆相,杨怡,范志康.烧结熔渗过程中W和Ti扩散溶解的研究[J].稀有金属材料与工程,2009(07):1193-1197.
[6] 王赞海,王星明,储茂友,郭奋,赵鑫,沈剑韵.惰性气体热压法制备W/Ti合金靶材研究[J].稀有金属,2006(05):688-691.
[7] Kecskes J L;Hall I W .Microstructural effects in hot-explosively-consolidated W-Ti alloys[J].Journal of Materials Processing Technology,1994,94:247-260.
[8] 陶杰;姚正军;薛烽.材料科学基础[M].北京:化学工业出版社,2006:150-153.
[9] Massalski T B;Okamoto H;Subramanian P R.Binary Alloy Phase Diagrams[M].Scott W W.New York,1990
[10] Chi-Fung Lo;Paul Gilman .Particle generation in W-Ti deposition[J].Journal of Vacuum Science & Technology, A. Vacuum, Surfaces, and Films,1999(2):608-610.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%