{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"建立了以甲苯-甲基异丁基酮为萃取剂、罗丹明B为显色剂分光光度法测定黄磷电尘灰冶炼物料中镓的方法.试样采用体积分数10%硫酸溶解后,加入三氯化钛还原铁至二价,在6mol/L盐酸中用甲苯-甲基异丁基酮萃取罗丹明B与镓生成络合物,有机相经硫脲、三氯化钛和罗丹明B溶液洗涤后,在最大吸收波长560 nm测定吸光度,同时采用校正法消除样品分解带来的方法系统误差.镓的质量浓度在0~1.0 μg/mL时,吸光度与浓度呈线性关系,相关系数为0.999.将实验方法与传统溶样方法的测定值进行对照,结果一致.对6个黄磷电尘灰冶炼物料样品中镓进行测定,结果的相对标准偏差小于10%,加标回收率在96%~103%之间.","authors":[{"authorName":"龙萍","id":"2dbc769d-659c-427b-8137-a90d27ee5206","originalAuthorName":"龙萍"},{"authorName":"吴鉴","id":"ae75428d-85f7-4e4a-a218-a41a76c1b697","originalAuthorName":"吴鉴"},{"authorName":"谢克强","id":"b4e84ad6-d8a3-4a53-b505-407bad22549f","originalAuthorName":"谢克强"},{"authorName":"毛禹平","id":"29704b98-6220-4ef3-b35b-f6a187822106","originalAuthorName":"毛禹平"}],"doi":"","fpage":"64","id":"d48b6dc4-4e11-407a-aae6-68c4a6813e54","issue":"8","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"49a92a2d-db11-49cc-a263-aefb6542a0ea","keyword":"黄磷电尘灰","originalKeyword":"黄磷电尘灰"},{"id":"90a95c84-4661-408d-974e-020f5559a2be","keyword":"冶炼物料","originalKeyword":"冶炼物料"},{"id":"0e5ec71a-7f06-4925-942c-62bd7dddb0e0","keyword":"镓","originalKeyword":"镓"},{"id":"74dcd736-52df-4121-a7b4-468dbad3c28f","keyword":"分光光度法","originalKeyword":"分光光度法"}],"language":"zh","publisherId":"yjfx201308014","title":"罗丹明B萃取分光光度法测定黄磷电尘灰冶炼物料中镓","volume":"33","year":"2013"},{"abstractinfo":"采用特殊的含有铁粉的物料(F料)冶炼高牌号纯铁,用F料配加废钢可在普通电弧炉上冶炼出YT4和超低磷、硫纯铁,讨论了其热力学条件,在建立了冶炼过程的微观动力学和宏观动力学的图示模型基础上,研究了其脱碳、脱磷过程的动力学.","authors":[{"authorName":"方民宪","id":"4973a203-47d9-4e4b-9a10-6993f732e5fc","originalAuthorName":"方民宪"},{"authorName":"陈建钢","id":"a5c397d4-f53a-445f-a260-822140463a53","originalAuthorName":"陈建钢"},{"authorName":"冯庆芬","id":"c27f492d-370e-4b52-93e3-0252f1071b1c","originalAuthorName":"冯庆芬"},{"authorName":"刘蓉生","id":"419680a5-4b8d-482b-8b26-f5ea4a85e2bf","originalAuthorName":"刘蓉生"},{"authorName":"丁华东","id":"5e88d8be-111d-48ee-ae0c-0d35f68ec56b","originalAuthorName":"丁华东"}],"doi":"10.3969/j.issn.1004-244X.2002.05.010","fpage":"40","id":"4ce0df12-85a6-4f7d-9e27-07b61aeeb3fd","issue":"5","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程 "},"keywords":[{"id":"44df803a-2980-4d5f-81c1-c14e5d2ba98c","keyword":"冶炼","originalKeyword":"冶炼"},{"id":"1de5ca35-f042-4619-b738-591f6be4c713","keyword":"脱碳","originalKeyword":"脱碳"},{"id":"9e888f1b-bc05-4469-89ff-00cac4ec36bc","keyword":"脱磷","originalKeyword":"脱磷"},{"id":"d4ee0be0-94ef-40e8-b3c7-322e25e2753c","keyword":"热力学","originalKeyword":"热力学"},{"id":"51cd81d2-568b-40f9-919e-b4d7d060d801","keyword":"动力学","originalKeyword":"动力学"}],"language":"zh","publisherId":"bqclkxygc200205010","title":"铁粉物料混合废钢冶炼纯铁的脱碳、脱磷研究","volume":"25","year":"2002"},{"abstractinfo":"将等离子体光谱法和X荧光光谱法应用于贵金属湿法冶炼物料中金的测定.通过对多种不同组成物料的测定及与经典火试金法进行的大量对照试验,拟定了测定金的新方法.光谱法具有测定快速、线性范围宽、准确度好、精密度高等优点,完全能满足生产控制及科研的需要.","authors":[{"authorName":"傅俊卫","id":"ef8a0fc0-2e80-4bc9-b0e6-8521c7d73135","originalAuthorName":"傅俊卫"},{"authorName":"夏珍珠","id":"0144e130-5550-40e2-bb18-e2d54d10aedb","originalAuthorName":"夏珍珠"}],"doi":"10.3969/j.issn.1000-7571.2003.03.017","fpage":"48","id":"08cb4a7b-a4d6-4171-b136-2cb16b4fc37c","issue":"3","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"9d1a481b-4add-42a9-98aa-4a820a0d9c6c","keyword":"湿法冶炼","originalKeyword":"湿法冶炼"},{"id":"7c170beb-efd1-4f11-aeb8-0b93506a8b22","keyword":"金","originalKeyword":"金"},{"id":"33f24545-73fa-4b51-919e-ec19a7ed27f0","keyword":"火试金","originalKeyword":"火试金"},{"id":"3520cf1f-94a9-4585-9777-a2fa704bfb44","keyword":"ICP-AES","originalKeyword":"ICP-AES"},{"id":"46d5c274-5eb3-44dd-9e87-b0197780f84b","keyword":"半定量分析","originalKeyword":"半定量分析"}],"language":"zh","publisherId":"yjfx200303017","title":"光谱法测定贵金属湿法冶炼物料中的金","volume":"23","year":"2003"},{"abstractinfo":"红土镍矿焙砂、烟尘及电炉渣等镍铁冶炼过程物料经氧化预处理后熔融制样,采用铁矿石、转炉渣标准样品与自制的红土镍矿标样组合建立X射线荧光光谱(XRF)分析校准曲线,实现了镍铁冶炼过程物料中Ni、Fe、SiO2、MgO、CaO、P2O5、Al2O3、Cr2O3、MnO、Co等10种组分的快速准确测定.试验发现,样品粒度为200目(74 μm),900℃温度下空气氧化45min后,各还原性组分的质量分数均较低,在此氧化条件下经氧化灼烧的红土镍矿焙砂、烟尘及电炉渣样品中金属单质及残碳质量分数均可降至0.1%以下,达到了使用铂黄合金坩埚对样品制备熔融片的要求.选择偏硼酸锂和四硼酸锂混合熔剂、稀释比为10、在1 050℃熔融15 min,熔融效果较好.采用理论α系数进行基体校正,各测定组分校准曲线的线性相关系数达到0.999以上.采用红土镍矿及其焙砂、烟尘和电炉渣样品进行分析,精密度实验结果表明,各组分测定值的相对标准偏差(RSD,n=9)小于5%.测定结果根据灼烧减量校正计算后得出样品中各组分含量,结果与化学法测定值基本一致.","authors":[{"authorName":"施善林","id":"f52fea2f-b840-4071-9f88-016c84e7698c","originalAuthorName":"施善林"},{"authorName":"郭阳","id":"22d1ee94-818d-4fa1-8acd-ddd12763fc11","originalAuthorName":"郭阳"},{"authorName":"李东麟","id":"7b93b756-742e-4155-ad53-9c218f6a7877","originalAuthorName":"李东麟"},{"authorName":"王永海","id":"b7cb902e-af4c-4261-bd35-7f2d9f742e4a","originalAuthorName":"王永海"}],"doi":"10.13228/j.b0yuan.issn1000-7571.009540","fpage":"54","id":"f9d7e5c6-4f3a-495f-91d4-b7425f07e278","issue":"7","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"3d59dd30-e691-4012-ba1d-989d3026c465","keyword":"红土镍矿","originalKeyword":"红土镍矿"},{"id":"afd32da2-6223-45f0-bf4e-7c3a838eb238","keyword":"焙砂","originalKeyword":"焙砂"},{"id":"35f2d068-169d-4b0f-a99a-c772680b670a","keyword":"镍铁冶炼过程物料","originalKeyword":"镍铁冶炼过程物料"},{"id":"2df6bceb-57c6-4354-9f07-db283713b2f3","keyword":"氧化灼烧","originalKeyword":"氧化灼烧"},{"id":"dd386069-a2dc-4fca-bcf0-54e7a07f41c8","keyword":"熔融制样","originalKeyword":"熔融制样"},{"id":"3e233de9-3a9e-4a56-bf73-6fe366e43125","keyword":"X射线荧光光谱法","originalKeyword":"X射线荧光光谱法"}],"language":"zh","publisherId":"yjfx201507010","title":"熔融制样-X射线荧光光谱法测定镍铁冶炼过程物料中10种组分","volume":"35","year":"2015"},{"abstractinfo":"介绍宝钢1550热镀锌机组焊缝跟踪和物料跟踪控制系统的配置和功能,以及系统应用软件的功能和现场使用情况.","authors":[{"authorName":"祃丽婷","id":"03e2dce2-cff4-407d-96ee-2660d3c3740e","originalAuthorName":"祃丽婷"}],"doi":"10.3969/j.issn.1001-7208.2004.06.007","fpage":"29","id":"4c9e66ad-82bd-4595-9cdd-00eafc85c9bc","issue":"6","journal":{"abbrevTitle":"SHJS","coverImgSrc":"journal/img/cover/SHJS.jpg","id":"59","issnPpub":"1001-7208","publisherId":"SHJS","title":"上海金属"},"keywords":[{"id":"66cc4863-7c24-43f7-ab75-385a1898043f","keyword":"焊缝跟踪","originalKeyword":"焊缝跟踪"},{"id":"b32b26cb-fa8b-43f0-86fe-0d78615993ea","keyword":"物料跟踪","originalKeyword":"物料跟踪"},{"id":"ab649312-2076-450f-b702-9b8a1d1ad1a2","keyword":"人机接口","originalKeyword":"人机接口"},{"id":"0fbcf516-f30a-4c36-8689-2fdddef7f19b","keyword":"焊缝同步检测装置","originalKeyword":"焊缝同步检测装置"}],"language":"zh","publisherId":"shjs200406007","title":"焊缝跟踪和物料跟踪","volume":"26","year":"2004"},{"abstractinfo":"基于已完成的进口含锌物料固体废物鉴别实践,系统地介绍了所遇到的进口含锌物料的申报品名、每种品名所占的比例、种类以及每种种类的特征、固体废物鉴别的关键方法和每种鉴别结果所占的比例,其中申报品名中锌精矿或锌矿砂所占比例为55.2%,而鉴别结果中锌精矿仅占3.4%。重点介绍了锌精矿、副产品氧化锌、电弧炼钢烟尘、冶炼渣、固体废物简单处理产物等含锌物料的鉴别方法:首先进行外观观察和必要的试验分析,包括肉眼观察物料的外观特征,利用烘箱测量含水率、X射线荧光光谱仪分析主要成分和含量、滴定法确认锌元素及典型重金属元素的准确含量,另外,利用X射线衍射仪及矿相显微镜确定物料的物相组成,对于粉末物料,还需利用激光粒度仪分析其粒度分布;其次,根据物料的外观特征和试验结果,通过资料对比、实地调研、专家咨询的方法,判断出物料的产生来源;最后,根据《固体废物鉴别导则》(试行)得出物料的固体废物鉴别结论。所进行的研究为进口含锌物料的固体废物鉴别和监管提供参考,对将含锌冶炼渣、含锌烟尘、含锌固体废物简单处理产物等固体废物堵在国门之外具有重要意义。","authors":[{"authorName":"郝雅琼","id":"c6dee800-9cd3-4512-adc4-dfe77f1c8471","originalAuthorName":"郝雅琼"}],"doi":"10.13228/j.boyuan.issn1000-7571.009864","fpage":"34","id":"af89c167-66ed-4c0b-a1d8-01bff660c8fa","issue":"10","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"058562a7-31a6-465b-a1fc-190ff02fa71e","keyword":"含锌物料","originalKeyword":"含锌物料"},{"id":"679e5d0c-e553-4b68-9971-8225fc8415bd","keyword":"固体废物","originalKeyword":"固体废物"},{"id":"8fbc13e2-3d56-4ae3-9daa-f94649d11420","keyword":"鉴别方法","originalKeyword":"鉴别方法"},{"id":"75b3b831-c76c-4fd4-b5d9-76ce7c912b6a","keyword":"锌精矿","originalKeyword":"锌精矿"},{"id":"b4f788f4-8a27-4a3b-b67b-a7d62d62734f","keyword":"副产品氧化锌","originalKeyword":"副产品氧化锌"},{"id":"91ec5953-1129-49b8-bc1d-345839858e1d","keyword":"电弧炼钢烟尘","originalKeyword":"电弧炼钢烟尘"},{"id":"07e9bb2e-82df-4db6-ab30-cf985cb9c7e8","keyword":"冶炼渣","originalKeyword":"冶炼渣"},{"id":"09a4e9b0-c889-4c73-b81b-fc4e8ed2f713","keyword":"固体废物简单处理产物","originalKeyword":"固体废物简单处理产物"}],"language":"zh","publisherId":"yjfx201610011","title":"进口含锌物料的固体废物鉴别方法","volume":"36","year":"2016"},{"abstractinfo":"通过对3个进口含铜物料的固体废物鉴别,得到了进口含铜物料的固体废物鉴别方法,即含铜物料的固体废物鉴别通常包括3步:第1步,确定物料的自然属性,包括利用肉眼进行外观和杂质观察;利用X射线荧光光谱(XRF )进行半定量分析,确认物料的主要成分及其质量分数;利用X射线衍射仪(X RD )和矿相显微镜进行物相组成分析,得到物料的主要物相组成;对于极细粉末类含铜物料,还需要利用扫描电子显微镜(SEM )分析物料的微观形态和粒度分布。第2步,确定物料的产生来源,具体是指根据物料的外观特征和试验结果,通过资料对比、实地调研、专家咨询的方法,判断出物料的产生工艺,最终明确该物料是否有意识生产等信息。第3步,确定物料的固体废物属性,即根据《固体废物鉴别导则》(试行)得出物料的固体废物鉴别结论。在此所鉴别的3个含铜物料固体废物鉴别结论分别是铜冶炼过程中产生的铜渣、含铜电镀污泥、废黄杂铜冶炼中渣/烟灰/二级泥渣的混合物料,均属于我国禁止进口的固体废物。实验研究为进口含铜物料的固体废物鉴别和监管提供参考,对将铜渣、铜电镀污泥、含铜渣/灰/泥混合物料等固体废物堵在国门之外具有重要意义。","authors":[{"authorName":"郝雅琼","id":"16e979fc-b087-44fe-b11c-8be03cb66d4b","originalAuthorName":"郝雅琼"}],"doi":"10.13228/j.boyuan.issn1000-7571.009936","fpage":"26","id":"51e3cf1e-1b23-41d3-8c9f-48b6b3166ad6","issue":"1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"eab1a688-e009-4113-843b-2716083ced6a","keyword":"铜渣","originalKeyword":"铜渣"},{"id":"81c04324-4678-47c5-91ce-b8ec0c76414a","keyword":"含铜电镀污泥","originalKeyword":"含铜电镀污泥"},{"id":"a9443170-af90-427c-aeed-1e759d655e96","keyword":"废黄杂铜冶炼中渣/烟灰/二级泥渣的混合物料","originalKeyword":"废黄杂铜冶炼中渣/烟灰/二级泥渣的混合物料"},{"id":"e519899d-0d5b-4ca9-b328-432f2c3b7b39","keyword":"固体废物","originalKeyword":"固体废物"},{"id":"0e8fa9d3-8d49-4177-a2e3-87356dcbd382","keyword":"鉴别方法","originalKeyword":"鉴别方法"},{"id":"5aaceca9-409d-47f0-9d51-e1821435b46a","keyword":"X射线荧光光谱","originalKeyword":"X射线荧光光谱"},{"id":"74e088b9-66b5-4860-90d2-2e9686612fb5","keyword":"X射线衍射仪","originalKeyword":"X射线衍射仪"},{"id":"cb28d0c3-5a21-42b5-86d6-fb1a6e03d62c","keyword":"矿相显微镜","originalKeyword":"矿相显微镜"},{"id":"1b834a49-a2a4-4302-813f-bf977cbe655e","keyword":"扫描电子显微镜","originalKeyword":"扫描电子显微镜"}],"language":"zh","publisherId":"yjfx201701006","title":"多种进口含铜物料的固体废物鉴别方法","volume":"37","year":"2017"},{"abstractinfo":"介绍了液体物料透明度的几种测量方法,供业内人士参考,目的是提高液体物料透明度测量的准确性、科学性.","authors":[{"authorName":"窦明","id":"1caf2984-ba4f-42d4-806f-3f44c6e2ec16","originalAuthorName":"窦明"}],"doi":"10.3969/j.issn.0253-4312.2002.09.016","fpage":"37","id":"53cb8dfa-7f39-4e62-a402-0654d7ef9fbd","issue":"9","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"d71d79ed-30b3-48e1-ae57-d179d37ffb55","keyword":"透明度","originalKeyword":"透明度"},{"id":"e0a198aa-507a-41c2-a3e4-e73f50fb728b","keyword":"液体","originalKeyword":"液体"},{"id":"352e3959-60fe-44d1-a36e-22e656ecad12","keyword":"测量方法","originalKeyword":"测量方法"}],"language":"zh","publisherId":"tlgy200209016","title":"液体物料透明度的测量","volume":"32","year":"2002"},{"abstractinfo":"介绍了几种高炉喷吹物料的作用及现状,指出凡是可以块状形式从炉顶加入的物料,均可以粉末形式从风口喷入炉内,作为高炉冶炼达到优质、高产、低耗、长寿的必要调剂手段;高炉喷吹应向以喷吹煤粉为主的复合喷吹方向发展,并与环境保护及二次资源利用结合起来.建议进一步开展对复合喷吹的研究开发工作,以及开展对高炉喷吹废弃可燃物(如废塑料、废轮胎)的有关研究开发工作.","authors":[{"authorName":"杨绍利","id":"766fee18-7c86-4bed-a9d2-35a2f2b1239b","originalAuthorName":"杨绍利"},{"authorName":"郭兴忠","id":"947a9fd4-48ac-4142-9c0a-4fcde82aa66d","originalAuthorName":"郭兴忠"},{"authorName":"徐楚韶","id":"e218cde0-2509-4de9-80ab-e1f4d14cce9e","originalAuthorName":"徐楚韶"},{"authorName":"张丙怀","id":"765b9e6e-8b46-4cfe-b4f7-486f733b1aa0","originalAuthorName":"张丙怀"}],"doi":"10.3969/j.issn.1004-7638.2000.02.008","fpage":"34","id":"71983972-b13a-4531-8f6c-05eebb3d6fab","issue":"2","journal":{"abbrevTitle":"GTFT","coverImgSrc":"journal/img/cover/gtft1.jpg","id":"28","issnPpub":"1004-7638","publisherId":"GTFT","title":"钢铁钒钛"},"keywords":[{"id":"8aabb477-1955-4303-ac9b-a597ee680153","keyword":"高炉","originalKeyword":"高炉"},{"id":"74f41706-90e4-43c5-b35e-a55c40b2b539","keyword":"喷吹","originalKeyword":"喷吹"},{"id":"3217fc44-8196-464c-b7c3-3ab8959a423e","keyword":"物料","originalKeyword":"物料"},{"id":"916c2b7d-019c-4549-8821-332d6827e0c4","keyword":"资源","originalKeyword":"资源"}],"language":"zh","publisherId":"gtft200002008","title":"高炉喷吹物料及其演变趋势","volume":"21","year":"2000"},{"abstractinfo":"以往的AOD炉高效化冶炼研究往往通过提高供氧强度,优化转炉的炉容比,提高终点命中率等技术缩短冶炼周期,需要充分利用现有的设备,优化炉料结构和供氧制度,对生产工艺参数进行优化,充分利用这些物理热和化学热,实现AOD炉的高效化冶炼。开发了AOD炉高效化冶炼模型,在AOD炉物料平衡和能量平衡的基础上,结合AOD炉冶炼的工艺特征,建立AOD炉耗氧量和冶炼周期模型,分析了AOD炉冶炼周期随着铁水比和废钢比的变化趋势,得出冶炼周期最短时的炉料结构。结果表明:电炉不锈钢母液加铁水冶炼时,冶炼周期随着铁水比的增加而增加。电炉不锈钢母液加废钢冶炼时,冶炼周期随着废钢比的增加而增加。铁水加废钢冶炼时,冶炼周期随着废钢比的增加而延长。以硅铁为发热剂比以碳粉为发热剂冶炼周期短。","authors":[{"authorName":"艾立翔","id":"19ac4c65-9487-4309-a010-0d4bc22ad034","originalAuthorName":"艾立翔"},{"authorName":"汪红兵","id":"dada04a2-2229-4448-a999-279236820be9","originalAuthorName":"汪红兵"},{"authorName":"徐安军","id":"1bd30075-d4e4-4b6a-96b2-338400bf9814","originalAuthorName":"徐安军"},{"authorName":"田乃媛","id":"5fb8d59d-3a91-4fb1-a431-16be6f304cf8","originalAuthorName":"田乃媛"},{"authorName":"贺东风","id":"bd2adc6e-f9bb-4bf6-b1a2-052df25aef8d","originalAuthorName":"贺东风"}],"doi":"","fpage":"22","id":"12e014e8-3c14-470e-bcf8-eac398ab9a5b","issue":"2","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"b0eef64c-4c36-44c8-bbae-f93fa8e7390c","keyword":"不锈钢","originalKeyword":"不锈钢"},{"id":"6e9fdff2-0ae7-4b13-a71a-deb1c9a7372f","keyword":"AOD炉","originalKeyword":"AOD炉"},{"id":"72e725fc-96e4-4973-94f4-440c63688161","keyword":"冶炼周期","originalKeyword":"冶炼周期"}],"language":"zh","publisherId":"gt201202005","title":"AOD炉的高效化冶炼模型","volume":"47","year":"2012"}],"totalpage":235,"totalrecord":2341}