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设计了一种适合于铌合金注射成形的低残碳粘结剂体系,为68% PW-5% LDPE-22% PMMA-5%SA(质量分数),并研究其脱脂工艺.结果表明:脱脂时间、温度及样品厚度对溶剂脱脂率影响显著.采用三氯乙烯为溶剂,在脱脂温度为40℃,溶剂脱脂6h,即可使粘结剂脱除率达到52.8 %,使后继热脱脂时间缩短至7.5 h.以粘结剂的DSC差热分析结果为指导,可快速制定合理的热脱脂工艺,在真空热脱脂气氛条件下可使脱脂坯残余碳、氧含量得到有效控制,分别为0.18%,0.25 %.

参考文献

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