欢迎登录材料期刊网

材料期刊网

高级检索

采用液相共沉淀法制备了Mg/Al-NO3--LDHs;以月桂酸为插层剂,采用离子交换法对合成产物进行了插层改性;采用X射线衍射(XRD)、热重及差热分析(TG-DTA)、红外光谱(FT-IR)、扫描电镜(SEM)、比表面积分析仪、四球摩擦实验机和齿轮实验机等对合成产物的结构和性能进行了评价.结果表明,插层前,晶体呈六方片状,晶片大小在50~70 nm,比表面较大(137.66m2/g).月桂酸插层后,产物的通道高度增加,但比表面积显著降低;Mg/Al-NO3--LDHs及其月桂酸插层产物可明显降低金属摩擦副的摩擦系数、磨斑直径、润滑介质温度以及驱动电机功耗,是具有良好应用前景的润滑-减摩-节能材料.

参考文献

[1] Miyata S .Anion-exchange properties of hydrotalcite-like compounds[J].Clays and Clay Minerals,1983,31:305-311.
[2] Gago S;Dias AS;Monteiro B;Pillinger M;Valente AA;Santos TM;Goncalves IS .Synthesis and characterization of layered double hydroxides intercalated by an oxomolybdenum complex[J].The journal of physics and chemistry of solids,2006(5/6):1011-1015.
[3] 段雪;张法智.插层组装与功能材料[M].北京:化学工业出版社,2007:7-18.
[4] Zhan L;Zhuang J P .Hydrogenation of ethyl acetate to ethanol over Ni-based catalysts obtained from Ni/Al hydrotalcite-like compounds[J].Molecules,2010,15:5139-5152.
[5] Wei M;Shi SX;Wang J;Li Y;Duan X .Studies on the intercalation of naproxen into layered double hydroxide and its thermal decomposition by in situ FT-IR and in situ HT-XRD[J].International Journal of Quantum Chemistry,2004(7):2534-2541.
[6] Fudala A.;Kiricsi I.;Palinko I. .Preparation and characterization of hybrid organic-inorganic composite materials using the amphoteric property of amino acids: Amino acid intercalated layered double hydroxide and montmorillonite[J].Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics,1999(21):4653-4658.
[7] 史翎,李殿卿,李素锋,王建荣,Evans D G,段雪.Zn-Mg-Al-CO3 LDHs的结构及其抑烟和阻燃性能[J].科学通报,2005(04):327-330.
[8] Palmer S J;Frost R L .Use of hydrotalcite for the removal of toxic anions from aqueous solution[J].Industrial and Engineering Chemistry Research,2010,49:8969-8976.
[9] 董伟达.工程机械减摩自修复材料技术[J].机械工程师,2003(03):3-6.
[10] 张博,徐滨士,许一,王晓丽.微纳米层状硅酸盐矿物润滑材料的摩擦学性能研究[J].中国表面工程,2009(01):29-32,36.
[11] 欧忠文,刘维民,徐滨士,丁培道,马世宁.月桂酸铅的原位合成及摩擦学性能研究[J].中国矿业大学学报,2001(05):506-510.
[12] 郑崇辉,王君,刘岩峰,孙炜岩,仲崇娜,尤佳,景晓燕,张密林,段雪.阴离子柱撑磁性镍铝水滑石的制备及表征[J].应用化学,2007(08):883-887.
[13] 董凌,陈国需,方建华,娄方.Mg-Sn型复合纳米粒子的摩擦学和磨损修复性能[J].石油学报(石油加工),2009(z1):67-72.
[14] 董凌,陈国需,方建华,娄方.Si-Sn型复合纳米粒子添加剂的摩擦磨损和自修复性能[J].石油炼制与化工,2008(11):39-44.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%