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介绍了行业标准--金锗合金化学分析方法两个标准分析方法的制定过程。第1部分,锗量的测定采用电感耦合等离子体发射光谱法,测定范围为0.5%~5%;第2部分锗量的测定新采用碘酸钾电位滴定法,测定范围为5%~30%。

The process of two standard analytical methods for gold germanium alloy chemical analysis as an industry standard was introduced. The first part is the determination of germanium content, method using inductively coupled plasma atomic emission spectrometry, measuring range is 0.5%~5%; the second part is the determination of germanium content, method using potassium iodate potentiometric titration, measuring range is 5%~30%.

参考文献

[1] Q/GYB105.1-2012.金锗合金化学分析方法锗量的测定碘酸钾电位滴定法[S].昆明:贵研铂业股份有限公司,2012.
[2] Q/GYB105.2-2012.金锗合金化学分析方法锗量的测定电感耦合等离子体原子发射光谱法[S].昆明:贵研铂业股份有限公司,2012.
[3] GB/T 23523-2009.再生锗原料中锗的测定方法[S].北京:中国标准出版社,2009.
[4] GB/T 23513-2009.锗精矿化学分析方法第 1 部分:锗量的测定碘酸钾滴定法[S].北京:中国标准出版社,2009.
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[6] Sung-Min Choi;Gae-Ho Lee;Jae-Kil Han .Determination of Trace Elements of Ge and P in a Gold Bonding Wire by Inductively Coupled Plasma Atomic Emission Spectrometry[J].Bulletin of the Korean Chemical Society,2008(2):393-397.
[7] LiuPengyu;Li Na;Shao Rongzhen .ICP-AES Determination of Germanium in GdSiGe Series Alloys as Magnetic Refrigeration Material[J].Journal of Rare Earths,2007(3):377-380.
[8] Yuetsu Danzaki;Kazuaki Wagatsuma .Prevention of Ge Volatilization in the Chemical Treatment of Ge-Cr-Al-Ce-Sm Amorphous Alloy for the Determination of Ge by ICP-AES[J].Analytical Sciences: The International Journal of The Japan Society for Analytical Chemistry,2002(7):847-849.
[9] 李莎莎,申志云.电感耦合等离子体原子发射光谱法测定锡锗中间合金中锗[J].理化检验-化学分册,2008(08):732-733.
[10] GB/T 26292-2010.金锗蒸发料[S].北京:中国标准出版社,2009.
[11] 杨萍;宋永胜;陈云红 等.金锗合金的溶样方法[P].中国,CN98103054.8,2000-02-02.
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