本文以硅渣为主要原料,利用熔融法制备了高强度微晶玻璃.采用差热分析(DTA)、X射线衍射(XRD)和扫描电镜(SEM)研究了不同晶化温度对硅渣微晶玻璃的晶相演变、显微结构、形成机理和样品性能的影响规律.研究结果表明:在最佳晶化温度870℃时,主晶相为铁板钛矿(Fe2 TiO5)和透辉石(CaMgSi2O6)复合晶相,微观结构致密,晶粒呈球状,抗折强度为270MPa,维氏显微硬度为989.72MPa,耐化学腐蚀性能较好.
参考文献
| [1] | S .M.Salman,H.Darwish,E.A.Mahdy.The influence of Al2O3,MgO and ZnO on the crytallization characteristic and properties of lithium silicate glasses and glass-ceramics[J].Materials Chemistry and Physics,2008,112 |
| [2] | Paya J,Monzo J,Borrachero M.Physical,chemical and mechanical properties of fluid catalytic cracking catalyst residue (FC3R) blended cements[J].Cement and Concrete Research,2001(31):57~61.,2001. |
| [3] | Raungrut Cheerarot,Chai Jaturapitakkul.A study of disposed fly ash from landfill to replace Portland cement[J].Waste Management.2004,Vol.24 (7):701~709.,2004. |
| [4] | Massimiliano Guazzato,Mohammad Albakry,Simon P Ringer,Michael V Swain .Strength,fracture toughness and microstructure of a selection of all-ceramic materials.Part Ⅰ.Pressable and alumina glass-infiltrated ceramics[J].Dental Materials,2003,20(5):441~448.,2003. |
| [5] | W .Li,B.S.Mitchell.Nucleation and crystallization in calcium aluminate glasses,[J].Non-Cryst.Sol.1999,1999,255 |
| [6] | 张全鹏,刘立强,井敏,李航,王明国,牛文贺,王正,邢瑞平.钢渣-赤泥微晶玻璃的制备及性能[J].材料科学与工程学报,2013(06):896-900. |
| [7] | 杨家宽,肖波,唐东羚,王秀萍.钢渣基微晶玻璃的制备与显微结构分析[J].材料科学与工程学报,2003(01):34-36. |
| [8] | 姜斌,张金朝,宋鹂.Ce-YAG微晶玻璃的制备及其发光性能[J].材料科学与工程学报,2012(01):45-49. |
| [9] | 宁莉萍,王齐华,简令奇.微晶玻璃的摩擦学特性研究进展[J].材料科学与工程学报,2005(02):306-309. |
| [10] | 杨娟 .LTCC基板用MgO-Al<,2>O<,3>-SiO<,2>系微晶玻璃及其流延工艺研究[D].国防科学技术大学,2006. |
| [11] | 王浩,陆雷,吴国芳,隋普辉.低温烧结法制备LZS系微晶玻璃及其性能[J].材料科学与工程学报,2008(04):616-619. |
| [12] | Institute of Nuclear Energy Research .Research and development of the Utilization of MSW Incinerator Ashes (Third Year):The Evaluation of Thermal Plasma Molten Method for Treating MSW Incinerator Fly Ashes[J].EPA of ROC,2000,8:The Evaluation of Thermal Plasma Molten Method for Treating MSW Incinerator Fly Ashes[J].EPA of ROC,EPA-89-U1H1-03-280,2000,8:1~8,2000. |
| [13] | Barbieri L.,Karamanov A.,Corradi A.,et al .Structure,chemical durability and crystallization behavior of incineratorbased glassy systems[J].Non-crystalline Solids,2008,354 |
| [14] | E .M,Rabinovich.Nucleation and crystallization in glass[J].Amer.Cera.Soei.,1982,61(3):334.,1982. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%