{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":4,"startPagecode":1},"records":[{"abstractinfo":"建立了动物性食品中包括代谢产物在内的54种有机磷农药残留及其代谢产物的双气相色谱-双脉冲火焰光度检测器( GC- PFPD)检测方法.动物组织样品经丙酮提取后以二氯甲烷进行液-液萃取,经凝胶渗透色谱净化后采用配有双脉冲火焰光度检测器的气相色谱仪测定.采用外标法定量,有机磷农药的响应与其浓度在线性范围内均呈良好的线性关系,相关系数在0.9905 ～0.9999之间.分别在空白鸡肉、羊肉、牛肉和猪肉样品中添加低、中和高3个加标水平的标准品进行了回收试验,回收率在50.5％ ～ 128.1％之间,相对标准偏差(n=6)在1.1％～25.5％之间,证明该方法的精密度和准确度良好.各有机磷农药的检出限在0.001 ～0.170mg/kg之间,定量限在0.002 ～0.455 mg/kg之间.对从市场采集的动物组织样品进行了测定,检出敌敌畏、乙拌磷亚砜等有机磷农药残留.本方法灵敏度高、特异性强,且能同时检测有机磷农药多残留及其代谢产物,能够更加真实地反映动物性食品中有机磷农药的残留水平.","authors":[{"authorName":"<span style=\"color:red\">杨立新</span>","id":"8dbf9c3d-161a-486e-985d-616f810f190c","originalAuthorName":"杨立新"},{"authorName":"李荷丽","id":"b8510654-da0d-42ca-a83d-c0aaf3fce665","originalAuthorName":"李荷丽"},{"authorName":"苗虹","id":"c4bb17a9-5287-49dd-b86c-429a79327783","originalAuthorName":"苗虹"},{"authorName":"曾凡刚","id":"0f2032cf-1ebb-4ac4-b2e7-cb1436fab9a5","originalAuthorName":"曾凡刚"},{"authorName":"李瑞丰","id":"6173737d-11d5-4ff4-a8a2-8b18ce1505ec","originalAuthorName":"李瑞丰"},{"authorName":"陈惠京","id":"7402e7ad-46f8-49af-9e64-8c078ae518bc","originalAuthorName":"陈惠京"},{"authorName":"赵云峰","id":"ffce6f67-002b-4850-93a9-4da8f95e0a05","originalAuthorName":"赵云峰"},{"authorName":"吴永宁","id":"10ca9dc6-ce3f-4d8a-b672-e74c352b73da","originalAuthorName":"吴永宁"}],"doi":"10.3724/SP.J.1123.2011.01010","fpage":"1010","id":"4e2da9a9-08e0-4722-9b07-de2aa9500973","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"c7647bbf-1beb-46ec-9f89-ea93e0a45e42","keyword":"凝胶渗透色谱净化","originalKeyword":"凝胶渗透色谱净化"},{"id":"fb327f75-37b8-4771-accc-0206ddf1948e","keyword":"双气相色谱-双脉冲火焰光度检测","originalKeyword":"双气相色谱-双脉冲火焰光度检测"},{"id":"99f2665e-ed63-4b4e-a68e-5d91e0bd0356","keyword":"有机磷农药","originalKeyword":"有机磷农药"},{"id":"fc445300-3a32-4a46-8ee5-b80316cdb8a4","keyword":"代谢产物","originalKeyword":"代谢产物"},{"id":"249ccf40-65f1-4870-b414-02abb4f9704e","keyword":"动物性食品","originalKeyword":"动物性食品"}],"language":"zh","publisherId":"sp201110012","title":"双气相色谱-双脉冲火焰光度法高通量检测动物性食品中有机磷农药残留及其代谢产物","volume":"29","year":"2011"},{"abstractinfo":"在前期大量古铜矿冶炼遗物系统研究的基础上,本文利用ICP等手段对一些出土先秦时期的冶炼红铜与自然铜进行了稀土等微量元素的测定和对比分析,初步结果显示,稀土等微量元素含量可以作为区分冶炼红铜和自然铜的判别标志.","authors":[{"authorName":"秦颖","id":"758199f4-fce6-4744-840e-20cca1e19325","originalAuthorName":"秦颖"},{"authorName":"罗武干","id":"174c4293-28f8-4272-89a4-4b9e74b10ea3","originalAuthorName":"罗武干"},{"authorName":"魏国锋","id":"9df4f8bd-aa58-4fa2-8d22-5cc24e0a06e2","originalAuthorName":"魏国锋"},{"authorName":"王昌燧","id":"5c10f1c4-3268-4ecf-915b-751fc861bf01","originalAuthorName":"王昌燧"},{"authorName":"<span style=\"color:red\">杨立新</span>","id":"a3b5e8e2-abc9-4426-ac2d-b6addc87b84a","originalAuthorName":"杨立新"},{"authorName":"龚长根","id":"24a7fc1f-1e4a-4435-a8f8-846dfd8cf11c","originalAuthorName":"龚长根"},{"authorName":"曲艺","id":"1854cf4c-1f01-41da-b532-18185597301a","originalAuthorName":"曲艺"}],"doi":"10.3969/j.issn.1004-0277.2007.04.018","fpage":"75","id":"77662e08-b184-495e-8ef5-deec249b8998","issue":"4","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"999deaf0-34a0-417f-80bf-c1a030b8b720","keyword":"冶炼红铜","originalKeyword":"冶炼红铜"},{"id":"9d79764f-e02b-4833-b76d-ff10b5b87801","keyword":"自然铜","originalKeyword":"自然铜"},{"id":"d618483b-cc07-4071-8a7e-a4e5e76c84dd","keyword":"稀土元素","originalKeyword":"稀土元素"},{"id":"a7fb372c-726c-4d52-9f2b-1728217f5b3d","keyword":"区分","originalKeyword":"区分"}],"language":"zh","publisherId":"xitu200704018","title":"利用稀土等微量元素区分自然铜与早期冶炼红铜的初步研究","volume":"28","year":"2007"},{"abstractinfo":"本文利用CFD模拟手段对电加热水箱换热器流动传热特性进行三维数值计算,通过对流场和温度场的分析,改进原设计中不利于热量传递的结构特征.在保证水箱基本结构尺寸不变的前提下,对箱体内两块折流板的位置及其几何形状进行多种结构模型的数值模拟和比较分析,实现了基于CFD数值模拟结果进行换热器局部结构优化设计的工程应用.","authors":[{"authorName":"赵楠","id":"f9d267c4-53a5-416c-8b90-f3d8ddd24135","originalAuthorName":"赵楠"},{"authorName":"<span style=\"color:red\">杨立新</span>","id":"0370fadf-2853-4a82-afa6-45c97bcb93ce","originalAuthorName":"杨立新"}],"doi":"","fpage":"1039","id":"44081663-08ca-4cce-a475-5d761cf83a90","issue":"6","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"a80ecc59-e017-40eb-8477-1d31a22064ad","keyword":"换热器","originalKeyword":"换热器"},{"id":"3c038189-6c6f-4c61-86f5-0bf771e57d0e","keyword":"CFD","originalKeyword":"CFD"},{"id":"a76d6cc1-c924-4779-9b8e-6126b8e0237e","keyword":"优化设计","originalKeyword":"优化设计"}],"language":"zh","publisherId":"gcrwlxb200906038","title":"CFD在换热器局部结构优化设计的应用","volume":"30","year":"2009"},{"abstractinfo":"本文通过实验及理论分析,对Ni纳米线在旋转磁场下的运动行为进行研究.Ni纳米线的旋转运动分为同步旋转和异步旋转两种形式.通过受力分析结合量纲比较的手段得到,本文研究范围内流体惯性作用、纳米线运动惯性作用的影响可以忽略,而磁场力矩和流体力矩是控制纳米线旋转运动的主要因素.建立了纳米线旋转运动的控制模型,并得到了区分同步旋转和异步旋转运动的判据.分别针对同步旋转运动和异步旋转运动进行分析,对比不同参数对纳米线运动的影响.","authors":[{"authorName":"<span style=\"color:red\">杨立新</span>","id":"1a209933-5b7b-4791-b5b0-73e6104cfa46","originalAuthorName":"杨立新"},{"authorName":"赵楠","id":"62b5a2ad-76a6-490a-a48f-1a02edd15074","originalAuthorName":"赵楠"}],"doi":"","fpage":"838","id":"4887f05a-0ac9-4b4e-965d-26100e060a69","issue":"4","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"be6be22f-b4b6-4cb6-b41a-5352b27e472e","keyword":"Ni纳米线","originalKeyword":"Ni纳米线"},{"id":"c3b54178-fc23-4368-a92f-50208f0e610d","keyword":"旋转磁场","originalKeyword":"旋转磁场"},{"id":"9a37cee4-93e2-404c-852f-7d08060ba84c","keyword":"同步异步旋转","originalKeyword":"同步异步旋转"}],"language":"zh","publisherId":"gcrwlxb201504030","title":"Ni纳米线在旋转磁场下的运动行为研究","volume":"36","year":"2015"},{"abstractinfo":"本文以去离子水为实验工质,对常压下竖直窄缝通道内过冷流动沸腾的气泡特性进行了实验研究.通过可视化实验分析发现,汽化核心密度主要受壁面过热度影响,气泡脱离直径受壁面过热度、主流过冷度以及质量流速影响.拟合了汽化核心密度和气泡脱离直径的经验关系式,预测结果与实验值误差较小.","authors":[{"authorName":"郭昂","id":"820cac88-720d-40e7-81fd-1704173b3324","originalAuthorName":"郭昂"},{"authorName":"<span style=\"color:red\">杨立新</span>","id":"94034484-042b-41c7-ab15-ae5d620c126f","originalAuthorName":"杨立新"}],"doi":"","fpage":"1836","id":"50454351-3f1f-481c-9ff6-a63fc42b5151","issue":"9","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"be583b73-ddeb-4a7f-94b7-4d2f5949f4ac","keyword":"窄缝通道","originalKeyword":"窄缝通道"},{"id":"42c4fdea-22f8-42ad-8617-63cc2666cc9b","keyword":"过冷沸腾","originalKeyword":"过冷沸腾"},{"id":"d5a3517c-14bc-4c87-a299-f933f8c2fb3f","keyword":"气泡","originalKeyword":"气泡"}],"language":"zh","publisherId":"gcrwlxb201409034","title":"竖直矩形窄缝通道过冷流动沸腾的实验研究","volume":"35","year":"2014"},{"abstractinfo":"综述了无甲醛耐热荧光树脂颜料的研究进展,并介绍了这类荧光颜料的制备方法、特点及应用领域.","authors":[{"authorName":"潘煜怡","id":"776514bb-3dc2-45e1-93c1-23022764c4b5","originalAuthorName":"潘煜怡"},{"authorName":"马胜军","id":"ec38b837-0610-40ce-ab4d-adceef03c0a1","originalAuthorName":"马胜军"},{"authorName":"富秀玲","id":"52f3d10d-0f48-40c7-a1fa-db6e77f45969","originalAuthorName":"富秀玲"},{"authorName":"李敏","id":"d156eab2-1169-4994-8aac-47e89290a7c2","originalAuthorName":"李敏"},{"authorName":"<span style=\"color:red\">杨立新</span>","id":"79b52bfd-c51c-49da-9d33-fba0767ac96b","originalAuthorName":"杨立新"}],"doi":"10.3969/j.issn.0253-4312.2003.07.014","fpage":"39","id":"9c162dd1-d699-4b2a-9e20-3ec94cb7e4ab","issue":"7","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"3e6f2847-db93-4409-a3cd-64007c947dd0","keyword":"荧光树脂颜料","originalKeyword":"荧光树脂颜料"},{"id":"92893d1c-6fd1-43e4-b328-bb8fc4b2db1e","keyword":"无甲醛","originalKeyword":"无甲醛"},{"id":"eb524f67-01b7-460c-b8a0-0d7a77aba93e","keyword":"耐热颜料","originalKeyword":"耐热颜料"}],"language":"zh","publisherId":"tlgy200307014","title":"无甲醛耐热荧光树脂颜料的研究进展","volume":"33","year":"2003"},{"abstractinfo":"以聚乳酸二醇、六次甲基二异氰酸酯和二溴新戊二醇设计合成出一系列阻燃型聚乳酸基聚氨酯.通过核磁、凝胶色谱和红外等表征了材料的结构性能.结果表明,二溴新戊二醇作为扩链剂可满足制备高相对分子质量聚氨酯的要求,材料的热学性能随聚乳酸二醇相对分子质量和硬段质量分数的增加而增加.同时该类聚氨酯具有较好的力学性能,拉伸强度在50 MPa附近,接近工业级别的聚乳酸.材料的阻燃性能随着溴质量分数的增加而增强.当溴质量分数为8.6％,聚氨酯的极限氧指数(LOI)为28,属于难燃级别材料.","authors":[{"authorName":"<span style=\"color:red\">杨立新</span>","id":"441c485a-fa1b-41e5-84c5-0da73f2f7097","originalAuthorName":"杨立新"},{"authorName":"胡秀丽","id":"fa15f333-e6f1-4655-959f-aababde4237f","originalAuthorName":"胡秀丽"},{"authorName":"黄宇彬","id":"2624d18c-d6b4-4b90-be65-d6a9e2ba15ff","originalAuthorName":"黄宇彬"},{"authorName":"景遐斌","id":"87127cff-3179-4215-bb81-00fbb446bf8d","originalAuthorName":"景遐斌"}],"doi":"10.11944/j.issn.1000-0518.2016.01.150174","fpage":"47","id":"a9eeddda-7bd9-4822-bf98-549d683dbfa6","issue":"1","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"660f914b-3d24-4aa0-adfe-2b7133109302","keyword":"含溴阻燃剂","originalKeyword":"含溴阻燃剂"},{"id":"9b54494d-3840-4788-8114-28800a2782c3","keyword":"聚乳酸","originalKeyword":"聚乳酸"},{"id":"a2d68351-4ef4-44a7-bf51-fd1b3ebc6329","keyword":"聚氨酯","originalKeyword":"聚氨酯"}],"language":"zh","publisherId":"yyhx201601006","title":"阻燃型聚乳酸基聚氨酯的合成与表征","volume":"33","year":"2016"},{"abstractinfo":"蛭石改型与功能化制备复合功能材料属于层状硅酸盐高值化利用领域.本文总结了蛭石改型的方法,探讨了储热、催化、环境、保温、抗菌、隔声等蛭石基功能复合材料的研究进展.同时指出了蛭石基功能复合材料今后的发展方向.","authors":[{"authorName":"李传常","id":"0cd9dd3a-fac1-4a2e-ba96-33c0ac5852bc","originalAuthorName":"李传常"},{"authorName":"<span style=\"color:red\">杨立新</span>","id":"60146113-491a-4348-9869-f51597df6ee1","originalAuthorName":"杨立新"},{"authorName":"肖桂雨","id":"31508275-92f3-4bd3-bc33-58f00c685f80","originalAuthorName":"肖桂雨"},{"authorName":"曾铃","id":"e2baa2cd-ee91-4c0a-a0eb-e6ac91c891b6","originalAuthorName":"曾铃"},{"authorName":"何忠明","id":"0266f6ee-3a69-4265-b030-2febae11f833","originalAuthorName":"何忠明"},{"authorName":"陈荐","id":"a9fb4d91-7bde-4a41-ae71-80b6b8a23764","originalAuthorName":"陈荐"}],"doi":"","fpage":"1203","id":"11de7853-4169-4ecc-80d3-e34b08ef6b2e","issue":"4","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"e35678ae-ffc9-4c3d-a1aa-de1fb80947a3","keyword":"蛭石","originalKeyword":"蛭石"},{"id":"d2b3408a-6242-451c-b93b-0dff2a055099","keyword":"改型","originalKeyword":"改型"},{"id":"63722e76-51bf-4918-abaf-679b6b2e638a","keyword":"功能化","originalKeyword":"功能化"}],"language":"zh","publisherId":"gsytb201704018","title":"蛭石改型及其功能化研究进展","volume":"36","year":"2017"},{"abstractinfo":"通过混合集成型结构光学拾音器的光学设计和芯片设计,制作了包含微光学棱镜、光电探测器和信号放大电路的混合集成型光学拾音器.经过测试,发现有较好的信号输出特性,表明混合集成型光学拾音器已基本研制成功.","authors":[{"authorName":"刘畅","id":"6e20a981-25ca-487a-9210-cb9b5dddd674","originalAuthorName":"刘畅"},{"authorName":"<span style=\"color:red\">杨立新</span>","id":"3c745b3c-4d1c-4eb8-8c1b-e3a26697e1bb","originalAuthorName":"杨立新"},{"authorName":"陈学良","id":"ebd4b00c-0cc0-4452-8df1-0d188f2037bf","originalAuthorName":"陈学良"}],"doi":"10.3969/j.issn.1007-4252.2002.02.012","fpage":"149","id":"152e6bb6-a552-4685-a3d8-eafee207801d","issue":"2","journal":{"abbrevTitle":"GNCLYQJXB","coverImgSrc":"journal/img/cover/GNCLYQJXB.jpg","id":"34","issnPpub":"1007-4252","publisherId":"GNCLYQJXB","title":"功能材料与器件学报   "},"keywords":[{"id":"d2f2a7ea-ca36-40c4-be14-641c811f32a6","keyword":"混合集成型光学拾音器","originalKeyword":"混合集成型光学拾音器"},{"id":"f9c1339c-ccc3-42e5-a7e2-e7aee6e72f61","keyword":"微光学棱镜","originalKeyword":"微光学棱镜"},{"id":"632fe5b8-932a-448f-bed2-bad3e17363c8","keyword":"光电探测器","originalKeyword":"光电探测器"},{"id":"24d09801-cb8f-42bd-a7cc-0e7d3cebb8ac","keyword":"CMOS集成电路","originalKeyword":"CMOS集成电路"}],"language":"zh","publisherId":"gnclyqjxb200202012","title":"混合集成型光学拾音器的设计与制作","volume":"8","year":"2002"},{"abstractinfo":"本文应用MUSIG模型[1]和均一直径模型对某溶液堆台架模型堆芯内气液流动传热进行了数值模拟.在MUSIG模型中堆芯内离散相气泡被分为5组不同直径的气泡,用于分析堆芯内气泡的流动变化和大小分布,采用Luo and Svendsen[2]和Prince and Blanch[3]模型描述不同直径气泡组间的破裂和聚合.在均一直径模型中,堆芯内的气体被考虑为同一直径的组分,并且不考虑其破裂与聚合现象.计算得到采用两个模型的模拟结果并且对其进行了对比研究.结果显示应用MUSIG模型的计算结果与台架实验结果吻合更好.","authors":[{"authorName":"<span style=\"color:red\">杨立新</span>","id":"eefa7d0c-63c5-4752-8023-6aa12ab23177","originalAuthorName":"杨立新"},{"authorName":"巴黎明","id":"283c35e0-48e9-49e1-936c-d4529057f6ff","originalAuthorName":"巴黎明"},{"authorName":"李星","id":"76ca296c-1722-4de0-9b4b-beadd1da8abd","originalAuthorName":"李星"}],"doi":"","fpage":"93","id":"a9d546e9-74ff-4ca3-95a7-9f566693d8b0","issue":"z2","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"679ab0d4-77dd-4adc-bcb8-d6e088cfcb4f","keyword":"MUSIG","originalKeyword":"MUSIG"},{"id":"23704aa3-9093-4181-a044-856edcbd87c7","keyword":"均一直径","originalKeyword":"均一直径"},{"id":"245a6cb8-c566-44d8-844b-31f74be0acc5","keyword":"两相流","originalKeyword":"两相流"},{"id":"e29ad8bc-c7ec-41a8-8e1c-f591bb7340d4","keyword":"溶液堆","originalKeyword":"溶液堆"}],"language":"zh","publisherId":"gcrwlxb2007z2025","title":"两种气液两相流模型的应用和比较","volume":"28","year":"2007"}],"totalpage":4,"totalrecord":39}