{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以草酸和乙酸镍为原料,通过低温固相法合成前驱体(NiC2O4.2H2O)粉末。用此前驱体粉末与固态NaOH混合并充分研磨制得纳米Ni(OH)2粉末。经SEM、XRD测试表明,制得的纳米Ni(OH)2粉末是平均粒径约为12nm的β-Ni(OH)2。用循环伏安法、恒流充放电测试和交流阻抗谱研究Ni(OH)2电极的电化学电容特性。结果表明在电流密度为1A.g-1时,其比电容高达2271F.g-1,且经多次循环后表现出较好的循环稳定性能。","authors":[{"authorName":"","id":"e692100f-8752-405d-a768-4cdb5245b436","originalAuthorName":"刘亚威"},{"authorName":"赵雯雯","id":"e6c22d1a-3ff9-452c-b51c-61e280840453","originalAuthorName":"赵雯雯"},{"authorName":"张昌远","id":"6320c00d-d358-470f-8346-5e6f60be37c4","originalAuthorName":"张昌远"},{"authorName":"黄祥平","id":"88c6fd63-79d1-4287-99f7-0aba99d3c690","originalAuthorName":"黄祥平"},{"authorName":"毛峰","id":"7fe8ded3-8c75-42c5-a598-10f34c1aec0b","originalAuthorName":"毛峰"},{"authorName":"杨学林","id":"8bacf16a-c703-4fd4-ab72-0b6b6e86af04","originalAuthorName":"杨学林"}],"doi":"","fpage":"606","id":"76e93ee5-953e-451a-bb7e-ec62183e9347","issue":"4","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"df7bc841-1e7e-4741-aa75-e5c58b0b8c6b","keyword":"氢氧化镍","originalKeyword":"氢氧化镍"},{"id":"424b5f1c-3b0f-4449-87c8-c12ec1b78fe9","keyword":"低温固相法","originalKeyword":"低温固相法"},{"id":"2c16081e-ec84-4dd3-ace2-d8b6e0637039","keyword":"超级电容器","originalKeyword":"超级电容器"}],"language":"zh","publisherId":"clkxygc201204025","title":"高比容纳米Ni(OH)_2的制备及其电化学电容性能","volume":"30","year":"2012"},{"abstractinfo":"在酸性介质中,Ce(Ⅳ)氧化连二亚硫酸钠产生较弱的化学发光,异丙可以明显增强此发光,增加的发光强度与异丙的质量浓度在0.1~10 mg/L范围内呈良好的线性关系(r=0.999 7),由此建立了一种测定异丙的流动注射化学发光新方法,检出限为80 μg/L(3σ). 对1.0 mg/L的异丙连续平行测定11次,其相对标准偏差为3.3%. 用于测定环境水样和大米中异丙含量,回收率为96.1%~99.4%.","authors":[{"authorName":"何树华","id":"ddd88840-b82f-4dbe-96bc-8c6b25f77861","originalAuthorName":"何树华"},{"authorName":"何德勇","id":"262a9e5f-a82a-4402-ad02-84c20f0eefb2","originalAuthorName":"何德勇"},{"authorName":"章竹君","id":"6615a3ad-3033-4433-8e65-1a8bc6e98c59","originalAuthorName":"章竹君"}],"doi":"10.3969/j.issn.1000-0518.2006.11.025","fpage":"1298","id":"5b26f68e-711a-4916-8ae1-a967fbaff776","issue":"11","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"6b2de841-074a-44ad-aaec-d1798c023745","keyword":"化学发光","originalKeyword":"化学发光"},{"id":"08c3aee1-5095-4292-bf30-13e1829bebef","keyword":"流动注射","originalKeyword":"流动注射"},{"id":"30b6f22a-ba76-4bf0-bf43-de9c87b6cfa6","keyword":"连二亚硫酸钠","originalKeyword":"连二亚硫酸钠"},{"id":"7d855b27-3bab-486d-9c28-ce3220cdaf9a","keyword":"异丙","originalKeyword":"异丙威"}],"language":"zh","publisherId":"yyhx200611025","title":"流动注射化学发光法测定异丙","volume":"23","year":"2006"},{"abstractinfo":"文中,关于贝氏体形成机制,包括形核过程的文献很少被引述。作者(等)的主要论点为贝氏体铁素体以无扩散、非切变机制在奥氏体内贫碳区形核,并未引述形成贫碳区的必要条件。本文作者强调,在钢及铜合金中,不可能由Spinodal分解和位错偏聚形成贫溶质区。等的理念未得到先进理论观点和精细实验结果的支持。在文中,据此对临界核心大小和形核能的计算并无显著意义,期望青年学者对贝氏体相变机制作进一步研究。","authors":[{"authorName":"徐祖耀","id":"f5bc6b26-ec4d-45e7-a1da-067daa9d3115","originalAuthorName":"徐祖耀"}],"doi":"","fpage":"158","id":"66a9e9e8-09a0-408c-8c33-bc00aeff35c0","issue":"2","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"5224cfe0-dd6d-4ccc-aac3-2bed80f388a5","keyword":"贝氏体形核","originalKeyword":"贝氏体形核"},{"id":"cae16aae-8a2b-43f5-9886-1ca5759c5972","keyword":"扩散机制","originalKeyword":"扩散机制"},{"id":"36bc9f8f-ee13-4c27-8020-c2c5b0dfca8f","keyword":"切变机制","originalKeyword":"切变机制"},{"id":"a3bb808d-ba7a-4c9a-90ff-d5e59a6a0f1a","keyword":"贫碳区","originalKeyword":"贫碳区"}],"language":"zh","publisherId":"jsrclxb201202033","title":"评宗昌等《贝氏体铁素体的形核》一文","volume":"33","year":"2012"},{"abstractinfo":"利用质子激发X射线荧光分析(PIXE)测试分析汝官瓷、张公巷窑青瓷和家门窑青瓷样品的主要化学组成,用多元统计判别分析方法对数据进行分析,以确定它们的分类和起源关系.结果表明:汝官瓷、张公巷窑青瓷和家门窑青瓷釉基本能很好的区分;但是胎区分得不是很理想,张公巷窑青瓷的胎可以和汝官瓷、家门窑青瓷胎很好的区分,汝官瓷胎和家门窑青瓷胎有个别样品不能分开.","authors":[{"authorName":"蔡敏敏","id":"bf1f4660-208a-4999-ac81-266bf48c5bcb","originalAuthorName":"蔡敏敏"},{"authorName":"李国霞","id":"f8d3a4dc-7472-4dd6-9382-9f4430feef58","originalAuthorName":"李国霞"},{"authorName":"赵维娟","id":"9572b140-eca3-4192-af6e-ab9fdb21502b","originalAuthorName":"赵维娟"},{"authorName":"李融武","id":"e2d1fb82-016c-4ae3-9ee6-0cabbe60a2a0","originalAuthorName":"李融武"},{"authorName":"赵文军","id":"ea875a05-c1f7-4a8f-b405-2005de7db87c","originalAuthorName":"赵文军"},{"authorName":"承焕生","id":"9ff5fa85-a1fb-4cd2-bdc3-3bd240fd6894","originalAuthorName":"承焕生"},{"authorName":"郭敏","id":"d4074d21-787e-429b-8123-a13fcf5ce433","originalAuthorName":"郭敏"}],"doi":"","fpage":"1363","id":"f1ea8842-b3fe-42a2-9557-aa4c186cac5a","issue":"6","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"d281b6ff-a4b5-41d8-ad69-47236e801de5","keyword":"汝官瓷","originalKeyword":"汝官瓷"},{"id":"adf8b648-9625-4b38-96ff-ec6174d0c5d4","keyword":"张公巷窑青瓷","originalKeyword":"张公巷窑青瓷"},{"id":"3a61e23c-a3f8-43e6-84fc-1b7cd4edef5b","keyword":"家门窑青瓷","originalKeyword":"刘家门窑青瓷"},{"id":"494e2983-99cd-4c53-a919-4bfad5b7c54a","keyword":"判别分析","originalKeyword":"判别分析"}],"language":"zh","publisherId":"gsytb201206005","title":"汝官瓷、张公巷窑青瓷和家门窑青瓷的判别分析研究","volume":"31","year":"2012"},{"abstractinfo":"建立了花生中涕灭及其代谢物涕灭砜、涕灭亚砜的高效液相色谱-线性离子阱三级质谱分析方法.样品经环己烷饱和的乙腈提取,凝胶渗透色谱净化后,用高效液相色谱-线性离子阱三级质谱法对样品中的目标物进行定性确证和定量分析.在Capcell PAK CR色谱柱上以含5 mmol/L NH4Ac-HAc的乙腈为流动相进行梯度洗脱分离.采用电喷雾离子源正离子模式进行三级选择离子监测,以涕灭-d3作为3个目标物的内标物.通过比较基质匹配曲线和纯溶剂标准曲线计算回收率评估基质效应.方法的线性范围为10 ~ 500μg/L,检出限为4~5μg/kg.涕灭、涕灭砜、涕灭亚砜在3个加标水平(10、20、40 μg/kg)的回收率为81.5%~115%,相对标准偏差为6.35%~ 15.1%.应用该方法对花生样品进行了测定,结果令人满意.","authors":[{"authorName":"杨欣","id":"cf79ed21-e40c-4c55-9b4a-26c9b0d549bc","originalAuthorName":"杨欣"},{"authorName":"李鹏","id":"b79f4450-9683-4de1-bbb4-401e4306337f","originalAuthorName":"李鹏"},{"authorName":"赵云峰","id":"040f78a9-e607-4ea7-b8ce-24b4f3fd6fa2","originalAuthorName":"赵云峰"},{"authorName":"吴永宁","id":"93e09887-4e58-4408-8ef9-7997ae8fee6f","originalAuthorName":"吴永宁"}],"doi":"10.3724/SP.J.1123.2011.11027","fpage":"309","id":"33028f97-80d2-4553-bcb1-636c0cb41f51","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"ac371baa-60da-4eae-b972-93befd51c36b","keyword":"高效液相色谱-线性离子阱三级质谱法","originalKeyword":"高效液相色谱-线性离子阱三级质谱法"},{"id":"659a271d-abd1-4598-8d1b-6607abc0ff4e","keyword":"凝胶渗透色谱净化","originalKeyword":"凝胶渗透色谱净化"},{"id":"4436a032-c8c9-4826-9f36-a75e4f30b364","keyword":"涕灭","originalKeyword":"涕灭威"},{"id":"b3fc5141-94a7-450d-93ac-99de16f334b9","keyword":"涕灭砜","originalKeyword":"涕灭威砜"},{"id":"883cddb3-4958-48a3-a760-eb05620b7e55","keyword":"涕灭亚砜","originalKeyword":"涕灭威亚砜"},{"id":"dbc29004-723d-43e4-b9f2-a3b7ada8b54e","keyword":"花生","originalKeyword":"花生"}],"language":"zh","publisherId":"sp201203016","title":"高效液相色谱-线性离子阱三级质谱法检测花生中涕灭及其代谢物涕灭砜、涕灭亚砜","volume":"30","year":"2012"},{"abstractinfo":"介绍了干式金斯气柜橡胶密封膜的工作原理、技术要求、制作材料、成型工艺及应用情况.","authors":[{"authorName":"张霞","id":"2e1291ae-fd63-4211-943b-3dba81ed85a7","originalAuthorName":"张霞"}],"doi":"10.3969/j.issn.1003-1545.2000.03.008","fpage":"26","id":"dd6477e1-5ed3-49d1-8416-4d92f6cee4f5","issue":"3","journal":{"abbrevTitle":"CLKFYYY","coverImgSrc":"journal/img/cover/CLKFYYY.jpg","id":"10","issnPpub":"1003-1545","publisherId":"CLKFYYY","title":"材料开发与应用"},"keywords":[{"id":"d57fdcc0-5a5b-4e4f-b700-3c14bf849536","keyword":"干式金斯气柜","originalKeyword":"干式威金斯气柜"},{"id":"49555d87-f801-4fae-ae34-d6f540054208","keyword":"橡胶密封膜","originalKeyword":"橡胶密封膜"},{"id":"e589b5e3-6d3e-41c1-aa91-7a66a9ce5ab2","keyword":"转炉煤气","originalKeyword":"转炉煤气"},{"id":"01f8d582-bf64-4435-917b-644a3b687062","keyword":"胶布","originalKeyword":"胶布"},{"id":"510c2ad9-bfb0-44d8-818a-14d2c275b02b","keyword":"粘接缝","originalKeyword":"粘接缝"}],"language":"zh","publisherId":"clkfyyy200003008","title":"干式金斯气柜橡胶密封膜及其应用","volume":"15","year":"2000"},{"abstractinfo":"为了精确地估计真空荧光显示器(VFD)的可靠性寿命,节省试验测试时间,通过建立加速寿命试验模型开展了4组恒定应力加速寿命试验,采用布尔函数描述VFD寿命分布,利用最小二乘法(LSM)估计布尔参数,完成了试验数据的统计分析,并自行开发了寿命预测软件,确定了加速寿命方程,实现了VFD的寿命估计.数值结果表明,试验设计方案是正确可行的,VFD的寿命服从布尔分布,其加速模型符合线性阿伦尼斯方程,每个加速应力水平下VFD的失效机理不变,精确计算出的VFD寿命对其生产厂商和技术人员具有重要的指导意义.","authors":[{"authorName":"张建平","id":"a4f4a54b-5f55-444d-a910-8899e4908540","originalAuthorName":"张建平"},{"authorName":"王睿韬","id":"c51ff80e-cd1f-4328-a582-744e0e07e0e4","originalAuthorName":"王睿韬"}],"doi":"10.3969/j.issn.1007-2780.2010.02.010","fpage":"205","id":"dd47e756-eb23-4f3f-82d6-5ec7345ea979","issue":"2","journal":{"abbrevTitle":"YJYXS","coverImgSrc":"journal/img/cover/YJYXS.jpg","id":"72","issnPpub":"1007-2780","publisherId":"YJYXS","title":"液晶与显示 "},"keywords":[{"id":"7f5443b7-07f2-44e4-a387-358873ffd2ce","keyword":"真空荧光显示器","originalKeyword":"真空荧光显示器"},{"id":"b2dd5c56-937c-423a-92e1-2abf4e8e71ce","keyword":"可靠性寿命","originalKeyword":"可靠性寿命"},{"id":"887156cc-5364-4ded-9ffb-bb6c955328dc","keyword":"加速寿命试验","originalKeyword":"加速寿命试验"},{"id":"33c661dd-acf7-4cd5-b827-80a1873ff61d","keyword":"恒定应力","originalKeyword":"恒定应力"},{"id":"e1840997-9c8d-42bc-af8e-f05c250a8f59","keyword":"布尔分布","originalKeyword":"威布尔分布"}],"language":"zh","publisherId":"yjyxs201002010","title":"布尔分布下VFD恒定应力加速寿命试验与统计分析","volume":"25","year":"2010"},{"abstractinfo":"本文采用质子激发X射线荧光分析(PIXE)技术测试了34个汝官瓷样品、30个蓝色系列钧官瓷样品(不含红釉系列)和17个家门窑青瓷样品的主量化学组成含量,根据这些样品的主量化学组成含量数据,应用多元统计分析方法进行分析.结果表明:汝官瓷、钧官瓷和家门窑青瓷的釉样品能够较好的区分开;但是3种瓷胎并不能很好的分开.","authors":[{"authorName":"肖朋飞","id":"6c5bc42f-0f99-48b4-b412-749a9ae0e046","originalAuthorName":"肖朋飞"},{"authorName":"赵红梅","id":"27edfee9-f617-4a36-af10-1a11a2aec85c","originalAuthorName":"赵红梅"},{"authorName":"李融武","id":"019184bd-8770-4aad-9618-4e2e6642f646","originalAuthorName":"李融武"},{"authorName":"赵文军","id":"6c10bb80-2026-4274-9965-bf564b102cc6","originalAuthorName":"赵文军"},{"authorName":"李国霞","id":"6f63b95a-67cb-4f68-b4b5-7c0b6f8f38e7","originalAuthorName":"李国霞"},{"authorName":"赵维娟","id":"ee11e4bc-a40c-4de3-90c4-e81dd16a55e3","originalAuthorName":"赵维娟"},{"authorName":"承焕生","id":"528f9874-c9c9-4258-bc3c-5a0d9ea8b362","originalAuthorName":"承焕生"}],"doi":"","fpage":"312","id":"3b352bdd-7627-42ad-a3b3-45e88dc561eb","issue":"2","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"080b7cee-826f-4a82-af62-9feed6531e66","keyword":"汝官瓷","originalKeyword":"汝官瓷"},{"id":"684a6128-65b6-45ce-be61-e74720b4c844","keyword":"钧官瓷","originalKeyword":"钧官瓷"},{"id":"14ccb09f-07d1-4f4b-bb41-c0ad3eea1fa0","keyword":"家门窑青瓷","originalKeyword":"刘家门窑青瓷"},{"id":"4b254520-d0a1-406e-a9ef-92267cd23fb0","keyword":"PIXE","originalKeyword":"PIXE"},{"id":"12b26595-24a4-4ea9-b303-ae046a74c72d","keyword":"因子分析","originalKeyword":"因子分析"}],"language":"zh","publisherId":"gsytb201102013","title":"汝官瓷、钧官瓷和家门窑青瓷的多元统计分析","volume":"30","year":"2011"},{"abstractinfo":"Sepharose CL-4B经碳酰二咪唑(CDI)活化后与纯化的克百抗体共价偶联,合成了免疫亲和色谱(IAC)固定相,并用其制备了对克百具有特异性亲和力的IAC柱.对IAC条件进行了优化,选择0.02 mol/L pH 7.2磷酸盐缓冲液(PB)作为吸附与平衡介质,60%(体积分数)甲醇水溶液作为洗脱剂.结果表明:在优化条件下,IAC柱对克百的动态柱容量达1.58 mg/L.当标样溶液中克百质量浓度低于 2 μg/L时,经IAC柱富集的效率高于167倍.在河水中按0.1 mg/L水平添加克百标准品,经IAC柱分离富集,洗脱液采用包被抗体直接竞争酶联免疫吸附分析(ELISA)法检测,5次重复测定的平均回收率为89.8% ,相对标准偏差为4.8% .同时采用高效液相色谱(HPLC)法测定洗脱液,与ELISA法测定结果基本一致.","authors":[{"authorName":"曙照","id":"1a513624-4b52-4a50-8f86-6ebd8a8d0cda","originalAuthorName":"刘曙照"},{"authorName":"韦林洪","id":"c4854249-d3a4-492a-a56f-6d23df833e82","originalAuthorName":"韦林洪"},{"authorName":"徐维娜","id":"fa7222c6-365a-4e81-840e-cf2b7683e251","originalAuthorName":"徐维娜"}],"doi":"10.3321/j.issn:1000-8713.2005.02.004","fpage":"134","id":"6982a5a2-d5c6-45cc-93ae-7a7a4931214a","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"b3c8825e-1214-499b-9ee9-9fc6ef06b297","keyword":"免疫亲和色谱","originalKeyword":"免疫亲和色谱"},{"id":"b6fe4082-3cec-46c2-b1d2-3d22fb2f5837","keyword":"酶联免疫吸附分析","originalKeyword":"酶联免疫吸附分析"},{"id":"b4706bc9-4e38-4fbf-9b94-22d7e5be7e79","keyword":"高效液相色谱","originalKeyword":"高效液相色谱"},{"id":"4e774b05-460c-48f7-bae5-2b58d1900ef6","keyword":"克百","originalKeyword":"克百威"}],"language":"zh","publisherId":"sp200502004","title":"克百的免疫亲和色谱分析研究","volume":"23","year":"2005"},{"abstractinfo":"采用液相色谱-串联质谱法( LC-MS/MS)研究了白菜中涕灭及其代谢物的残留动态行为.按农民常用施药量(3 000 g/hm2)将涕灭沟施予田地后,定期取样检测,并建立其残留行为的数学模型.结果表明,用 LC-MS/MS 测定涕灭及其代谢物,在0. 005~0. 2 mg/L范围内线性关系良好,平均回收率为78. 9%~108. 5%,相对标准偏差为2. 03%~8. 91%( n=8).涕灭在白菜中的浓度升高和降低的过程均符合一级动力学模型( c=0. 020e0. 136t和c=0. 65e-0. 059t ),相关系数( r2 )分别为0. 888和0. 979,半衰期为29. 1天.代谢产物涕灭砜和涕灭亚砜在白菜中的浓度降低时同样符合一级动力学方程( c=23. 4e-0. 044t和 c=4. 54e-0. 027t ),r2 分别为 0. 916 和 0. 972.涕灭、涕灭砜和涕灭亚砜在白菜中的含量要降到国内外限量要求 0. 01 mg/kg,分别需要 70. 7、226. 6 和 176. 3 天.白菜生长周期为120天,收获时涕灭砜和涕灭亚砜含量仍超过国内外限量要求.因此,在本文施药量下,涕灭不能使用.该数据为涕灭的安全使用和农药残留动态行为研究提供了理论依据.","authors":[{"authorName":"丁葵英","id":"84a6b174-5ee6-4fce-b15e-613f0c6358ef","originalAuthorName":"丁葵英"},{"authorName":"许文娟","id":"42487f29-00db-4c0f-89b7-164ae975e337","originalAuthorName":"许文娟"},{"authorName":"李凯","id":"73c85861-9ff9-40b7-86d1-939d70e38faa","originalAuthorName":"李凯"},{"authorName":"郭礼强","id":"4ba21f91-d877-445e-acae-1c3857082fb7","originalAuthorName":"郭礼强"},{"authorName":"孙军","id":"e4fbfa1f-a525-40cb-a85d-81995f3d8667","originalAuthorName":"孙军"}],"doi":"10.3724/SP.J.1123.2015.08018","fpage":"165","id":"a1a1a036-6b5e-46e7-8a79-471c62eb87ec","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"01192dba-f189-43ea-b411-8d70e4b53867","keyword":"液相色谱-串联质谱","originalKeyword":"液相色谱-串联质谱"},{"id":"b397d32a-c75e-4e8b-8216-40b0986ae59a","keyword":"涕灭","originalKeyword":"涕灭威"},{"id":"bb5c162b-1b04-41f3-a26a-8857eb71b816","keyword":"残留","originalKeyword":"残留"},{"id":"d118caa5-827e-4972-a1a8-0d651474746d","keyword":"动力学","originalKeyword":"动力学"},{"id":"55c4303f-c503-4974-8193-1d0916d24e9f","keyword":"数学模型","originalKeyword":"数学模型"}],"language":"zh","publisherId":"sp201602007","title":"液相色谱-串联质谱法研究涕灭及其代谢物在白菜中的动态行为","volume":"34","year":"2016"}],"totalpage":442,"totalrecord":4419}