{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以非织造布(NWF)为支撑材料,以带有催化活性基团的聚合物——磺化聚醚砜(SPES)/聚醚砜(PES)共混物为膜材料,采用浸渍—溶液相转化法制备出具有高孔隙率的SPES/PES/NWF复合催化膜,组装膜反应器,以乙酸和乙醇为原料制备乙酸乙酯.研究显示:在单次贯流模式操作下,反应温度328 K,醇酸摩尔比3.9∶1,停留时间330 s时,乙酸转化率达到75.5％.在循环贯流模式操作下,乙酸的平衡转化率达到91.0％;与渗透汽化耦合后,平衡转化率提高到95.4％.该复合膜催化技术有望为乙酸乙酯和相关酯类的绿色合成提供新的技术支持.","authors":[{"authorName":"<span style=\"color:red\">郭</span><span style=\"color:red\">士</span><span style=\"color:red\">伟</span>","id":"9ab1468d-51a2-4efe-a5d3-652e3bef224f","originalAuthorName":"郭士伟"},{"authorName":"石文英","id":"6e5146d0-51b3-4a75-973a-b43f119c0119","originalAuthorName":"石文英"},{"authorName":"何本桥","id":"9d3af13c-00ee-4046-acb5-0dc6e53ad361","originalAuthorName":"何本桥"},{"authorName":"李建新","id":"f9390867-e56e-4b16-9610-a611a1ce73bd","originalAuthorName":"李建新"},{"authorName":"崔振宇","id":"1fed1a3c-dc6f-44ba-abab-f2b783909169","originalAuthorName":"崔振宇"},{"authorName":"严峰","id":"b3eee37f-e9f0-4321-ad73-28f7b0c22a11","originalAuthorName":"严峰"},{"authorName":"程煜","id":"bbe7e5d0-ea46-44ce-8905-a694df9797a3","originalAuthorName":"程煜"}],"doi":"","fpage":"22","id":"ace3695f-b9f1-4e3b-bee6-d79b28aab1db","issue":"5","journal":{"abbrevTitle":"MKXYJS","coverImgSrc":"journal/img/cover/MKXYJS.jpg","id":"54","issnPpub":"1007-8924","publisherId":"MKXYJS","title":"膜科学与技术   "},"keywords":[{"id":"21d35d39-8602-49cc-8d21-d27a982057d4","keyword":"复合催化膜","originalKeyword":"复合催化膜"},{"id":"217fffc0-ad5f-4386-94ba-3939f3777bca","keyword":"酯化反应","originalKeyword":"酯化反应"},{"id":"e039bdd0-8a56-4c8e-9c38-14aa7837c2f3","keyword":"乙酸乙酯","originalKeyword":"乙酸乙酯"},{"id":"88858062-a639-4a42-aaa6-e3afa194f31b","keyword":"渗透汽化","originalKeyword":"渗透汽化"},{"id":"d27e589a-27b7-4959-b072-34a764c7fe27","keyword":"磺化聚醚砜","originalKeyword":"磺化聚醚砜"}],"language":"zh","publisherId":"mkxyjs201405005","title":"SPES/PES/NWF复合膜催化酯化制备乙酸乙酯","volume":"34","year":"2014"},{"abstractinfo":"内蒙古锡林<span style=\"color:red\">郭</span>勒盟东部金属成矿带是中国重要的黑色金属、有色金属、贵金属成矿带,成矿带岩浆活动频繁,构造活动强烈,具备有利的成矿条件.通过对2个成矿带(东乌旗成矿带、西乌旗成矿带)的地质背景及成矿条件的研究,将东乌旗成矿带分为4个成矿亚带,西鸟旗成矿带分为2个成矿亚带,为下一步的地质找矿工作提供依据.","authors":[{"authorName":"杜继旭","id":"fd584c9e-5605-4769-b01e-db0a7c05ac10","originalAuthorName":"杜继旭"},{"authorName":"潘成林","id":"2d9e2d78-d308-4289-9a42-7a54cc16cd55","originalAuthorName":"潘成林"},{"authorName":"邱金柱","id":"2474a6dc-72af-4a95-9e2f-56448fd73709","originalAuthorName":"邱金柱"},{"authorName":"杨云鹏","id":"1e1d74b3-d31a-49a3-a790-1c80da0a957f","originalAuthorName":"杨云鹏"}],"doi":"10.11792/hj20160807","fpage":"29","id":"500e6a9a-d291-4f67-9d99-2d0225acffb5","issue":"8","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"234ef34d-b332-4ab1-b80d-bb028910cf34","keyword":"成矿带","originalKeyword":"成矿带"},{"id":"8090e080-2ef1-43ff-a166-52884abebb15","keyword":"成矿亚带","originalKeyword":"成矿亚带"},{"id":"214d318d-1c65-4ea5-b498-a4819fa7778c","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"722c1f11-cd69-4dfa-8936-52ad489667aa","keyword":"划分","originalKeyword":"划分"},{"id":"a8343aef-70ac-4a69-a653-fbf9d67b10a2","keyword":"锡林<span style=\"color:red\">郭</span>勒盟东部","originalKeyword":"锡林郭勒盟东部"},{"id":"4cb1d4e4-8634-47ac-9f44-fffea1d483e7","keyword":"内蒙古","originalKeyword":"内蒙古"}],"language":"zh","publisherId":"huangj201608007","title":"内蒙古锡林<span style=\"color:red\">郭</span>勒盟东部金属成矿亚带的划分及其意义","volume":"37","year":"2016"},{"abstractinfo":"建立了反相高效液相色谱法定量分析全血中马钱子碱和<span style=\"color:red\">士</span>的宁含量的方法.该方法应用Oasis R ○MCX固相萃取小柱进行提取、采用XTerraTM RP18色谱柱进行分离.在该条件下马钱子碱和<span style=\"color:red\">士</span>的宁的线性范围为0.05～10 mg/L,最小检出限为0.15 ng.该方法测得马钱子碱和<span style=\"color:red\">士</span>的宁在低、中、高浓度下的回收率均在90%以上,日内、日间精密度均符合方法学要求.该方法灵敏、快速、准确,适用于临床血药浓度监测和法医毒化检验.","authors":[{"authorName":"王朝虹","id":"36d19504-f0f5-41be-8b5c-9b8cb78c19d8","originalAuthorName":"王朝虹"},{"authorName":"果德安","id":"b272dcdb-2876-4f96-ba88-7a99113b387b","originalAuthorName":"果德安"},{"authorName":"胡春华","id":"8b4aa6f0-41f4-441f-be91-80ea07a5c63d","originalAuthorName":"胡春华"}],"doi":"10.3321/j.issn:1000-8713.2003.04.019","fpage":"382","id":"c8d07a7e-297b-4b5e-80fa-44e2ad719708","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"afab0561-882a-4d35-842d-eaa3644d0677","keyword":"固相萃取","originalKeyword":"固相萃取"},{"id":"b7201ec9-67ef-43a1-8fba-5f3e5b55d32b","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"8a0ed3c0-dd9e-4eda-b95e-87135a691096","keyword":"马钱子碱","originalKeyword":"马钱子碱"},{"id":"892fa553-5340-439a-a1ae-371cdd73d272","keyword":"<span style=\"color:red\">士</span>的宁","originalKeyword":"士的宁"}],"language":"zh","publisherId":"sp200304019","title":"反相高效液相色谱法测定全血中马钱子碱和<span style=\"color:red\">士</span>的宁的含量","volume":"21","year":"2003"},{"abstractinfo":"根据电化学原理, 得到高阻值衬层穿透性裂纹的电沉积电流与时间的关系曲线, 利用计算机数据采集及处理系统, 对高阻值衬层进行分析与检测, 由此可以定量确定裂纹的大小, 再通过观测在裂纹处所沉积的金属（或采用电极扫描技术）来确定裂纹的位置及表面形状, 最终可以实现对高阻值衬层的快速无损探伤.","authors":[{"authorName":"<span style=\"color:red\">郭</span>志猛","id":"a59895a1-e4a8-4a35-a331-9748f7c5978a","originalAuthorName":"郭志猛"},{"authorName":"庄奋强","id":"d8cd23d4-33dd-4328-a00d-72b9a514f2fb","originalAuthorName":"庄奋强"},{"authorName":"林涛","id":"b5f727f0-0703-4ff1-b13c-2745dba602f5","originalAuthorName":"林涛"},{"authorName":"吴峰松","id":"ba35ec5c-8dad-4a09-b74d-d7b0570a72b3","originalAuthorName":"吴峰松"},{"authorName":"殷声","id":"646d55f6-70b4-4352-88ac-c1e271dba40a","originalAuthorName":"殷声"}],"categoryName":"|","doi":"","fpage":"124","id":"e5e5e0ed-8166-4f8a-b28e-d665b6d67a6f","issue":"2","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"65638d24-a49c-4c62-bf5d-fc361122209b","keyword":"高阻值衬层","originalKeyword":"高阻值衬层"},{"id":"48e71879-91d1-4f48-953e-71210906e540","keyword":"null","originalKeyword":"null"},{"id":"7b4996f6-ca76-4816-9879-97c3dd341e49","keyword":"null","originalKeyword":"null"},{"id":"4e24337c-4431-4601-96bf-b869291af036","keyword":"null","originalKeyword":"null"}],"language":"zh","publisherId":"0412-1961_1999_2_20","title":"<span style=\"color:red\">郭</span>志猛 庄奋强","volume":"35","year":"1999"},{"abstractinfo":"","authors":[{"authorName":"林卓毅","id":"3382858d-f48a-4578-b506-c18413ee59d5","originalAuthorName":"林卓毅"}],"doi":"10.3969/j.issn.1000-6826.2001.05.016","fpage":"14","id":"32377a54-79b0-4d09-9ca2-fa41568747a2","issue":"5","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"d2ee66c3-e724-46f2-ab0a-be626378b6ed","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj200105016","title":"神秘的大马<span style=\"color:red\">士</span>革钢","volume":"","year":"2001"},{"abstractinfo":"","authors":[],"doi":"","fpage":"49","id":"8f8db74f-74a4-44f5-86ac-394d6e2f2cb8","issue":"1","journal":{"abbrevTitle":"HCCLLHYYY","coverImgSrc":"journal/img/cover/HCCLLHYYY.jpg","id":"42","issnPpub":"1671-5381","publisherId":"HCCLLHYYY","title":"合成材料老化与应用"},"keywords":[{"id":"50c41a4b-e447-4ddd-818c-208cac4b571b","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"hccllhyyy200501020","title":"高性能纳米粘<span style=\"color:red\">士</span>配混料","volume":"34","year":"2005"},{"abstractinfo":"在不锈钢水轮机母材上,用周期反相电镀稀土铬,镀层厚度约0.3 mm,镀层由金属基相和稀土盐颗粒第二相组成,硬度为900Hv～1000 Hv.阳极极化曲线测量表明:镀层的腐蚀阻力为母材的7～8倍.在模拟式小水轮机上考核,镀层的抗磨蚀性为母材的25～28倍,为离子氮化不锈钢的10～12倍.在水电生产中应用,电镀水轮机的工作寿命比原不锈钢高2～6倍.","authors":[{"authorName":"王飚","id":"53753101-c3d1-4061-9957-21f87b10442a","originalAuthorName":"王飚"},{"authorName":"王宇栋","id":"fd6df185-fb5b-445a-8056-58952fb486f9","originalAuthorName":"王宇栋"},{"authorName":"张自华","id":"5ce1efb4-2792-4919-969a-c16a317d4c9e","originalAuthorName":"张自华"}],"doi":"10.3969/j.issn.1005-4537.2003.01.008","fpage":"34","id":"7c2ef714-b0c3-4fca-a95f-d55f5817cc38","issue":"1","journal":{"abbrevTitle":"ZGFSYFHXB","coverImgSrc":"journal/img/cover/中国腐蚀封面19-3期-01.jpg","id":"81","issnPpub":"1005-4537","publisherId":"ZGFSYFHXB","title":"中国腐蚀与防护学报"},"keywords":[{"id":"ff985634-90a6-4591-8452-84c763bc3d87","keyword":"水轮机","originalKeyword":"水轮机"},{"id":"93b0f989-800e-49b3-8503-a34fb7377e3c","keyword":"空蚀磨损","originalKeyword":"空蚀磨损"},{"id":"0b0583c4-3938-4817-9ffa-a3e774c55f77","keyword":"电镀","originalKeyword":"电镀"},{"id":"c7bd30d8-de4d-4a75-9790-50b614639bfe","keyword":"稀土铬","originalKeyword":"稀土铬"}],"language":"zh","publisherId":"zgfsyfhxb200301008","title":"电镀稀<span style=\"color:red\">士</span>铬提高水轮机的抗空蚀磨损能力","volume":"23","year":"2003"},{"abstractinfo":"","authors":[],"doi":"","fpage":"63","id":"7ec0ff1b-2c6c-4f5d-88eb-84b412d83f69","issue":"9","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"88cc7b83-07d7-4474-9fae-1b9e688b5203","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"gfzclkxygc200809040","title":"我刊主编徐僖教授当选英国皇家化学会会<span style=\"color:red\">士</span>","volume":"24","year":"2008"},{"abstractinfo":"利用静态浸泡法通过绘制增重率-时间曲线及采用红外光谱研究了环氧粉末涂层在高温稀氯化钠溶液中抗介质渗透能力.探讨了高温(120℃)下该涂层在蒸馏水及稀氯化钠溶液中 ?传输行为.试验结果表明,交联度小的环氧涂层在氯化钠溶液中的增重率较水中的增重率无明显的变化;而交职大的环氧涂层在氯化钠溶液中的增重率则小于其在水中的增重率.","authors":[{"authorName":"王震宇","id":"498d1bbc-dcc3-4f27-9a85-4bdb7001f522","originalAuthorName":"王震宇"},{"authorName":"李劲","id":"87548394-06e7-426a-ad1c-3c2ff408a36e","originalAuthorName":"李劲"},{"authorName":"柯<span style=\"color:red\">伟</span>","id":"d7069b8c-c06d-455b-8e80-082b683ef832","originalAuthorName":"柯伟"},{"authorName":"张立新","id":"e20751de-889e-4521-84d5-faa69ebae6df","originalAuthorName":"张立新"},{"authorName":"史志明","id":"afc5bef9-a40a-4d54-9359-eaccb4f738f8","originalAuthorName":"史志明"}],"doi":"10.3969/j.issn.0253-4312.2000.08.002","fpage":"5","id":"813b1d9a-e7a3-48f8-8473-1acefdf52408","issue":"8","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"a474adb6-b31f-46d6-86a3-9ed7026773ad","keyword":"环氧树脂","originalKeyword":"环氧树脂"},{"id":"d93aab8b-559f-4377-9743-d563b95dd8a5","keyword":"粉末涂料","originalKeyword":"粉末涂料"},{"id":"62cbbdc5-98f0-4013-b1ea-7a3e5feeedc5","keyword":"介质传输","originalKeyword":"介质传输"},{"id":"06efe6ea-a05f-4a77-973e-0599a981adc2","keyword":"静态浸泡","originalKeyword":"静态浸泡"}],"language":"zh","publisherId":"tlgy200008002","title":"环氧粉末涂层在高温稀氯化钠溶液中介质<span style=\"color:red\">伟</span>输行为研究","volume":"","year":"2000"},{"abstractinfo":"","authors":[],"doi":"","fpage":"3","id":"1a545525-a55b-4008-a34b-14e0c1bc23e8","issue":"3","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"bb2e88db-b3d2-4033-a38a-92e2289ed901","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"gsytb200003001","title":"中国化学家、材料科学家--中科院院士<span style=\"color:red\">郭</span>景坤","volume":"19","year":"2000"}],"totalpage":15,"totalrecord":143}