{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"通过浮石负载壳聚糖制备了吸附剂壳聚糖/浮石复合物,采用扫描电子显微镜(SEM)、热重分析(TGA)、元素分析、傅里叶红外光谱(FT-IR)、X射线衍射(XRD)和X射线荧光光谱(XRF)等技术手段表征了吸附剂性质,考察了吸附剂量、吸附时间、溶液pH值、离子强度和温度对该吸附剂吸附去除水中丙溴磷的影响,研究了再生吸附剂的吸附性能. 结果表明,负载在浮石上的壳聚糖占吸附剂总量的8.69%;在pH值3.0~7.0内,壳聚糖/浮石对丙溴磷的吸附率大于90%;这种吸附剂对丙溴磷的吸附受溶液离子强度影响较小,随温度升高而稍微减小. 在溶液温度25 ℃、pH=7.0、丙溴磷浓度40 mg/L、壳聚糖/浮石剂量为0.7 g/L和吸附平衡时间为90 min条件下,此吸附剂对丙溴磷最大吸附率为93.3%(最大吸附量为53.4 mg/g). 壳聚糖/浮石连续经过3次吸附/再生循环,每次循环对丙溴磷的吸附率下降约12%. 可见壳聚糖/浮石通过吸附可有效地去除水中的农药丙溴磷.","authors":[{"authorName":"彭炳先","id":"e2490ff9-5ff2-448c-9c11-08a6ca3461b9","originalAuthorName":"彭炳先"},{"authorName":"周爱红","id":"7414ba24-8049-4a02-a793-565c62872bdf","originalAuthorName":"周爱红"}],"doi":"10.11944/j.issn.1000-0518.2017.04.160263","fpage":"464","id":"7d9c8f7f-1cc3-41f4-a945-9a8593394169","issue":"4","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"23cf6024-a5b1-4a59-b125-22ecce1e4220","keyword":"丙溴磷","originalKeyword":"丙溴磷"},{"id":"057dfe41-b525-4ce2-ba37-457ceb4f2cf7","keyword":"壳聚糖/浮石","originalKeyword":"壳聚糖/浮石"},{"id":"0e60c4cb-6a7b-45f4-83a4-10e12562b500","keyword":"吸附","originalKeyword":"吸附"},{"id":"ebdb92cf-d432-4bb7-a27a-714c4fa72ec7","keyword":"去除","originalKeyword":"去除"}],"language":"zh","publisherId":"yyhx201704014","title":"浮石负载壳聚糖吸附去除水中丙溴磷","volume":"34","year":"2017"},{"abstractinfo":"报道了一种简便、快速的西红柿、卷心菜中丙溴磷的提取净化及测定方法.采用丙酮-正己烷(体积比为1:1)提取西红柿、卷心菜中的丙溴磷,经活性炭净化后,用气相色谱-火焰光度检测法直接测定其含量.丙溴磷在西红柿、卷心菜中的加标回收率分别为96.2%~105.9%,94.7%~102.3%,RSD分别为3.7%~4.9%,3.7%~5.0%.西红柿、卷心菜中丙溴磷的最低检出限为0.06 mg/kg.","authors":[{"authorName":"陈雁君","id":"11bb4dde-d375-4ba6-b34d-7ebf96d2c64e","originalAuthorName":"陈雁君"},{"authorName":"卢英华","id":"4dde50f6-fe61-4796-b75f-cabf25f758f6","originalAuthorName":"卢英华"},{"authorName":"张娟","id":"7d0efa86-07b4-41ee-8964-5b9e0d11b356","originalAuthorName":"张娟"},{"authorName":"刘君","id":"01e18b4c-9c0a-41bb-a956-a548a848cd45","originalAuthorName":"刘君"},{"authorName":"温新民","id":"fbe12dcd-be41-4a38-a977-c9471805e432","originalAuthorName":"温新民"}],"doi":"10.3321/j.issn:1000-8713.2001.03.029","fpage":"283","id":"00acd22a-3bee-47a8-981c-021075830fac","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"15d8e89d-39f5-4807-aa78-a9e0568fc371","keyword":"气相色谱法-火焰光度检测器","originalKeyword":"气相色谱法-火焰光度检测器"},{"id":"c885f35a-9f5e-4cd0-afb0-f9caba448ee2","keyword":"丙溴磷","originalKeyword":"丙溴磷"},{"id":"2ab09195-5548-4980-a483-8b2326e0cc17","keyword":"残留量","originalKeyword":"残留量"},{"id":"d76a2974-351d-4a86-8ce8-8edf31288f87","keyword":"提取","originalKeyword":"提取"},{"id":"4b8d8a70-4c7b-4abb-9f22-9e97d143dd60","keyword":"西红柿","originalKeyword":"西红柿"},{"id":"901f6798-dd1b-4357-a55b-4ea76d0b373b","keyword":"卷心菜","originalKeyword":"卷心菜"}],"language":"zh","publisherId":"sp200103029","title":"西红柿、卷心菜中残留丙溴磷的提取及气相色谱-火焰光度检测法分析","volume":"19","year":"2001"},{"abstractinfo":"在酸性条件下,溴丙胺太林(PB)分子中N原子被质子化后与阴离子AuCl-4形成离子缔合物,该缔合物被二氯甲烷带入鲁米诺的氯化十六烷基三甲基铵微乳液中,离解出来的AuCl-4立即与鲁米诺产生化学发光. 在一定浓度范围内,发光强度与溴丙胺太林的含量呈线性关系,从而间接测定溴丙胺太林的含量. 在优化的试验条件下,线性范围为0.001~10×10 -6 g/mL,检出限(3σ)为0.04×10 -9 g/mL,对浓度为1×10 -6 g/mL的溴丙胺太林进行11次平行测定,RSD为1.32%.","authors":[{"authorName":"石文兵","id":"1e27b8e3-38bf-4b95-9edc-a2e6f378cc89","originalAuthorName":"石文兵"}],"doi":"10.3969/j.issn.1000-0518.2008.05.018","fpage":"583","id":"f6908e31-20bd-4f28-a095-fa66c3f3da26","issue":"5","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"9683117f-9577-4300-92fb-e970240dde87","keyword":"微乳液","originalKeyword":"微乳液"},{"id":"42f485c4-6b0d-46cf-b934-f656f9420d69","keyword":"溴丙胺太林","originalKeyword":"溴丙胺太林"},{"id":"5713a725-77f2-4f51-b275-38f1c48844e3","keyword":"化学发光","originalKeyword":"化学发光"}],"language":"zh","publisherId":"yyhx200805018","title":"流动注射微乳液化学发光法测定溴丙胺太林","volume":"25","year":"2008"},{"abstractinfo":"溴化四正丙基胺在化学化工方面有着广泛的应用,尤其在合成催化剂时可作为相转移催化剂制备均匀颗粒.本文研究了反应温度、反应时间、不同溶剂对溴化四正丙基胺产率的影响,在80℃反应10 h,以N,N-二甲基甲酰胺做溶剂时,产率最高达到27.50%.红外光谱表明,溴化四正丙基胺需在80℃以下干燥,温度过高会使其分解.","authors":[{"authorName":"王明华","id":"97e1e133-e379-4a2a-bc5b-396a4f4d3a11","originalAuthorName":"王明华"},{"authorName":"黎潮","id":"9f76e086-0f39-4642-9f32-e113c619c129","originalAuthorName":"黎潮"},{"authorName":"王凤栾","id":"dbc915ae-ffb1-4178-a7ff-784f14370dd8","originalAuthorName":"王凤栾"},{"authorName":"宫振宇","id":"5741974e-ceaf-4331-b62a-05e239e1806e","originalAuthorName":"宫振宇"},{"authorName":"翟玉春","id":"8306f664-28d4-4043-835c-b6ffbc869966","originalAuthorName":"翟玉春"}],"doi":"10.3969/j.issn.1671-6620.2011.04.004","fpage":"249","id":"a161e970-e078-4cc0-a7a4-6e050d864c0e","issue":"4","journal":{"abbrevTitle":"CLYYJXB","coverImgSrc":"journal/img/cover/CLYYJXB.jpg","id":"17","issnPpub":"1671-6620","publisherId":"CLYYJXB","title":"材料与冶金学报"},"keywords":[{"id":"0c9a020f-e971-4253-8012-f8b12f617a35","keyword":"溴化四正丙基胺","originalKeyword":"溴化四正丙基胺"},{"id":"4f4200ff-a359-4a80-8fa9-f2336160ef96","keyword":"产率","originalKeyword":"产率"},{"id":"0647453a-ed93-4a04-a722-2fff96a2a1d3","keyword":"红外表征","originalKeyword":"红外表征"}],"language":"zh","publisherId":"clyyjxb201104004","title":"由溴丙烷和三正丙胺合成溴化四正丙基胺","volume":"10","year":"2011"},{"abstractinfo":"采用常规乳液聚合方法,以环氧树脂改性含有磷酸酯功能单体的苯丙乳液来制备水性防锈乳液.苯乙烯(St)、丙烯酸丁酯(BA)等为共聚单体,引入环氧树脂及具有抗闪蚀功能的磷酸酯功能单体,考察了乳化剂、引发剂、环氧树脂、磷酸酯单体不同用量对乳液及其漆膜的影响,并对乳液的粒径、固含量及漆膜的耐盐水性、附着力等性能进行测试,逐步优化聚合工艺来合成具有高效防锈的新型环氧防锈乳液.研究表明,乳化剂用量、引发剂用量、环氧树脂用量、磷酸酯单体用量分别为单体总量的1.5%、0.6%、7%、3%时,可制得性能较好的水性环氧改性含磷苯丙防锈乳液.","authors":[{"authorName":"徐晶","id":"88ec288d-abc7-41d8-b012-53e9e40a8e5d","originalAuthorName":"徐晶"},{"authorName":"刘国军","id":"13a86bd5-36af-49af-a3e9-b5cff8a89791","originalAuthorName":"刘国军"},{"authorName":"刘素花","id":"4037e38e-3575-478a-a34e-ba33b3cd7ac7","originalAuthorName":"刘素花"},{"authorName":"王玉标","id":"872f1c1a-0476-4635-ac13-f5152cb0df2c","originalAuthorName":"王玉标"},{"authorName":"于晓茹","id":"4b8596ae-b0e0-4793-a3b5-bbefb82e3867","originalAuthorName":"于晓茹"},{"authorName":"罗茜","id":"c415f320-6a86-4513-ac33-d740dacbfd46","originalAuthorName":"罗茜"}],"doi":"10.3969/j.issn.0253-4312.2011.03.010","fpage":"42","id":"ef0556b1-1fa7-4d29-85aa-f524c42e1cbb","issue":"3","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"2572b742-c196-4af6-8eb2-98e68d9d19c2","keyword":"防锈乳液","originalKeyword":"防锈乳液"},{"id":"075de0bd-de7b-495d-801e-3c92d8638f91","keyword":"环氧树脂","originalKeyword":"环氧树脂"},{"id":"c079d923-b3af-4d2b-8fed-ff8dc098f9fe","keyword":"磷酸酯功能单体","originalKeyword":"磷酸酯功能单体"},{"id":"4fa3965a-9b94-46fb-9950-f7845b23e093","keyword":"苯丙乳液","originalKeyword":"苯丙乳液"}],"language":"zh","publisherId":"tlgy201103010","title":"环氧改性含磷苯丙防锈乳液的合成","volume":"41","year":"2011"},{"abstractinfo":"研究了新显色剂5,10,15-三(对氯苯基) 20-丙氧苯基卟啉三乙基溴化铵与铜的显色反应.结果表明:在中性介质中,沸水浴加热10min形成1:1的络合物,λmax=417nm,在0~1.2μg/10mL范围内吸光度与铜浓度的关系符合比尔定律,表观摩尔吸光系数ε=3.58×105.该法具有灵敏度高及选择性好的特点,用于水样实际测定,结果满意.","authors":[{"authorName":"霍广进","id":"9b95285b-a252-47db-aad1-4ce053dc80fb","originalAuthorName":"霍广进"},{"authorName":"闫俊英","id":"30da1871-6a39-4ad5-9763-8b1a1f1b6775","originalAuthorName":"闫俊英"},{"authorName":"韩士田","id":"fbfd95e9-29ec-49e2-9fb1-d06dc7c9d8ad","originalAuthorName":"韩士田"}],"doi":"10.3969/j.issn.1000-7571.2000.01.003","fpage":"8","id":"3496b0c0-e053-4485-8e63-98c673045995","issue":"1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"09da96c8-6b6b-485a-b051-e6d126da5389","keyword":"铜","originalKeyword":"铜"},{"id":"0902ccee-50cc-4508-933b-e7b1cfac8ce5","keyword":"分光光度法","originalKeyword":"分光光度法"},{"id":"4dca8f0f-5662-44c8-8b47-20f0fc78ec78","keyword":"5,10,15-三(对氯苯基)20-丙氧苯基卟啉三乙基溴化铵","originalKeyword":"5,10,15-三(对氯苯基)20-丙氧苯基卟啉三乙基溴化铵"}],"language":"zh","publisherId":"yjfx200001003","title":"5,10,15-三(对氯苯基)20-丙氧苯基卟啉三乙基溴化铵显色剂与铜的显色反应","volume":"20","year":"2000"},{"abstractinfo":"2-溴-4-氟苯甲酰肼(1)与芳香醛缩合得到酰腙(2a~2i),再与丙酸酐环反应合成了9种新型的2-芳基-3-N-丙酰基-5-(2-溴-4-氟苯基)-1,3,4-(噁)二唑啉类衍生物(3a~3i),收率79%~84%.化合物的结构经元素分析、IR、1H NMR和MS确证.初步的抗菌试验表明,部分目标化合物表现出较好的抑菌活性.","authors":[{"authorName":"李德江","id":"7837ad5b-aa2e-4270-8a31-1eea3b513866","originalAuthorName":"李德江"},{"authorName":"傅和青","id":"38dfc3f3-382d-4fac-a788-5ba1a01b3511","originalAuthorName":"傅和青"},{"authorName":"葛正鸿","id":"464008a1-d7e0-47d1-acae-5b71886085d5","originalAuthorName":"葛正鸿"}],"doi":"10.3969/j.issn.1000-0518.2006.08.027","fpage":"936","id":"771505ba-d664-47af-abf8-ed5d5a2400ad","issue":"8","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"10e79871-a458-42c8-b27c-9ecd0132b50e","keyword":"(噁)二唑啉衍生物","originalKeyword":"(噁)二唑啉衍生物"},{"id":"171ae0ea-396f-46b5-ae40-6657fd47af46","keyword":"合成","originalKeyword":"合成"},{"id":"f85071c2-56f3-4c45-b824-2ef88bbcd8b0","keyword":"结构表征","originalKeyword":"结构表征"},{"id":"39088fd6-27eb-4080-85eb-1318d78d8da9","keyword":"抑菌活性","originalKeyword":"抑菌活性"}],"language":"zh","publisherId":"yyhx200608027","title":"2-芳基-3-N-丙酰基-5-(2-溴-4-氟苯基)-1,3,4-(噁)二唑啉类衍生物的合成及抗菌活性","volume":"23","year":"2006"},{"abstractinfo":"目的:制备一种新型磷氮类紫外光固化膨胀阻燃涂层,研究磷氮复合成分对阻燃性能及膨胀行为的影响。方法采用丙烯酸正丁酯、甲基丙烯酸甲酯、甲基丙烯酸缩水甘油酯为原料制备环氧侧基聚丙烯酸酯,进一步利用丙烯酸开环环氧制备光固化聚丙烯酸酯,并结合前期所合成的含磷单体磷杂环丙烯酸酯磷酸酯( PGMH)和含氮光固化单体三嗪基四丙烯酸酯( BDAETH)制备光固化膨胀阻燃涂层。通过热重法和红外光谱研究了PGMH对光固化聚丙烯酸酯固化膜热降解机理的影响。采用极限氧指数对涂层阻燃性能进行研究,设计并自制设备对涂层的膨胀行为进行监测。结果随着磷氮复合阻燃剂的添加,涂层在450~480℃之间快速膨胀,其最大单向膨胀度可达14。膨胀碳层隔绝氧气,从而提升阻燃性能,将光固化聚丙烯酸酯的氧指数从19提升到28.5。结论磷氮复合阻燃剂的添加可有效赋予涂层在升温或燃烧过程中的膨胀特性,生成隔绝氧气的膨胀碳层,提高涂层的阻燃性能。","authors":[{"authorName":"卜江","id":"702bf69e-b164-40f0-88a0-48799759005f","originalAuthorName":"卜江"},{"authorName":"梁红波","id":"8ff6af49-9eb5-49c1-9a5e-ba4dacb45148","originalAuthorName":"梁红波"},{"authorName":"刘彦余","id":"65698569-118e-49e8-87fe-e27b16531a3c","originalAuthorName":"刘彦余"},{"authorName":"黄圣梅","id":"1e275cec-f25e-4167-96ae-b1e7d160a434","originalAuthorName":"黄圣梅"},{"authorName":"熊磊","id":"065401a6-a546-4543-8c19-756f05117b57","originalAuthorName":"熊磊"},{"authorName":"徐海涛","id":"97701973-ede6-4f07-8bd3-1771eaff545c","originalAuthorName":"徐海涛"}],"doi":"10.16490/j.cnki.issn.1001-3660.2015.08.010","fpage":"55","id":"d92e43ec-187d-44ed-b224-e880c6e266e8","issue":"8","journal":{"abbrevTitle":"BMJS","coverImgSrc":"journal/img/cover/BMJS.jpg","id":"3","issnPpub":"1001-3660","publisherId":"BMJS","title":"表面技术 "},"keywords":[{"id":"372f53bb-d8e2-4267-8343-a58fd1a460f6","keyword":"光固化","originalKeyword":"光固化"},{"id":"9ecfbf23-0c71-40b5-912e-a2981391d7e9","keyword":"膨胀阻燃涂层","originalKeyword":"膨胀阻燃涂层"},{"id":"97bbcfdd-5f11-4a53-af5c-9df2cc21c1aa","keyword":"膨胀行为","originalKeyword":"膨胀行为"}],"language":"zh","publisherId":"bmjs201508010","title":"磷氮阻燃剂/纯丙树脂光固化复合膨胀阻燃涂层制备及膨胀行为","volume":"","year":"2015"},{"abstractinfo":"研制成硅丙乳胶涂料.介绍了硅丙乳液的合成方法和制漆工艺.比较了硅丙乳胶涂料、苯丙乳胶涂料和纯丙乳胶涂料的性能.讨论了乳化剂、缓冲剂、有机硅种类对硅丙乳液性能的影响.","authors":[{"authorName":"杨慕杰","id":"fac44ec0-cbff-410b-b8e3-f6cf1082e6f6","originalAuthorName":"杨慕杰"},{"authorName":"刘宏伟","id":"0f12c981-0dbb-4829-b67b-f29a96b168be","originalAuthorName":"刘宏伟"},{"authorName":"张火明","id":"61033751-ef7a-45e0-8417-01d9b062743d","originalAuthorName":"张火明"},{"authorName":"陈德铨","id":"3309ac03-1b16-4207-8f3d-f5577c407be9","originalAuthorName":"陈德铨"},{"authorName":"王坚","id":"9a8d9a1c-6a20-4882-b344-98940993ca26","originalAuthorName":"王坚"},{"authorName":"王辰","id":"4d336253-27bc-48c8-bfa1-b36298e2103f","originalAuthorName":"王辰"}],"doi":"10.3969/j.issn.0253-4312.2000.01.004","fpage":"12","id":"9a090fc4-a94f-4550-a19a-fe31bbc7925a","issue":"1","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"4f451c36-497e-4c23-8cae-a56082d8ad9e","keyword":"硅丙乳胶涂料","originalKeyword":"硅丙乳胶涂料"},{"id":"50fd5b05-9027-4b96-ac1e-ae7cc726d86f","keyword":"苯丙乳胶涂料","originalKeyword":"苯丙乳胶涂料"},{"id":"dc89bac4-93fc-4224-a972-853af2661be4","keyword":"纯丙乳胶涂料","originalKeyword":"纯丙乳胶涂料"},{"id":"675e5084-4f2f-4b74-b481-086edd27bbf9","keyword":"建筑涂料","originalKeyword":"建筑涂料"}],"language":"zh","publisherId":"tlgy200001004","title":"硅丙乳胶涂料","volume":"","year":"2000"},{"abstractinfo":"以胶乳法制备了溴化天然橡胶(BNR),研究了溴化工艺条件如平平加O用量、溴化时间、溴浓度和溴化方式对BNR产物溴含量和凝胶含量的影响.结果表明,BNR产物溴含量和凝胶含量随平平加O用量的增加而下降;溴化时间为5min时,BNR产物的溴含量和凝胶含量分别达到14.8%和12.7%;当溴浓度为0.05mol/L时,BNR产物凝胶含量为14.8%,而采用分步溴化的凝胶含量则降至9.2%.BNR产物在甲苯中溶解性能随着凝胶含量降低而增大,凝胶含量小于15.7%的BNR的样品大部分都可溶解.","authors":[{"authorName":"赵法敏","id":"a548deb0-1ebb-478c-934f-af43e8d43243","originalAuthorName":"赵法敏"},{"authorName":"薛行华","id":"5a2e9c0b-18d1-4fb3-af07-9592641f4708","originalAuthorName":"薛行华"},{"authorName":"张子琦","id":"9e003a4a-e66c-4131-adaf-0f3b60181fb6","originalAuthorName":"张子琦"},{"authorName":"张利伟","id":"2aede402-215f-4beb-a7f0-573b7742127b","originalAuthorName":"张利伟"},{"authorName":"李光","id":"5e45d295-961b-4f14-8da2-bc9fffe6414e","originalAuthorName":"李光"}],"doi":"","fpage":"113","id":"934b300f-1734-4423-bc36-cdfc540f2a19","issue":"8","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"c3984fe8-2d38-47f5-b3b9-564414bc5a8a","keyword":"溴化天然橡胶","originalKeyword":"溴化天然橡胶"},{"id":"f0b2783a-8087-419c-9f64-ab4de7d7a856","keyword":"胶乳法","originalKeyword":"胶乳法"},{"id":"6446fb86-fd47-4872-aee1-cebd297a529d","keyword":"溴化工艺","originalKeyword":"溴化工艺"},{"id":"b6537bbc-411d-405e-b673-bc2829de63d7","keyword":"凝胶含量","originalKeyword":"凝胶含量"},{"id":"6c183f9d-59d2-4fa0-b599-2f4e9dcdc913","keyword":"溶解性能","originalKeyword":"溶解性能"}],"language":"zh","publisherId":"gfzclkxygc201308028","title":"溴化工艺对溴化天然胶乳结构与溶解性的影响","volume":"29","year":"2013"}],"totalpage":538,"totalrecord":5371}