{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"介绍了电镀<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>的原理,给出了分别适用于钢铁及黄铜基体的工艺流程及配方,阐述了<span style=\"color:red\">镀</span>液中各组分的作用,描述了常见故障(如镀层出现条纹、起皮、粗糙等)的产生原因及其解决方法,指出了操作过程中应注意的问题.","authors":[{"authorName":"程沪生","id":"557f1c21-bcda-446b-9c60-e1f45d5d13d3","originalAuthorName":"程沪生"}],"doi":"","fpage":"11","id":"aa5ae3ec-7f19-4e84-be52-9ae05974eeff","issue":"11","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"c821eaf1-09d1-4993-a81e-e4d68cd1fa53","keyword":"钢铁","originalKeyword":"钢铁"},{"id":"f17ccd58-370f-472e-a44a-30820fb2122d","keyword":"黄铜","originalKeyword":"黄铜"},{"id":"7e930488-bd1b-4c70-97ba-6ce1af575a6b","keyword":"<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>","originalKeyword":"镀黑镍"},{"id":"7597800a-a51d-43a5-87bd-b4a9d515053f","keyword":"配方","originalKeyword":"配方"},{"id":"4f458349-0489-4719-b44c-f9a94fb65e5a","keyword":"故障排除","originalKeyword":"故障排除"}],"language":"zh","publisherId":"ddyts200811004","title":"<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>工艺及其故障排除","volume":"","year":"2008"},{"abstractinfo":"","authors":[{"authorName":"张振赟","id":"f7778de3-5955-403b-8d1e-039b3a59d2b9","originalAuthorName":"张振赟"}],"doi":"10.3969/j.issn.1001-1560.2001.02.027","fpage":"52","id":"c65b18f9-1d76-4dfc-a37a-18291217158c","issue":"2","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"b6543cf9-aa85-4369-8f0d-2895d189becd","keyword":"电镀","originalKeyword":"电镀"},{"id":"41d72a8f-b6aa-4fcd-92c6-f73337a04f7e","keyword":"铝合金","originalKeyword":"铝合金"},{"id":"07316636-bd3c-4f3b-9f4e-b1eae78fbd99","keyword":"<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>","originalKeyword":"镀黑镍"}],"language":"zh","publisherId":"clbh200102027","title":"铝及铝合金<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>工艺控制","volume":"34","year":"2001"},{"abstractinfo":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液是<span style=\"color:red\">镀</span><span style=\"color:red\">镍</span>工序中常用的一种工序,它的电镀效果较好.但是其<span style=\"color:red\">镀</span>液的分析方法却很复杂,且鲜有资料系统地提出其详细的分析资料.现提供一种<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液中主要成分硫酸<span style=\"color:red\">镍</span>、硫酸锌、硫酸<span style=\"color:red\">镍</span>铵、硫氰酸铵及硼酸的分析方法,以供大家参考.","authors":[{"authorName":"李成虹","id":"8926fac8-ee2b-4840-8732-566bdb97fabf","originalAuthorName":"李成虹"}],"doi":"10.3969/j.issn.1001-3849.2004.03.010","fpage":"36","id":"606be320-1656-4b19-9938-ddccd4ce64ab","issue":"3","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰   "},"keywords":[{"id":"007c5658-fe97-4ba2-8e30-9a28cc34a338","keyword":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液","originalKeyword":"黑镍镀液"},{"id":"ba977eeb-6b75-44d8-abb7-fbcda3f90727","keyword":"硫酸<span style=\"color:red\">镍</span>","originalKeyword":"硫酸镍"},{"id":"535d3590-ad00-4fd8-b886-101b5f7cd91c","keyword":"硫酸锌","originalKeyword":"硫酸锌"},{"id":"b7d7f0a8-cc4e-4832-a731-58164af44dfd","keyword":"硫酸<span style=\"color:red\">镍</span>铵","originalKeyword":"硫酸镍铵"},{"id":"b2cfe5a3-6680-4f73-aeb0-6c8454f4dc58","keyword":"硫氰酸铵","originalKeyword":"硫氰酸铵"},{"id":"29982d74-03dc-4915-b1d3-ebf61ed57f36","keyword":"硼酸","originalKeyword":"硼酸"}],"language":"zh","publisherId":"ddjs200403010","title":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液的分析","volume":"26","year":"2004"},{"abstractinfo":"介绍了一种<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液中氯化<span style=\"color:red\">镍</span>、氯化锌和硫氰酸钾含量的快速分析方法:用分光光度法测定氯化<span style=\"color:red\">镍</span>和硫氰酸钾的含量;用标准EDTA溶液滴定法测定<span style=\"color:red\">镍</span>锌总量;氯化锌的含量则由<span style=\"color:red\">镍</span>锌总量扣除<span style=\"color:red\">镍</span>的含量后获得.该方法的回收率高(NiCl295.0%,KSCN 96.8%,ZnCl292.9%),操作简便,快速、准确.","authors":[{"authorName":"张春艳","id":"a354b942-a13c-4c8d-a204-936bad92939e","originalAuthorName":"张春艳"}],"doi":"","fpage":"44","id":"159fa521-5e04-4dcb-8cb9-1d2e61d1e21f","issue":"10","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"4e7c1769-68b3-4032-a630-ad4e81ec15cb","keyword":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液","originalKeyword":"黑镍镀液"},{"id":"a49e180e-c446-42ce-b7c0-4aa72ba91aeb","keyword":"<span style=\"color:red\">镍</span>","originalKeyword":"镍"},{"id":"45d94a38-7e1e-46b0-92e5-3fb95b2d7272","keyword":"锌","originalKeyword":"锌"},{"id":"db84af06-d1ce-4bcb-a10d-74598d137a48","keyword":"硫氰酸钾","originalKeyword":"硫氰酸钾"},{"id":"85e7a728-5e6e-47d0-918a-c65ac27576bd","keyword":"测定","originalKeyword":"测定"}],"language":"zh","publisherId":"ddyts201010012","title":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液中<span style=\"color:red\">镍</span>(Ⅱ)、锌(Ⅱ)及硫氰酸钾的快速分析","volume":"29","year":"2010"},{"abstractinfo":"针对具有特殊要求的<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>零件,对其前处理、<span style=\"color:red\">镀</span>光亮<span style=\"color:red\">镍</span>、闪<span style=\"color:red\">镀</span><span style=\"color:red\">镍</span>等工艺做了较详细的实验研究,确定了最佳工艺流程和工艺范围,获得了外观乌黑光亮及防变色能力、结合力和耐蚀性优良的镀层,满足了大生产需要和零件对镀层的特殊要求.","authors":[{"authorName":"任雅勋","id":"3c26f142-deee-48f9-8f6b-cc838b22874f","originalAuthorName":"任雅勋"}],"doi":"10.3969/j.issn.1001-3849.2007.02.010","fpage":"34","id":"e086323d-1ea3-4a4e-9441-1dc3c5709f9a","issue":"2","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰   "},"keywords":[{"id":"741bc6c4-0427-4313-a77b-803676f59705","keyword":"青铜","originalKeyword":"青铜"},{"id":"61619b92-95d3-436e-a6b1-52628554cb38","keyword":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>","originalKeyword":"黑镍"},{"id":"10029408-4a35-40ae-87bd-222b8e3467ca","keyword":"结合力","originalKeyword":"结合力"}],"language":"zh","publisherId":"ddjs200702010","title":"青铜薄片状零件<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>工艺探析","volume":"29","year":"2007"},{"abstractinfo":"以硝酸银标准溶液作为滴定剂,用电位滴定法测定<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>溶液中的硫氰酸铵的质量浓度,本方法回收率为97.81%～100.54%,相对标准偏差为0.14%,该方法自动控制滴定过程,判断测定终点,结果准确、重现性好.","authors":[{"authorName":"马春华","id":"75db9d6b-d719-48f0-abff-bc59f2e04459","originalAuthorName":"马春华"}],"doi":"10.3969/j.issn.1001-3849.2008.12.012","fpage":"41","id":"e75e51c0-87a1-4f3b-92f5-743a8754ab6f","issue":"12","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰   "},"keywords":[{"id":"1ebf3032-d19f-4dc6-82fa-43c8377f15f5","keyword":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>","originalKeyword":"黑镍"},{"id":"5e9c92af-ec55-4a6e-9814-5cae2cc6fd14","keyword":"NH4CNS","originalKeyword":"NH4CNS"},{"id":"f17022c3-8d7c-410f-82f0-31d3a9c45b33","keyword":"电位滴定","originalKeyword":"电位滴定"}],"language":"zh","publisherId":"ddjs200812012","title":"电位滴定法测定<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>溶液中硫氰酸铵","volume":"30","year":"2008"},{"abstractinfo":"利用重铬酸钾氧化硫氰酸钾的反应,测定铬(Ⅲ)的吸光度,以求得硫氰酸钾含量,实验结果表明,在硫酸介质中显色体系最大吸收波长位于595 nm处,硫氰酸钾的质量浓度介于0～1.8 mg/mL遵守比尔定律,应用于<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液中硫氰酸钾的测定,方法简便快捷,分析的准确度和精密度能满足实际生产要求.","authors":[{"authorName":"丘山","id":"46334706-8479-4815-a351-56343224c8fc","originalAuthorName":"丘山"},{"authorName":"丘星初","id":"c1b906eb-1f4c-428b-8c57-c5bf9adee766","originalAuthorName":"丘星初"},{"authorName":"黄曙明","id":"2e5adcfc-2ea2-4020-a062-0404fe1ab9e5","originalAuthorName":"黄曙明"}],"doi":"10.3969/j.issn.1001-3849.2004.04.012","fpage":"38","id":"59c7e42c-7def-4fec-90ea-917284ff63d3","issue":"4","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰   "},"keywords":[{"id":"1b3c2493-183a-425c-936b-88d1a0149be9","keyword":"硫氰酸钾","originalKeyword":"硫氰酸钾"},{"id":"0a4f025f-d9f9-44c0-aba3-8c746a5d1b98","keyword":"光度法","originalKeyword":"光度法"},{"id":"5f43498a-80c1-4ee5-a283-5c57006ff4f2","keyword":"重铬酸钾","originalKeyword":"重铬酸钾"},{"id":"209cc5a4-a989-456e-bd9e-d1fec01ca732","keyword":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液","originalKeyword":"黑镍镀液"}],"language":"zh","publisherId":"ddjs200404012","title":"光度法快速测定<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液中的硫氰酸钾","volume":"26","year":"2004"},{"abstractinfo":"硫氰酸钾是<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液的重要成分之一,其含量高低直接影响镀层质量.为了检测硫氰酸钾含量是否在最佳的范围内,采用硫酸铁铵作显色剂,用分光光度法测定其含量.结果表明,硫氰酸钾含量介于0～20靏/mL遵守比尔定律,方法简便易行,分析结果的准确度和精密度完全能满足生产实际的要求.","authors":[{"authorName":"丘山","id":"97970ead-79ba-4632-9fea-ff57506b52bc","originalAuthorName":"丘山"},{"authorName":"丘星初","id":"4c30c375-dfc0-4ca7-9d3a-ea4291c0b6ee","originalAuthorName":"丘星初"},{"authorName":"黄曙明","id":"614896cc-fe03-4f5f-916d-589a1239b676","originalAuthorName":"黄曙明"}],"doi":"10.3969/j.issn.1001-1560.2004.10.022","fpage":"57","id":"c150af66-462e-447c-9b22-bea1f7beb00e","issue":"10","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"eb83aace-a54f-4119-ba1f-b74746d9cbc7","keyword":"硫氰酸钾测定","originalKeyword":"硫氰酸钾测定"},{"id":"dc2a1bdb-468e-4713-9232-1b92b42515c9","keyword":"光度法","originalKeyword":"光度法"},{"id":"362ac514-fa73-4296-979b-016051402764","keyword":"硫酸铁铵","originalKeyword":"硫酸铁铵"},{"id":"86bd0ee3-0029-4de0-afaf-7a5fe7b04fe8","keyword":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液","originalKeyword":"黑镍镀液"}],"language":"zh","publisherId":"clbh200410022","title":"<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span><span style=\"color:red\">镀</span>液中硫氰酸钾的快速测定","volume":"37","year":"2004"},{"abstractinfo":"介绍了一种<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span>铬工艺.阐述了<span style=\"color:red\">镀</span>液中各成分的作用及<span style=\"color:red\">镀</span>液的维护,分析了常见故障的原因并提出了解决方法.","authors":[{"authorName":"李贤成","id":"4df98576-673d-47cc-900d-ce9382ddba96","originalAuthorName":"李贤成"}],"doi":"10.3969/j.issn.1004-227X.2002.05.015","fpage":"51","id":"eabbe456-099e-4edd-950d-a71c42dc3e28","issue":"5","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"f7bd7577-81a8-40b8-8dbc-290686c0f486","keyword":"<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span>铬","originalKeyword":"镀黑铬"}],"language":"zh","publisherId":"ddyts200205015","title":"实用<span style=\"color:red\">镀</span><span style=\"color:red\">黑</span>铬工艺","volume":"21","year":"2002"},{"abstractinfo":"采用直流电沉积技术在改性的Watt<span style=\"color:red\">镀</span><span style=\"color:red\">镍</span>溶液中获得了纳米晶<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>薄膜, 采用SEM和XRD对薄膜的表面形貌和相组成进行了表征, 采用循环伏安法和电化学阻抗谱对<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>薄膜的初始电沉积行为进行了研究. 结果表明, <span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>薄膜表面平整光亮, 具有纳米晶结构; <span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>薄膜的电沉积过程遵循3D成核/生长机制; 随着阴极沉积电势(负偏压)的增大, 黄铜电极表面Ni的电沉积反应\\linebreak 由UPD沉积、异质成核/生长转化为最终的同质成核/生长, 相应的电荷转移电阻<em>R</em><sub>t</sub>的值先增大然后减小; 在较高的阴极沉积电势作用下, 由于吸附H原子(H<sub>2</sub>分子)的结晶阻止作用和(<span style=\"color:red\">镍</span>)羟基化合物的吸附作用, 电沉积EIS图出现低频和超低频感抗弧.","authors":[{"authorName":"宋利晓张昭张鉴清曹楚南","id":"dcbb1cff-b8e1-406a-a782-3528dd0c5db7","originalAuthorName":"宋利晓张昭张鉴清曹楚南"}],"categoryName":"|","doi":"10.3724/SP.J.1037.2010.00268","fpage":"123","id":"c6e144ef-4aae-4978-a810-bbe3328f47ed","issue":"1","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"004e3085-a623-41dc-9c8c-15b4d597366e","keyword":"纳米晶<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>薄膜","originalKeyword":"纳米晶黑镍薄膜"},{"id":"ba68ad26-bb90-43f0-9d28-857715878851","keyword":"electroplating","originalKeyword":"electroplating"},{"id":"21724101-b723-4be5-8ae3-768b07b299cf","keyword":"cyclic voltammetry","originalKeyword":"cyclic voltammetry"},{"id":"680bd4f7-9c4b-49d5-b968-66ecaae042a2","keyword":"electrochemical impedance spectroscopy","originalKeyword":"electrochemical impedance spectroscopy"}],"language":"zh","publisherId":"0412-1961_2011_1_5","title":"纳米结构<span style=\"color:red\">黑</span><span style=\"color:red\">镍</span>薄膜的电沉积机理","volume":"47","year":"2011"}],"totalpage":1136,"totalrecord":11355}