{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>法制备了CeO2纳米晶.XRD分析表明,所合成的CeO2纳米晶属于立方晶系.TEM分析表明,CeO2纳米粒子呈球形,粒度随焙烧温度的增加而增大.热失重分析表明,样品的热失重主要受温度的影响,而焙烧时间的影响不大.相对密度分析表明,随CeO2纳米晶粒度的增大,粉末的密度略有增加.","authors":[{"authorName":"盖广清","id":"25016c3f-c926-4b48-a75c-d7d3a7005643","originalAuthorName":"盖广清"},{"authorName":"董相廷","id":"dac174a2-82aa-400e-abf6-078149c2cc74","originalAuthorName":"董相廷"},{"authorName":"王进贤","id":"0f1b8dc4-e31a-41bd-a6d5-6883dcf8db85","originalAuthorName":"王进贤"},{"authorName":"李天乐","id":"0a642c7f-dff9-40be-94fe-857c09445b52","originalAuthorName":"李天乐"},{"authorName":"徐淑芝","id":"36b06ba0-e8c4-4bf1-8167-88e0ab943713","originalAuthorName":"徐淑芝"}],"doi":"","fpage":"437","id":"6d10085d-b78e-4df8-b7f4-a0b7ea6f8e57","issue":"z3","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"ecdabd73-6e93-42f2-8d09-eeb5d559a139","keyword":"铈","originalKeyword":"铈"},{"id":"7d2c1b98-dbd4-48d8-8a73-c0c0740526b1","keyword":"二氧化铈","originalKeyword":"二氧化铈"},{"id":"c1fa48af-470c-4de1-a7bd-a13a383d7ea3","keyword":"纳米晶","originalKeyword":"纳米晶"},{"id":"1a1d2de4-651d-42ea-b0aa-8c33a2a2003e","keyword":"纳米粒子","originalKeyword":"纳米粒子"},{"id":"ff17b5d2-c636-4891-8241-1e24a1e8dbe5","keyword":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>","originalKeyword":"室温固相反应法"}],"language":"zh","publisherId":"xyjsclygc2007z3104","title":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>法制备CeO2纳米晶","volume":"36","year":"2007"},{"abstractinfo":"以Mn(CH3COO)2·4H2O,Ni(CH3COO)2·4H2O,Co(CH3COO)2·4H2O和H2C2O4·2H2O为原料,采用<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>法制备出镍锰钴草酸盐前驱体,将该前驱体在850℃煅烧2 h得到尖晶石相Ni0 66Mn2.34xCoxO4(x=0.15,0.30,0.45,0.60)超细粉体.用XRD,TGA,SEM,沉降式粒度分析仪和热膨胀仪对镍锰钴草酸盐前驱体与Ni0.66Mn2.34-xCoxO4(x=0.15,0.30,0.45,0.60)超细粉体进行了表征.结果表明,由<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>得到的草酸盐前驱体是单相的镍锰钴复合草酸盐:在850℃煅烧2 h得到镍锰钴氧化物为纯尖晶石相,粉体颗粒为球形,团聚较少,粒径均匀,平均粒径约为0.2μm,有较好的烧结活性,是制备热敏陶瓷材料的理想粉体.","authors":[{"authorName":"朱运兵","id":"00d3aa77-5450-491d-a2f2-1c6508f73ce6","originalAuthorName":"朱运兵"},{"authorName":"方道来","id":"ea1a4f96-a746-4282-b28d-a8104ed37bf9","originalAuthorName":"方道来"},{"authorName":"王忠兵","id":"cf6f3620-5fea-49cc-b531-0fc697e93fa5","originalAuthorName":"王忠兵"},{"authorName":"杨萍华","id":"88e39ab5-b120-4b10-a09d-d08e66cfe307","originalAuthorName":"杨萍华"},{"authorName":"陈初升","id":"49301aea-74d5-46e0-bf29-d65ba58b2108","originalAuthorName":"陈初升"}],"doi":"","fpage":"724","id":"e101b404-49f0-4482-8928-09bde5f1643b","issue":"z2","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"1e0f30bc-4d9c-4911-b756-b46340d580f0","keyword":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>","originalKeyword":"室温固相反应法"},{"id":"28b98c18-b2d2-4ee1-94e5-40c831d7e649","keyword":"NTC","originalKeyword":"NTC"},{"id":"a4e64234-67e9-422e-b0b3-5a5972b37f9d","keyword":"热敏电阻","originalKeyword":"热敏电阻"},{"id":"9ad2ece3-e1ef-4412-80b0-0169f3ee3454","keyword":"超细粉体","originalKeyword":"超细粉体"}],"language":"zh","publisherId":"xyjsclygc2005z2029","title":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>法制备Ni0.66Mn2.34-xCoxO4(x=0.15,0.30,0.45,0.60)负温度系数热敏电阻","volume":"34","year":"2005"},{"abstractinfo":"以七水硫酸锌（ZnSO4.7H2O）和碳酸氢铵（NH4HCO3）为原料,以聚乙二醇-400（PEG-400）为模板,通过<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>制备了碳酸锌（ZnCO3）和碱式碳酸锌（ZnCO3.3Zn（OH）2.H2O,basic zinc carbon-ate,BZC）。通过XRD测试及其半定量成分分析,研究了PEG-400剂量和NH4HCO3与ZnSO4.7H2O摩尔比x值对合成产物物相的影响。总结了PEG-400模板辅助合成ZnCO3和BZC的<span style=\"color:red\">反应</span>机制。结果表明,PEG-400包覆ZnSO4.7H2O颗粒形成模板,模板层的厚度影响<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>的微观机制———薄层单向扩散与厚层互扩散,局部微环境的酸碱性决定着产物物相,酸性抑制ZnCO3水解,碱性促进ZnCO3水解生成BZC。由据此设计的较高x值（x=3.0）、较低PEG-400剂量（70μL）的合成工艺,制备了单相BZC粉体。","authors":[{"authorName":"刘长友","id":"03e4a4c0-9206-4704-9447-3b77525559f6","originalAuthorName":"刘长友"},{"authorName":"介万奇","id":"34b58d9c-345a-4f56-bde6-64d6d3d0df0b","originalAuthorName":"介万奇"},{"authorName":"王涛","id":"514e0842-24eb-47a1-ac65-2700baab4c52","originalAuthorName":"王涛"},{"authorName":"查钢强","id":"3a85cd1d-6949-4688-817e-09556cf4d3a0","originalAuthorName":"查钢强"},{"authorName":"谷智","id":"7a7b7581-2f52-4519-8e06-c7e36fe8b604","originalAuthorName":"谷智"},{"authorName":"孙晓燕","id":"41ee83fa-266c-4abc-b950-fddde0b3b2f5","originalAuthorName":"孙晓燕"}],"doi":"","fpage":"537","id":"7a2cd20e-8aa1-4e41-8765-a13b079dba33","issue":"4","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"ff4d5589-f540-422e-856e-34555de035b5","keyword":"碳酸锌","originalKeyword":"碳酸锌"},{"id":"0902b3af-4fde-4b02-be04-fe95d463c33c","keyword":"碱式碳酸锌","originalKeyword":"碱式碳酸锌"},{"id":"485a9e37-86f6-4854-8656-2381e1807d7c","keyword":"<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>","originalKeyword":"固相反应"},{"id":"466470b5-c5df-4298-a74a-6b462e50966f","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"gncl201204034","title":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>合成碱式碳酸锌","volume":"43","year":"2012"},{"abstractinfo":"以Y(NO3)3·6H2O和Fe(NO3)3·9H2O为原料,分别与NaOH和C6H8O7·H2O经<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>合成了粒径分布为20～40 nm的YIG纳米粉体.采用XRD和TEM对粉体产物的晶体结构、形貌、粒径进行了表征,并用该粉体制备了YIG多晶铁氧体,讨论了烧结温度对YIG铁氧体显微结构和磁性能的影响.结果表明:选取柠檬酸为原料其YIG结晶化温度比以NaOH为原料低了接近100 ℃;在1320 ℃烧结3 h可得到显微结构均匀致密的YIG铁氧体,其饱和磁化强度受烧结温度影响很小,基本上在170 mT左右.","authors":[{"authorName":"曾丽文","id":"19811e56-8cde-464a-ae41-9c47bfed4c47","originalAuthorName":"曾丽文"},{"authorName":"徐光亮","id":"1b028452-6a85-4d25-8310-66ced6894766","originalAuthorName":"徐光亮"},{"authorName":"刘桂香","id":"f532e8f1-30d7-4bca-ab5d-abfdb218137f","originalAuthorName":"刘桂香"},{"authorName":"余洪滔","id":"372cab33-bf1c-402c-ac2f-491e6428e173","originalAuthorName":"余洪滔"},{"authorName":"卢超","id":"eed23e44-c59a-4fab-b052-0da5cfd31998","originalAuthorName":"卢超"},{"authorName":"马拥军","id":"2b1f21e6-7e70-49b2-9641-65b606db9ad3","originalAuthorName":"马拥军"}],"doi":"","fpage":"1434","id":"7add14ed-8052-48c9-8009-e34bed2b1737","issue":"6","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"391687de-cf4d-4ac2-bd03-7669589e3f93","keyword":"YIG","originalKeyword":"YIG"},{"id":"b1f34c0b-82d7-4b6d-ba6a-023561164b5d","keyword":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>","originalKeyword":"室温固相反应"},{"id":"a1f22602-130e-4e54-99b4-dee9f599d6fc","keyword":"纳米粉体","originalKeyword":"纳米粉体"},{"id":"0d40b979-3d20-4199-88fe-ac8b4f6397eb","keyword":"磁性能","originalKeyword":"磁性能"}],"language":"zh","publisherId":"rgjtxb98201006017","title":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>法制备YIG纳米粉体","volume":"39","year":"2010"},{"abstractinfo":"以ZnO、Al(OH)3为原料,采用<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>合成了锌铝尖晶石粉体,研究了<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>温度、保温时间对粉体的相组成和显微结构的影响.并运用热分析、X射线衍射以及扫描电子显微镜等分析测试方法对制备的锌铝尖晶石粉体进行了表征.热分析显示,Al(OH)3的分解是分两步完成的；当<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>温度为800℃时,开始有锌铝尖晶石生成；适当延长保温时间有助于锌铝尖晶石生成.<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>合成锌铝尖晶石的最佳工艺条件为1400℃×3 h.合成的锌铝尖晶石粉体晶形发育完整,平均粒径为15 μm左右.","authors":[{"authorName":"许川","id":"62b1a4cc-8f2e-4fbe-a63a-cd75d67b72a3","originalAuthorName":"许川"},{"authorName":"马爱琼","id":"58488b18-9946-452b-99e9-9aa885e4c610","originalAuthorName":"马爱琼"},{"authorName":"刘民生","id":"2b7619b9-9012-4349-b9e7-14f83330aced","originalAuthorName":"刘民生"},{"authorName":"高云琴","id":"09f59d17-4eee-4ca7-97b8-8880f6991cc3","originalAuthorName":"高云琴"}],"doi":"","fpage":"455","id":"5a39c515-4240-4b97-a22a-173f58b7eee9","issue":"2","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"cdf39d02-9110-4464-8ec1-648315c110a0","keyword":"锌铝尖晶石","originalKeyword":"锌铝尖晶石"},{"id":"b635cee5-3b45-4945-a649-4da0f23030e8","keyword":"<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>","originalKeyword":"固相反应"},{"id":"d6edc9a0-1358-42ba-aed6-445c60bba3ac","keyword":"热分析","originalKeyword":"热分析"},{"id":"2fad0fe5-05c6-433e-b971-3005c8b261c1","keyword":"工艺","originalKeyword":"工艺"}],"language":"zh","publisherId":"gsytb201202047","title":"<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>合成锌铝尖晶石","volume":"31","year":"2012"},{"abstractinfo":"以六方氮化硼和炭黑(或石墨)为原料, 采用<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>合成了碳化硼粉体. 碳源、<span style=\"color:red\">反应</span>气氛和温度对粉体合成产生重要影响. 以炭黑为碳源, 在1900℃真空下保温5 h, 得到了平均粒径约为100 nm的碳化硼纳米粉体. 与商业粉体相比, 合成的粉体具有较好的烧结活性. 在2000℃/30 MPa/1 h条件下烧结, 样品的相对密度达到97.9%(商业粉体样品为93.1%), 这可归结于合成的粉体具有细小的粒径、低的氧含量和一定程度的孪晶结构.","authors":[{"authorName":"曾洪","id":"8f0aaa54-4b69-46a0-9c92-5b25b05164eb","originalAuthorName":"曾洪"},{"authorName":"阚艳梅","id":"a84e1b2d-c6ac-4506-94b3-6e4899e0369c","originalAuthorName":"阚艳梅"},{"authorName":"徐常明","id":"9e04450b-980e-47dd-9fdc-d0081c458e8e","originalAuthorName":"徐常明"},{"authorName":"王佩玲","id":"e295579f-70df-4db9-9dd0-2a467fed771d","originalAuthorName":"王佩玲"},{"authorName":"张国军","id":"fb7853fb-06d0-46d7-8ef8-1908d058cdad","originalAuthorName":"张国军"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2011.01101","fpage":"1101","id":"116f67a7-af5c-4dad-8dcd-f9ba920235d6","issue":"10","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"e633f0ec-e2a6-4a53-acea-3f160cb634e4","keyword":"碳化硼","originalKeyword":"碳化硼"},{"id":"c6a27004-3cb3-45f3-b4b0-66b51a5b9e3b","keyword":" boron nitride","originalKeyword":" boron nitride"},{"id":"5a7fb5ab-5c17-43a7-9702-14eaa798062c","keyword":" carbon black","originalKeyword":" carbon black"},{"id":"728c0847-48f8-4d07-b9e0-5143fdb4b9c3","keyword":" nano powder","originalKeyword":" nano powder"}],"language":"zh","publisherId":"1000-324X_2011_10_12","title":"<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>合成碳化硼纳米粉体","volume":"26","year":"2011"},{"abstractinfo":"以六方氮化硼和炭黑(或石墨)为原料,采用<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>合成了碳化硼粉体.碳源、<span style=\"color:red\">反应</span>气氛和温度对粉体合成产生重要影响.以炭黑为碳源,在1900℃真空下保温5h,得到了平均粒径约为100 nm的碳化硼纳米粉体.与商业粉体相比,合成的粉体具有较好的烧结活性.在2000℃/30 MPa/1 h条件下烧结,样品的相对密度达到97.9％(商业粉体样品为93.1％),这可归结于合成的粉体具有细小的粒径、低的氧含量和一定程度的孪晶结构.","authors":[{"authorName":"曾洪","id":"637501b1-3139-428b-811d-7c2937ba87a1","originalAuthorName":"曾洪"},{"authorName":"阚艳梅","id":"ed55d5f1-e166-47c1-b2f6-6c8fb1cb8023","originalAuthorName":"阚艳梅"},{"authorName":"徐常明","id":"04881147-579d-4cb9-ae4b-f19b209f4ade","originalAuthorName":"徐常明"},{"authorName":"王佩玲","id":"fa8b5bc0-4dcb-44dd-bbe0-19f2cc7523fb","originalAuthorName":"王佩玲"},{"authorName":"张国军","id":"fa066167-5bbf-4843-a9ba-8317eb6b886f","originalAuthorName":"张国军"}],"doi":"10.3724/SP.J.1077.2011.01101","fpage":"1101","id":"6d7ebd53-4353-4a8b-beab-25774c24ba9b","issue":"10","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"53373754-b8d8-45c7-b484-abba935083df","keyword":"碳化硼","originalKeyword":"碳化硼"},{"id":"d6e4c74b-d551-4850-b54a-89f352bca77f","keyword":"氮化硼","originalKeyword":"氮化硼"},{"id":"145d2bfb-5ef0-476d-93ad-46ce0434d49e","keyword":"炭黑","originalKeyword":"炭黑"},{"id":"cd392d97-a82a-49d2-9444-b087a7eb9f49","keyword":"纳米粉体","originalKeyword":"纳米粉体"}],"language":"zh","publisherId":"wjclxb201110017","title":"<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span><span style=\"color:red\">法</span>合成碳化硼纳米粉体","volume":"26","year":"2011"},{"abstractinfo":"以ZrOCl2·8H2O和NH4HCO3为原料, 在适量表面活性剂(PEG-400)存在下, 先在<span style=\"color:red\">室温</span>下充分混合研磨进行<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>, 得到的<span style=\"color:red\">反应</span>混合物再用水洗去其中的可溶性无机盐并烘干, 即得氧化锆前驱体. 前驱体经530 ℃下热解3 h即得氧化锆产品, 采用TG/DTA, XRD和TEM对前驱体及产品进行了表征. 结果表明, 所得产品氧化锆为结晶良好、以四方相为主的混合晶相, 其平均粒径约为25 nm.","authors":[{"authorName":"吴文伟","id":"51858d57-e2c2-4a1c-a7f5-fcaca8369546","originalAuthorName":"吴文伟"},{"authorName":"廖森","id":"99555f3d-6a02-42fa-a097-dfde78a94253","originalAuthorName":"廖森"},{"authorName":"姜求宇","id":"e434024e-39fa-4e8a-a44c-077290d80567","originalAuthorName":"姜求宇"},{"authorName":"宋宝玲","id":"da2acaee-9f64-4b5d-9014-828a55b4c145","originalAuthorName":"宋宝玲"},{"authorName":"黎子学","id":"758856d9-6fc4-42be-b58b-f2befa264f3c","originalAuthorName":"黎子学"},{"authorName":"邓广金","id":"5b571afc-418e-4f00-be7e-9f1f49d57138","originalAuthorName":"邓广金"}],"doi":"10.3969/j.issn.0258-7076.2005.04.044","fpage":"567","id":"6ca6fc19-81eb-4d2c-97b8-0884c9beb8b6","issue":"4","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"fd32b1c2-587b-43f5-92a2-a43b2f7f8cc0","keyword":"氧化锆","originalKeyword":"氧化锆"},{"id":"618a329b-8f4f-468b-9aad-afd29b058a40","keyword":"纳米","originalKeyword":"纳米"},{"id":"2936d05a-86fb-4200-9789-f4fa25f1fe0e","keyword":"氯氧化锆","originalKeyword":"氯氧化锆"},{"id":"3cc51881-a7c6-4121-a628-c44661ef3c62","keyword":"制备","originalKeyword":"制备"},{"id":"bba67840-1c7b-4b65-8369-80f0a026e272","keyword":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>","originalKeyword":"室温固相反应"}],"language":"zh","publisherId":"xyjs200504044","title":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>法制备纳米氧化锆及表征","volume":"29","year":"2005"},{"abstractinfo":"以CdO、CdCO3、CdCl2作Cd的前驱物,分别与Na2S·9H2O和Se粉在<span style=\"color:red\">室温</span>条件下,采用<span style=\"color:red\">固</span>相研磨法制备CdS1-xSex.XRD结果表明,合成产物与Cd的前驱物有关,即以CdO作Cd的前驱物时,得到的产物是CdS0.54Se0.46;而以CdCO3或CdCl2作Cd的前驱物时,得到的产物是CdS0.75Se0.25.吸收谱(U-3310 Spectrophotometer)和荧光谱(AFS AFS-230E)的测试结果进一步证实了CdS0.54Se0.46和CdS0.75Se0.25产物,最后对<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>合成CdS1-xSex的机理进行了探讨.","authors":[{"authorName":"陈玉凤","id":"25ff869d-6fe5-424d-98e0-8bece8d17445","originalAuthorName":"陈玉凤"},{"authorName":"欧阳毅","id":"6c7892d2-4291-4888-bf96-2609b8f8a541","originalAuthorName":"欧阳毅"}],"doi":"10.3969/j.issn.1001-1625.2007.04.038","fpage":"808","id":"b976efe5-a425-4874-b01f-f6c248098997","issue":"4","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"ce7670aa-a37e-476a-89eb-35e6cc49f763","keyword":"<span style=\"color:red\">室温</span>","originalKeyword":"室温"},{"id":"dd68fbdc-1e36-419c-84b0-b97cb609e738","keyword":"<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>","originalKeyword":"固相反应"},{"id":"e46c4887-2bd9-44e7-b82e-b20f297127e8","keyword":"CdS1-xSex","originalKeyword":"CdS1-xSex"},{"id":"95e221a6-4b64-41c4-87b1-f1643dafcfcf","keyword":"研磨","originalKeyword":"研磨"}],"language":"zh","publisherId":"gsytb200704038","title":"前驱物对<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>合成CdS1-xSex的影响","volume":"26","year":"2007"},{"abstractinfo":"以硝酸钴和碳酸氢铵为原料,采用<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>首先制备出前驱物碱式碳酸钴,然后将前驱物在250°C分解3h,得到纳米四氧化三钴.用X射线粉末衍射、透射电镜、热分析仪、扫描电镜对产物的组成、大小、形貌及有关性质进行了表征.结果表明获得了平均粒径在13nm、分布均匀、无团聚的纳米粉体.","authors":[{"authorName":"庄稼","id":"f78717c9-0c59-4567-806f-55232fdd8bfc","originalAuthorName":"庄稼"},{"authorName":"迟燕华","id":"5ad34b95-c06d-48dd-bad4-8eb306542a7f","originalAuthorName":"迟燕华"},{"authorName":"王曦","id":"e5b4db79-9c70-4d86-b4c3-4ad9760884b5","originalAuthorName":"王曦"},{"authorName":"王清成","id":"3022f336-558e-40e8-b8f6-db672410a525","originalAuthorName":"王清成"},{"authorName":"杨定明","id":"f639f12f-19ef-4076-a444-bc09d8fc9614","originalAuthorName":"杨定明"},{"authorName":"贾殿赠","id":"16e38eff-8e1e-47fe-9bc6-4c25b107158d","originalAuthorName":"贾殿赠"}],"doi":"10.3321/j.issn:1000-324X.2001.06.028","fpage":"1203","id":"64fc06e6-b0de-4c74-9361-a4f901552c28","issue":"6","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"fde856f1-76d5-4f0e-a0c1-6db9c045054a","keyword":"四氧化三钴","originalKeyword":"四氧化三钴"},{"id":"88d4901d-ddac-4b1c-82e7-2583f67d590a","keyword":"<span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>","originalKeyword":"固相反应"},{"id":"ff9a1296-9ca2-4d12-842d-d851177c3341","keyword":"纳米粉体","originalKeyword":"纳米粉体"}],"language":"zh","publisherId":"wjclxb200106028","title":"<span style=\"color:red\">室温</span><span style=\"color:red\">固</span><span style=\"color:red\">相反应</span>制备纳米CO3O4粉体","volume":"16","year":"2001"}],"totalpage":6765,"totalrecord":67644}