{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"目的研究<span style=\"color:red\">氯</span><span style=\"color:red\">原</span><span style=\"color:red\">酸</span>(CGA)对自发性肥胖糖尿病db/db小鼠糖脂代谢紊乱的影响及其作用机制。方法&quot;将13只5～6周龄雄性db/db小鼠随机分为db/db-CGA组（<em>n</em>=7）和db/db-CON组（<em>n</em>=6），13只5～6周龄雄性db/m小鼠随机分为db/m-CGA组（<em>n</em>=6）和db/m-CON组（<em>n</em>=7）；CGA组均给予80-mg/〖DK〗（kg&middot;d）CGA灌胃，CON组均给予等体积PBS灌胃。12周后检测血浆、肝脏、骨骼肌中糖脂生化指标，内脏脂肪组织中脂联素和内脂素含量，肝脏葡萄糖-〖KG*8〗6-磷酸酶（G-〖KG*8〗6-Pase）和过氧化物酶体增殖物激活受体-&alpha;（PPAR-&alpha;）的mRNA水平及其蛋白表达。结果&quot;给予CGA 12周后，db/db-CGA组小鼠血浆、肝脏和骨骼肌中三酰甘油含量和空腹血糖均明显低于db/db-CON组（<em>P</em>均&lt;0.05），肌糖原含量明显高于db/db-CON组（<em>P</em>&lt;0.05）；脂联素水平明显高于db/db-CON组（<em>P</em>&lt;0.01），低于db/m-CGA组（<em>P</em>&lt;0.05）；内脂素水平明显低于db/db-CON组（<em>P</em>&lt;0.01），高于db/m-CGA组（<em>P</em>&lt;0.05）；G-〖KG*8〗6-Pase mRNA表达水平较db/db-CON组明显下降（<em>P</em>&lt;0.05）， PPAR-&alpha; mRNA和蛋白表达水平均较db/db-CON组明显升高（<em>P</em>&lt;0.05）。结论&quot;CGA可改善自发性肥胖糖尿病小鼠糖脂代谢紊乱，其机理可能与调节脂肪因子分泌，上调肝脏PPAR-&alpha;水平及抑制G-〖KG*8〗6-Pase表达有关。","authors":[{"authorName":"张兰涛","id":"d229fc74-15f5-4cd4-b244-8b56f2e30cb3","originalAuthorName":"张兰涛"},{"authorName":"常翠青","id":"24f21a3b-3937-4086-b8db-5d2404f3f778","originalAuthorName":"常翠青"},{"authorName":"刘阳","id":"b16d2e48-c4d0-4ab5-b7de-eb7b4c7f9598","originalAuthorName":"刘阳"},{"authorName":"陈志民","id":"d8069adf-13ae-41f2-9345-066713372fe7","originalAuthorName":"陈志民"}],"categoryName":"|","doi":"10.3881/j.issn.1000-503X.2011.03.015","fpage":"281","id":"a139ce78-c187-4ffd-b7bb-31620aaf9d20","issue":"1","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[{"id":"0f3c3102-b90b-4d92-8ad0-0a706e93da24","keyword":"<span style=\"color:red\">氯</span><span style=\"color:red\">原</span><span style=\"color:red\">酸</span>","originalKeyword":"氯原酸"},{"id":"ec1baead-a3b9-433c-9b17-cbbcc8741211","keyword":" glucose-lipid metabolism","originalKeyword":" glucose-lipid metabolism"},{"id":"4d802900-e094-4c2b-8d74-d5ca0d04a449","keyword":" adiponectin","originalKeyword":" adiponectin"},{"id":"1da96ddd-a91a-4edd-922b-f53c974b0d98","keyword":" visfatin","originalKeyword":" visfatin"},{"id":"8ec7645c-04ea-48ef-8bb4-705802c52c05","keyword":" db/db mice","originalKeyword":" db/db mice"}],"language":"zh","publisherId":"1002-6495_2011_1_10","title":"<span style=\"color:red\">氯</span><span style=\"color:red\">原</span><span style=\"color:red\">酸</span>对db/db小鼠糖脂代谢紊乱的影响及其作用机制","volume":"1","year":"2011"},{"abstractinfo":"以土豆淀粉为原料、环氧<span style=\"color:red\">氯</span>丙烷为交联剂制备交联淀粉,再进行黄<span style=\"color:red\">原</span>酸化反应制备不溶性淀粉黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯,利黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯吸附电镀废水中的Cr(Ⅵ).通过正交试验确定黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯对含Cr(Ⅵ)废水的最佳实验条件,ρ[Cr(Ⅵ)]=25 mg/L时,以40 r/min慢速搅拌,在pH =8,反应t为40 min,投加4g/L黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯时,Cr(Ⅵ)去除率为99.7％,Cr(Ⅵ)的出水质量浓度为0.075 mg/L,低于国家最高允许排放限值中的新建电镀企业排放限值.","authors":[{"authorName":"严鹤峰","id":"d9cc40a5-c513-462f-a28b-2c67402a6cb4","originalAuthorName":"严鹤峰"},{"authorName":"李琛","id":"0eb234d0-b13b-43cd-9a69-c5e6e46dd64b","originalAuthorName":"李琛"}],"doi":"10.3969/j.issn.1001-3849.2013.05.012","fpage":"43","id":"63f48307-24dc-4c76-be45-dee6ecaabf0d","issue":"5","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰   "},"keywords":[{"id":"6b7ae21d-4765-4eda-9b4e-db95a8a77c47","keyword":"不溶性淀粉黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯","originalKeyword":"不溶性淀粉黄原酸酯"},{"id":"68619a69-662a-4e2c-8aa4-94157473a967","keyword":"Cr(Ⅵ)","originalKeyword":"Cr(Ⅵ)"},{"id":"74a31c14-93fe-4cf8-8eb2-db9c884d84b6","keyword":"电镀废水","originalKeyword":"电镀废水"},{"id":"48172b59-525c-4083-a00f-3125a72e3ac9","keyword":"重金属废水","originalKeyword":"重金属废水"}],"language":"zh","publisherId":"ddjs201305012","title":"不溶性淀粉黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯处理Cr(Ⅵ)废水的研究","volume":"35","year":"2013"},{"abstractinfo":"通过<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯和季戊四醇进行酯交换反应制备了双环<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯4-羟甲基-2,6,7-三氧杂二环(2,2,2)辛烷,提出采用<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯和季戊四醇在没有催化剂存在时直接反应,可以合成出4-羟甲基-2,6,7-三氧杂二环(2,2,2)辛烷,并研究了这种合成方法的合成机理.首次进行了双环<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯4-羟甲基-2,6,7-三氧杂二环(2,2,2)辛烷和大分子未封端聚醚预聚物聚醚的反应,得到了具有较大分子量的两端带有双环<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯膨胀基团的长链大分子膨胀单体.","authors":[{"authorName":"余红伟","id":"5fa458e4-0904-40c4-96aa-1450ec6dee52","originalAuthorName":"余红伟"},{"authorName":"王源升","id":"3f6288f4-6efb-4d44-852b-f5f7c258511f","originalAuthorName":"王源升"}],"doi":"","fpage":"47","id":"73a22a2e-3f0e-490f-849c-0b00bba7a9a4","issue":"5","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"d3f2c053-806b-4983-ab3a-a82e1f8c3969","keyword":"双环<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯","originalKeyword":"双环原酸酯"},{"id":"0a2a8e82-6884-4301-8d5e-92f37dcf015d","keyword":"膨胀单体","originalKeyword":"膨胀单体"},{"id":"df2783c5-3347-41a6-927a-efc0955e5e99","keyword":"膨胀聚合反应","originalKeyword":"膨胀聚合反应"}],"language":"zh","publisherId":"gfzclkxygc200505012","title":"双环<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯类膨胀单体的合成","volume":"21","year":"2005"},{"abstractinfo":"以环氧<span style=\"color:red\">氯</span>丙烷(EPC)为交联剂,在温和条件下“一锅法”制备了水溶性EPC交联黄<span style=\"color:red\">原</span>胶(XG),考察了交联度、NaCl质量分数、pH和温度对EPC交联XG(cXG)溶液流变性的影响.结果表明,随交联度增大,cXG溶液黏度和动力学模量均明显增大,弹性增强;随NaCl质量分数增大,溶液黏度和动力学模量均呈现先降低后增加趋势;pH在4～10范围内变化对体系流变性基本无影响;随温度升高,溶液黏度和动力学模量均降低,但与XG溶液相比,抗温性能明显提高.","authors":[{"authorName":"杨婷婷","id":"691c7d32-0639-4c2a-b64e-8a102df9efda","originalAuthorName":"杨婷婷"},{"authorName":"李海平","id":"eb0729df-6273-49cb-9bb5-5d1341ce624e","originalAuthorName":"李海平"},{"authorName":"侯万国","id":"78b90915-a4ae-47a7-9ac5-1c8489e65345","originalAuthorName":"侯万国"}],"doi":"","fpage":"39","id":"800285ba-6ac7-48c0-b184-cf8a8c5c0588","issue":"5","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"08189c7f-e717-47fa-b675-553c3378e8f5","keyword":"黄<span style=\"color:red\">原</span>胶","originalKeyword":"黄原胶"},{"id":"094e47dc-95a9-4116-91a8-a2db317d04bc","keyword":"环氧<span style=\"color:red\">氯</span>丙烷","originalKeyword":"环氧氯丙烷"},{"id":"a3b005b8-faab-4c47-bd0d-364abef3ea16","keyword":"交联","originalKeyword":"交联"},{"id":"9aa75464-c9d9-46cb-b045-33697692205b","keyword":"流变性","originalKeyword":"流变性"},{"id":"9954b849-ad2d-4915-9152-277d5233dcb0","keyword":"抗温性","originalKeyword":"抗温性"}],"language":"zh","publisherId":"gfzclkxygc201505007","title":"环氧<span style=\"color:red\">氯</span>丙烷交联黄<span style=\"color:red\">原</span>胶溶液的流变及抗温性能","volume":"31","year":"2015"},{"abstractinfo":"对黄<span style=\"color:red\">原</span>胶(XG)和丙烯<span style=\"color:red\">酸</span>(AA)进行60Co γ辐射制备黄<span style=\"color:red\">原</span>胶/丙烯<span style=\"color:red\">酸</span>接枝共聚物(XG-g-PAA).考察了原料配比及辐射条件对产品接枝率及接枝效率的影响,以FT-IR、XRD、SEM分析了接枝物的分子结构及形貌,以TG分析其热性能.结果表明,当XG质量浓度为10 g/L,AA与XG质量比为8,辐射总剂量为6.0 kGy,甲醇与水的体积比为7:3时,产品接枝率达130.8%,接枝效率达82.4%.SEM表明辐射引发较化学引发更易得到多孔疏松的产品,且添加甲醇水溶液可明显提高产品的孔隙率.初步探讨了辐射接枝机理.","authors":[{"authorName":"杨连利","id":"6eae8d08-ea4f-4973-abf3-9a8ed1f16bb7","originalAuthorName":"杨连利"},{"authorName":"梁国正","id":"2319ecc1-da79-4e6b-b54d-abd3e90cb367","originalAuthorName":"梁国正"}],"doi":"","fpage":"157","id":"0840be96-c94b-4e05-83c2-89ad1eb116ba","issue":"5","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"ce9a26b1-3b58-405b-a58a-95a8ac60643d","keyword":"黄<span style=\"color:red\">原</span>胶","originalKeyword":"黄原胶"},{"id":"a588a286-229a-4777-a325-8b94bbe75036","keyword":"丙烯<span style=\"color:red\">酸</span>","originalKeyword":"丙烯酸"},{"id":"ebc7fe4b-8acb-4f95-9a09-4c050f2efd20","keyword":"共辐射接枝","originalKeyword":"共辐射接枝"}],"language":"zh","publisherId":"gfzclkxygc200905045","title":"黄<span style=\"color:red\">原</span>胶共辐射接枝丙烯<span style=\"color:red\">酸</span>","volume":"25","year":"2009"},{"abstractinfo":"以正丁醇、氢氧化钠和二硫化碳为原料,水作溶剂合成正丁基黄<span style=\"color:red\">原</span>酸钠,再与一氯化硫反应,室温条件下合成对称的二硫化二正丁基黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯,并探讨了反应条件对合成正丁基黄<span style=\"color:red\">原</span>酸钠和二硫化二正丁基黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯产率的影响.通过红外(FT-IR)、核磁(1H NMR)、质谱(MS)及元素分析等技术手段确定了产物的结构.优化的合成条件为:n(正丁基黄<span style=\"color:red\">原</span>酸钠)∶n(S2Cl2) =2∶1.1,温度为室温,溶剂为THF,反应时间为2 min,产率可达83.2％,反应条件温和,反应迅速、收率高.","authors":[{"authorName":"曾燕飞","id":"9f6669f4-5042-445f-a3ba-bdd959f32d09","originalAuthorName":"曾燕飞"},{"authorName":"周元林","id":"0378ea88-bff6-4093-b4e2-da899ecf240f","originalAuthorName":"周元林"}],"doi":"10.3724/SP.J.1095.2014.30599","fpage":"1019","id":"088ae6d8-827e-4bc4-845c-b86b275ed9b1","issue":"9","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"b2ecc3eb-70da-4dc9-9f81-fa3bd0052d3b","keyword":"正丁基黄<span style=\"color:red\">原</span>酸钠","originalKeyword":"正丁基黄原酸钠"},{"id":"b8fa8c6d-ab32-435b-931a-58c944e4ddea","keyword":"二硫化二正丁基黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯","originalKeyword":"二硫化二正丁基黄原酸酯"},{"id":"61a9b906-a520-412a-b291-43525a9de38d","keyword":"促进剂","originalKeyword":"促进剂"},{"id":"4a454aad-2e0a-4c96-90b7-435fadf9ad00","keyword":"合成","originalKeyword":"合成"},{"id":"d5ae0837-1b8a-4a8f-89e3-d26ff06633c8","keyword":"表征","originalKeyword":"表征"}],"language":"zh","publisherId":"yyhx201409003","title":"室温合成二硫化二正丁基黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯及其表征","volume":"31","year":"2014"},{"abstractinfo":"提出了以淀粉黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯为富集剂,富集、分离和测定水中痕量镉的新方法.研究结果表明,富集实验条件pH为6.0,t为60min,富集在黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯上的镉用0.5 mol/L硫酸溶液洗脱,方法的检出限为0.0065 mg/L,相对标准偏差为2.7％(n=6),线性范围为0.05～1.00 mg/L,加标回收率为98.0％～102.2％.","authors":[{"authorName":"郑京","id":"2d09fb78-847a-4474-bb22-96e5ae7caa43","originalAuthorName":"郑京"}],"doi":"","fpage":"38","id":"8578fe8a-9294-42e7-8390-8f21dff93a7b","issue":"12","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰   "},"keywords":[{"id":"3c0a3a51-c468-4812-a191-dce884b39515","keyword":"火焰原子吸收光谱法","originalKeyword":"火焰原子吸收光谱法"},{"id":"90ffcaa4-bf56-4968-a15c-9ade8c3ef4d6","keyword":"富集","originalKeyword":"富集"},{"id":"dbb21b40-66ca-4505-b40b-e4b1da424bcc","keyword":"淀粉黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯","originalKeyword":"淀粉黄原酸酯"},{"id":"8abd3765-6bfa-4009-bc30-6f5d51ce5ea8","keyword":"镉","originalKeyword":"镉"},{"id":"e022d744-8484-4cc6-961e-f3d54c4a8638","keyword":"测定","originalKeyword":"测定"}],"language":"zh","publisherId":"ddjs201212010","title":"淀粉黄<span style=\"color:red\">原</span><span style=\"color:red\">酸</span>酯富集-火焰原子吸收光谱法测定痕量镉","volume":"34","year":"2012"},{"abstractinfo":"在非均相条件下，利用漆酶催化氧化<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>使其接枝到壳聚糖进行改性，初步探究改性过程中，反应体系各组分相对浓度的变化、改性壳聚糖上原儿茶<span style=\"color:red\">酸</span>的接枝反应历程以及改性壳聚糖抗氧化性能的提升效果。通过React IR(反应红外)分析表明壳聚糖先将<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>吸附到固相之后才发生进一步反应，通过Py-GC/MS(裂解气相色谱质谱联用)分析表明接枝反应后<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>是通过化学键连接到了壳聚糖，利用Solid-state 13 C NMR(固体核磁共振)和 FT-IR(红外光谱)检测到接枝前后新的化学键生成，进一步表明<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>通过化学键接枝到了壳聚糖，通过 ABTS 法测定接枝反应前后壳聚糖的抗氧化性能，发现接枝后壳聚糖抗氧化性能的提高显著。","authors":[{"authorName":"裴继诚","id":"03167529-f8bd-4721-853a-872a75e57266","originalAuthorName":"裴继诚"},{"authorName":"李中阳","id":"a2c3bea3-a3f1-4995-9251-3a7861953844","originalAuthorName":"李中阳"},{"authorName":"张方东","id":"e9b262f3-cdea-4399-b318-2f6bee5af07e","originalAuthorName":"张方东"},{"authorName":"王兵","id":"0fdc39e7-9a1c-47d7-bff5-0a9a5fd25331","originalAuthorName":"王兵"},{"authorName":"殷允北","id":"82c259b0-b770-4d5a-8d0d-c5df434e13c5","originalAuthorName":"殷允北"},{"authorName":"张冬旭","id":"c6a5dcba-b1ab-4497-ab97-b58373bd7699","originalAuthorName":"张冬旭"}],"doi":"10.3969/j.issn.1001-9731.2015.05.008","fpage":"5043","id":"0b9770b7-176d-4d0e-bb63-9159d50ebce5","issue":"5","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"faf8d3ac-e88e-4e52-979f-58a6e4fd102c","keyword":"<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>","originalKeyword":"原儿茶酸"},{"id":"3457d9a7-25b8-42b2-a5f2-f01fda6f2814","keyword":"漆酶","originalKeyword":"漆酶"},{"id":"f26d64d8-a4b0-4594-80cf-801f2d97d442","keyword":"壳聚糖","originalKeyword":"壳聚糖"},{"id":"c8cd971b-5dda-49ef-aa4e-1de0f778ab1c","keyword":"React IR","originalKeyword":"React IR"},{"id":"cea34766-c1f9-4c96-b6c5-4b940273547b","keyword":"Py-GC/MS","originalKeyword":"Py-GC/MS"},{"id":"08187f3c-5697-4354-b405-ca363561c139","keyword":"反应机理","originalKeyword":"反应机理"}],"language":"zh","publisherId":"gncl201505008","title":"漆酶催化<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>与壳聚糖接枝反应机理的初步探究?","volume":"","year":"2015"},{"abstractinfo":"建立了大鼠血浆中原儿茶<span style=\"color:red\">酸</span>含量测定的高效液相色谱方法.采用的色谱柱为DiamondsilTMC18柱(150 mm×4.6 mm,5 μm);流动相为乙腈-水(体积比为9:91,用H3PO4调pH至2.5);流速1.2 mL/min;检测波长260nm;内标为对羟基苯甲酸.<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>的线性范围为0.050～3.20 mg/L,线性相关系数为0.997 8,最低定量限为0.050 mg/L,日内和日间测定的精密度(以相对标准偏差表示)均低于7.0%,准确度(以相对误差表示)为-1.4%～2.6%;在0.050,0.40,3.20 mg/L低、中、高3个添加浓度水平下,血浆样品的提取回收率分别为83.4%,87.3%,91.1%.该方法简便,灵敏,准确,适用于大鼠体内<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>的药物动力学研究.","authors":[{"authorName":"韩(王莹)","id":"7a6c2d7a-960b-4dc4-8bc9-87fcb60ce9a9","originalAuthorName":"韩(王莹)"},{"authorName":"熊志立","id":"561d1b13-3fc1-4402-adc6-bf09b0675051","originalAuthorName":"熊志立"},{"authorName":"杨春娟","id":"2de00830-73c1-4834-b9dc-4f70e610f096","originalAuthorName":"杨春娟"},{"authorName":"刘曼","id":"baf0429e-29de-4ef5-88f8-457ebdde79ed","originalAuthorName":"刘曼"},{"authorName":"李发美","id":"3695d0a5-4b09-4cad-888d-978d60e42461","originalAuthorName":"李发美"}],"doi":"10.3321/j.issn:1000-8713.2007.02.016","fpage":"207","id":"70868875-412d-474c-b578-76f2610d0b56","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"c4faee45-4ff6-4514-9142-d5451202bb08","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"27d7e2ac-be5f-4308-993f-ebd41ca7f4a4","keyword":"<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>","originalKeyword":"原儿茶酸"},{"id":"1db78116-8b29-4dd3-be59-558b72670341","keyword":"大鼠血浆","originalKeyword":"大鼠血浆"}],"language":"zh","publisherId":"sp200702016","title":"高效液相色谱法测定大鼠血浆中的<span style=\"color:red\">原</span>儿茶<span style=\"color:red\">酸</span>","volume":"25","year":"2007"},{"abstractinfo":"采用双氧水盐酸混合溶金制得<span style=\"color:red\">氯</span>金<span style=\"color:red\">酸</span>溶液,在<span style=\"color:red\">氯</span>金<span style=\"color:red\">酸</span>溶液中加入氯化钾蒸发结晶得到桔黄色<span style=\"color:red\">氯</span>金<span style=\"color:red\">酸</span>钾晶体.研究表明,5g金粉中加入5倍理论量的双氧水和盐酸,100℃下搅拌反应20min,得到<span style=\"color:red\">氯</span>金<span style=\"color:red\">酸</span>溶液,溶液中加入理论量氯化钾,搅拌蒸发结晶得到KAuCl4·2H2O晶体.热重差热(TG-DTA)实验结果表明,样品在25～431.68℃有2个明显吸热过程和1个连续失重过程.根据X射线衍射(XRD)实验,329℃时KAuCl4·2H2O热分解固体产物为KAuCl4,376℃时KAuCl4热分解固体产物为Au和KCl.","authors":[{"authorName":"郑雅杰","id":"f0b3906b-7900-47c1-9e5d-12b71ff39a95","originalAuthorName":"郑雅杰"},{"authorName":"郭伟","id":"708e8599-d964-4c35-8fdb-6c99ec4060b6","originalAuthorName":"郭伟"},{"authorName":"白猛","id":"4ab45a40-b2f4-4a1d-9b71-a498031c132c","originalAuthorName":"白猛"}],"doi":"10.3969/j.issn.1004-0676.2007.03.001","fpage":"1","id":"d4b19543-3ca8-4867-9336-2fa65a1f0f9c","issue":"3","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"8e28e246-1994-4e79-a618-2bf2201739ae","keyword":"无机化学","originalKeyword":"无机化学"},{"id":"0106f936-6fb2-47e2-bada-dbe6ef1ba88a","keyword":"双氧水","originalKeyword":"双氧水"},{"id":"eb8c807e-8b19-44bb-8de3-985d574b4191","keyword":"盐酸","originalKeyword":"盐酸"},{"id":"d6a724b6-0039-4813-9a8f-5f547fc1dec5","keyword":"<span style=\"color:red\">氯</span>金<span style=\"color:red\">酸</span>","originalKeyword":"氯金酸"},{"id":"21c38756-960d-46f7-bd72-ec5e96c377ed","keyword":"氯化钾","originalKeyword":"氯化钾"},{"id":"6282a8e0-2a85-4f5f-848b-9f3acb989c6b","keyword":"<span style=\"color:red\">氯</span>金<span style=\"color:red\">酸</span>钾","originalKeyword":"氯金酸钾"},{"id":"0ece22e8-2492-40e8-84e4-a7d91b1d76dd","keyword":"热分解","originalKeyword":"热分解"}],"language":"zh","publisherId":"gjs200703001","title":"<span style=\"color:red\">氯</span>金<span style=\"color:red\">酸</span>钾制备及其热分解","volume":"28","year":"2007"}],"totalpage":1746,"totalrecord":17454}