{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用后交联技术,在滴加有机单体前调节反应体系的pH值,控制有机氧烷的水解,合成含量高达30%的自交联丙乳液.对该乳液进行交联度测定、红外光谱和粒径分析,证实了交联反应的发生.性能测试表明,提高含量极大地增强了聚合物的稳定性、耐水性、耐溶剂性和热稳定性.","authors":[{"authorName":"陈忠奎","id":"586ec70a-7bfd-4075-9cba-03b224c5a576","originalAuthorName":"陈忠奎"},{"authorName":"范慧俐","id":"7c0e5c0c-395b-4bd1-96f4-eab696786517","originalAuthorName":"范慧俐"},{"authorName":"康立训","id":"23bfeecc-7af1-4512-83f7-04e1da52c745","originalAuthorName":"康立训"},{"authorName":"肖军平","id":"42df255d-486c-4d88-9b81-35124d4d6739","originalAuthorName":"肖军平"}],"doi":"10.3969/j.issn.0253-4312.2004.12.005","fpage":"15","id":"5759503e-a148-4cfc-9ac0-6eb69bc626eb","issue":"12","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"9e137298-7e16-4e1d-af4e-f40cf86ff0d7","keyword":"含量","originalKeyword":"高硅含量"},{"id":"9768001b-97e1-4648-a850-3539a9d8730d","keyword":"自交联","originalKeyword":"自交联"},{"id":"96975f9c-f12d-470e-b7bc-7c5d14a77406","keyword":"丙乳液","originalKeyword":"硅丙乳液"},{"id":"f1f622c6-17fc-46a8-b0e5-ace91a521382","keyword":"性能","originalKeyword":"性能"},{"id":"b9dbf759-ece9-4902-b685-bdc0b39c61e5","keyword":"红外光谱","originalKeyword":"红外光谱"}],"language":"zh","publisherId":"tlgy200412005","title":"含量自交联丙乳液的合成及性能研究","volume":"34","year":"2004"},{"abstractinfo":"以甲基丙烯酸甲酯(MMA)、丙烯酸丁酯(BA)、苯乙烯(St)为主要原料,以乙烯基三甲氧基硅烷(A-171)为改性单体,以烯丙基聚乙氧基磺酸盐(SE - 10N)和十二烷基苯磺酸钠(DSB)为混合乳化剂,采用水溶性引发剂过硫酸铵(APS)和亚硫酸氢钠(SBS)与油溶性引发剂偶氮二异丁腈(AIBN)2种引发体系相配合的方式,通过烷氧基硅烷和苯乙烯混合单体对丙烯酸酯种子乳液先渗透溶胀,再进行聚合的方法(单体渗透法)合成了A - 171含量高达50%的-苯丙乳液.利用傅里叶变换红外光谱仪对聚合物结构进行了分析,证明了A-171的引入,通过透射电子显微镜(TEM)对粒子形态、粒径分布进行了表征,用原子力显微镜(AFM)、扫描电子显微镜(SEM)相结合的方法对乳液的成膜性能以及成膜助剂的作用进行了分析.最后通过性能测试证明,A -171含量的提高有利于降低涂膜的吸水率,增强涂膜的热稳定性.","authors":[{"authorName":"刘兴","id":"cd7aa680-2b02-49eb-8452-f95b07fc94d4","originalAuthorName":"刘兴"},{"authorName":"邱藤","id":"9202ef05-4be0-43dc-8d12-0aad0d17b09c","originalAuthorName":"邱藤"},{"authorName":"何立凡","id":"2cdf34ad-cf1a-4e39-ada1-2a193e3869f8","originalAuthorName":"何立凡"},{"authorName":"张胜文","id":"94b036a1-5f12-4fd3-ba64-1673db291f2e","originalAuthorName":"张胜文"},{"authorName":"李效玉","id":"6ade7391-4978-4b16-abd3-4e346c5fe563","originalAuthorName":"李效玉"}],"doi":"10.3969/j.issn.0253-4312.2012.11.018","fpage":"67","id":"4cb48a3c-4ad6-4b55-afab-69b141faa95e","issue":"11","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"edc7ccd9-c333-47c9-a580-810dca564cb9","keyword":"含量","originalKeyword":"高硅含量"},{"id":"30825de4-8de7-4d89-90c7-42baf4eabae1","keyword":"-苯丙乳液","originalKeyword":"硅-苯丙乳液"},{"id":"1df2b419-4da7-4148-a8dd-5810893ea879","keyword":"单体渗透","originalKeyword":"单体渗透"},{"id":"b76e4048-4b1a-4f0a-9702-6a5508238772","keyword":"成膜","originalKeyword":"成膜"}],"language":"zh","publisherId":"tlgy201211018","title":"含量-苯丙乳液的合成及性能研究","volume":"42","year":"2012"},{"abstractinfo":"以四甲基四乙烯基环四氧烷(Vi-D4)为有机单体,在乳液体系中开环聚合得到有机中间体,采用种子乳液聚合工艺,与丙烯酸单体共聚得到含量丙乳液.研究了体系的pH、加料方式、乳化剂的用量、引发剂的用量对乳液聚合稳定性的影响,发现Vi-D4在pH =3下开环聚合,引发剂用量为单体总量的0.4%,且其配比为3∶2,乳化剂的用量为3%,控制丙烯酸有机中间体的滴加时间分别为2h和3h制得的乳液稳定性.","authors":[{"authorName":"杨震","id":"0e13c8f2-3fb2-44e6-b876-df19a5420b12","originalAuthorName":"杨震"},{"authorName":"卿宁","id":"ce8a3b94-fc55-4f09-ab1c-c8de29e284af","originalAuthorName":"卿宁"}],"doi":"10.3969/j.issn.0253-4312.2012.03.008","fpage":"32","id":"4fafdf54-3546-4a90-8b7c-e4cd3cdee3cf","issue":"3","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"c65a5e07-2071-4587-9d67-203670803e25","keyword":"四甲基四乙烯基环四氧烷","originalKeyword":"四甲基四乙烯基环四硅氧烷"},{"id":"b0cee92f-9e7c-4bd0-9bd2-777a8698e27b","keyword":"聚合稳定性","originalKeyword":"聚合稳定性"},{"id":"aed89af0-c5a6-4bde-88b9-3188643cd726","keyword":"丙乳液","originalKeyword":"硅丙乳液"},{"id":"83f6daea-869f-4dda-8b9c-1d76c1892c8b","keyword":"含量","originalKeyword":"高硅含量"}],"language":"zh","publisherId":"tlgy201203008","title":"含量四甲基甲乙烯基环四氧烷改性丙烯酸酯乳液的聚合稳定性","volume":"42","year":"2012"},{"abstractinfo":"为了解决常规有机单体在乳液聚合反应中易水解的问题,通过γ-甲基丙烯酰氧丙基三甲氧基硅烷(KH-570)和三甲基氯硅烷间的取代反应合成了一种难水解的新型有机单体γ-甲基丙烯酰氧丙基三(三甲基氧基)硅烷,再以其和丙烯酸酯类单体为原料,采用种子乳液共聚法合成了含量有机-丙烯酸酯复合共聚乳液.采用傅里叶红外光谱(FTIR)、核磁共振(NMR)对新型有机单体进行了结构表征,利用红外光谱、表面接触角测试、热失重分析、拉伸测试等表征了乳液及乳胶膜性能.结果表明:新型有机改性丙烯酸酯乳胶膜比纯丙烯酸酯乳胶膜在耐水性、耐热性及力学性能等方面均有显著提高.","authors":[{"authorName":"孙亚月","id":"7a4d7434-739e-453a-811f-92cb598f53ff","originalAuthorName":"孙亚月"},{"authorName":"佘铜","id":"dbe5fa8b-95f6-4f98-b1bf-daf2e8dc7581","originalAuthorName":"佘铜"}],"doi":"","fpage":"22","id":"89dc60bd-485c-4453-ae92-7cf3c402d081","issue":"8","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"b5a5ef64-375c-47e0-bc0f-2f60dcfb8593","keyword":"复合共聚乳液","originalKeyword":"复合共聚乳液"},{"id":"8f0d3544-5421-4b11-984b-2e7eaf2da7e3","keyword":"有机改性","originalKeyword":"有机硅改性"},{"id":"7c2bbea6-e2fe-4120-868c-5382b4bd0237","keyword":"丙烯酸酯","originalKeyword":"丙烯酸酯"},{"id":"e0e63c3b-9d83-430b-882c-aeff27210285","keyword":"含量","originalKeyword":"高硅含量"},{"id":"9e1fb5b0-aba3-4ed8-a99f-351abfb1d14a","keyword":"耐水性","originalKeyword":"耐水性"},{"id":"c5a08266-ad2e-4aba-b764-0f0b82e0fd0a","keyword":"耐热性","originalKeyword":"耐热性"},{"id":"021b3386-e4f0-4dd8-8b69-91413e075082","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"clbh201408007","title":"新型有机改性丙烯酸酯乳液的制备及性能","volume":"47","year":"2014"},{"abstractinfo":"先合成了聚氧烷阴离子乳液以及链中含硅烷偶联剂和含氟单体的(甲基)丙烯酸酯聚合物乳液,并且利用羟基缩合反应,将2种乳液混合反应,通过乳液接枝共聚的方法合成了一种含量的有机改性氟代(甲基)丙烯酸酯聚合物乳液,并采用了红外光谱对聚合物乳液分子进行了表征.测试结果表明:有机质量分数为20%、有机氟质量分数为12%的聚合物乳液涂膜综合性能最佳,较不含有机氟的聚合物乳液涂膜,其水表面接触角由77.5°增加到96°,24 h吸水率由5.3%下降到2.3%,耐水性大大增加;玻璃化转变温度由8.53 ℃下降到-2.74℃,聚合物分子链的柔顺性有所提高;同时乳液涂膜的初始分解温度提高了77 ~ 92℃,热稳定性也明显提高,说明此方法合成的含量丙乳液可作为一类具有优良疏水性及低表面能的功能材料得以应用.","authors":[{"authorName":"赵苑","id":"0ba366cc-6410-4cc8-8805-03d4092d25da","originalAuthorName":"赵苑"},{"authorName":"刘伟区","id":"c7803e6a-7420-4448-8b39-732b7ac86955","originalAuthorName":"刘伟区"},{"authorName":"闫振龙","id":"22f44d1d-3c74-4fd3-8a9d-ed2479a00c05","originalAuthorName":"闫振龙"}],"doi":"10.3969/j.issn.0253-4312.2012.09.001","fpage":"1","id":"57f14ec6-c74b-4779-a57f-dbaf1b96bf0f","issue":"9","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"225eb216-1836-4905-a032-2af895382960","keyword":"长链聚氧烷","originalKeyword":"长链聚硅氧烷"},{"id":"8589ee8e-0c99-41fa-8512-daaf81bdd469","keyword":"含氟(甲基)丙烯酸酯聚合物","originalKeyword":"含氟(甲基)丙烯酸酯聚合物"},{"id":"57f259a8-cd16-4522-977d-28fea82913cf","keyword":"乳液","originalKeyword":"乳液"},{"id":"d09cedb1-1c41-4761-8cb7-fc02dcf067bc","keyword":"含量","originalKeyword":"高硅含量"}],"language":"zh","publisherId":"tlgy201209001","title":"有机改性含氟(甲基)丙烯酸酯聚合物乳液的制备及其性能研究","volume":"42","year":"2012"},{"abstractinfo":"利用甲基丙烯酰氧基丙基三甲氧基硅烷(MPS)的烷氧基与氯硅烷(CMS)的取代反应,合成了具有支化结构的含量反应性有机单体甲基丙烯酰氧基丙基三(三甲基氧基)硅烷(MATS),并用1H-NMR、FT-IR对其结构进行了表征.以MATS为功能性单体,与丙烯酸酯类单体进行乳液共聚合,制得了稳定的含量丙乳液.对乳液聚合物的力学性能、表面接触角、吸水率等的测试结果表明,MATS分子中的支化型大体积疏水基团能有效提高共聚物的有机含量,显著降低聚合物的表面能,提高其耐水性和力学性能,可制得一类具有优良疏水性及低表面能的功能材料.","authors":[{"authorName":"唐敏锋","id":"b31f4af4-9c54-4e5d-a1cb-ace840646ca4","originalAuthorName":"唐敏锋"},{"authorName":"范晓东","id":"a3b79490-de16-4a85-9358-5d17b3712227","originalAuthorName":"范晓东"},{"authorName":"王召娣","id":"f743e85b-c66d-4214-9578-360aa4bc62db","originalAuthorName":"王召娣"},{"authorName":"刘祥","id":"ad9a46c2-04cd-4208-af80-4f132d19927e","originalAuthorName":"刘祥"}],"doi":"","fpage":"44","id":"b96ec8e3-e3a8-44ed-a83f-6fce53946134","issue":"1","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"290ed336-192b-43fb-941f-a3faa2b29ad6","keyword":"支化型有机单体","originalKeyword":"支化型有机硅单体"},{"id":"d486274c-fe84-4af5-805d-ff2fde7e98e1","keyword":"含量","originalKeyword":"高硅含量"},{"id":"443d3f58-9059-4805-bd09-33f7059c02f5","keyword":"丙乳液","originalKeyword":"硅丙乳液"}],"language":"zh","publisherId":"gfzclkxygc200601011","title":"新型支化有机单体的合成及其丙乳液的研究","volume":"22","year":"2006"},{"abstractinfo":"将改性硅溶胶添加到聚丙烯酸酯乳液中制备含量SiO2/聚丙烯酸酯复合乳液(SiO2/PA).研究了硅溶胶用量对SiO2/PA乳液及涂膜性能的影响,结果发现SiO2/PA复合乳液的SiO2含量高达48%,贮存稳定性好,平均粒径为170 ~180 nm.随着硅溶胶与聚丙烯酸酯乳液配比的增大,涂膜的耐水性、耐醇性、摆杆硬度和拉伸强度都有所提高.扫描电子显微镜(SEM)测试发现含量涂膜表面平整致密,TGA分析表明SiO2/PA杂合涂膜热稳定性良好.","authors":[{"authorName":"叶光宝","id":"d736f007-5140-47e5-ae81-6c3df689447a","originalAuthorName":"叶光宝"},{"authorName":"瞿金清","id":"7ed88c79-0cac-4f07-a2dc-23d5b81e69da","originalAuthorName":"瞿金清"}],"doi":"","fpage":"44","id":"9ea28209-83bf-4959-9c5c-af7efe4f7455","issue":"4","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"b62a53af-0c9e-4e43-a306-d53736e6d38e","keyword":"硅溶胶","originalKeyword":"硅溶胶"},{"id":"9d468eff-7404-44d9-89e9-e37d70f1d8eb","keyword":"硅烷偶联剂","originalKeyword":"硅烷偶联剂"},{"id":"894fe131-c08c-4eb5-9551-b73c734385cb","keyword":"SiO2/PA复合乳液","originalKeyword":"SiO2/PA复合乳液"}],"language":"zh","publisherId":"tlgy201304009","title":"含量水性木器涂料的制备与性能","volume":"43","year":"2013"},{"abstractinfo":"针对航空航天电子封装用轻质铝合金材料,采用空气雾化水冷与真空包套热挤压工艺相结合的方法,制备了Al-30Si和Al-40Si铝合金,并利用金相显微镜、万能电子拉伸机、差热分析仪、TR-2热物性测试仪等设备系统测试和分析了该材料的显微组织、力学和热物理性能.结果表明:随着合金中含量的增加,经热挤压后的相尺寸相对要粗大一些;材料的热导率呈下降趋势,热导性能下降的幅度会随Si含量的增加而加大;热膨胀系数下降;材料的抗拉强度下降.","authors":[{"authorName":"杨伏良","id":"50a78ce7-b586-4045-bd52-0e62246faefb","originalAuthorName":"杨伏良"},{"authorName":"甘卫平","id":"f41e8558-5d97-49d0-b181-5b0f1d4c4b6e","originalAuthorName":"甘卫平"},{"authorName":"陈招科","id":"f1cecef7-3ee7-45b3-9469-fea6a5c2c044","originalAuthorName":"陈招科"}],"doi":"","fpage":"98","id":"7eed562d-2eca-44f4-878b-10fa2b4ea4ab","issue":"2","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"ccb62930-2fba-4661-b784-e3a0e882c6ea","keyword":"快速凝固","originalKeyword":"快速凝固"},{"id":"bc0a6ac5-6fff-407e-9e89-722e70cc27c7","keyword":"真空包套","originalKeyword":"真空包套"},{"id":"14326c64-4b84-4a0f-9e2c-ef565510e320","keyword":"热挤压","originalKeyword":"热挤压"},{"id":"35947a6d-a846-4c3b-b6cb-98a6a32ddd01","keyword":"Al-Si合金","originalKeyword":"Al-Si合金"},{"id":"73e3a5fc-489d-45c2-96c8-7b4405843337","keyword":"气密性","originalKeyword":"气密性"},{"id":"33c9db3a-5ce9-46b6-9c68-5ea70d187b11","keyword":"导热性","originalKeyword":"导热性"},{"id":"9c691993-6537-4207-afc3-3691d9b8348c","keyword":"电子封装","originalKeyword":"电子封装"}],"language":"zh","publisherId":"cldb200502029","title":"含量铝合金材料组织及性能的影响","volume":"19","year":"2005"},{"abstractinfo":"采用差示钼蓝光度法测定粘土和膨润土中高含量,测量范围为35%~ 65%.该法操作简便,快速,准确度较高.","authors":[{"authorName":"张桂华","id":"13aef849-64a3-4d1e-9f05-850ec26f983c","originalAuthorName":"张桂华"},{"authorName":"陈学琴","id":"8ce90a8b-d029-4266-8578-899956348596","originalAuthorName":"陈学琴"},{"authorName":"文红","id":"7cd63b98-2bb5-4078-83a2-4603b9a4ddf8","originalAuthorName":"高文红"}],"doi":"10.3969/j.issn.1000-7571.2000.03.023","fpage":"59","id":"203f3b8f-3440-49d6-bb46-df6538e477ce","issue":"3","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"d77cbd89-bba4-4060-b77d-5cc0d2ba2224","keyword":"含量","originalKeyword":"高含量硅"},{"id":"1b68de74-b9a6-467a-8ec3-eb5efd152fd3","keyword":"差示钼蓝光度法","originalKeyword":"差示硅钼蓝光度法"}],"language":"zh","publisherId":"yjfx200003023","title":"差示钼蓝光度法测定含量","volume":"20","year":"2000"},{"abstractinfo":"合成了有机含量的水性聚氨酯稳定乳液.测量了有机含量对水接触角的影响,并对乳液的稳定性、黏度及涂膜的FT-IR、DSC、机械性能等进行了表征.","authors":[{"authorName":"黄勤","id":"610beb48-11a7-4b44-b506-de4f93234c1c","originalAuthorName":"黄勤"},{"authorName":"张剑秋","id":"9b785841-c8a6-4b20-88ae-4c3430f8cb48","originalAuthorName":"张剑秋"},{"authorName":"封玉凤","id":"936005e5-176b-4730-87b2-651ff33a5068","originalAuthorName":"封玉凤"}],"doi":"10.3969/j.issn.0253-4312.2006.09.008","fpage":"26","id":"1f0af777-8b93-4584-aee6-28e0484d5db4","issue":"9","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 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