{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>,以壬基酚聚氧乙烯醚为修饰剂,水合肼为<span style=\"color:red\">还原</span>剂,在水及甲醇-水体系中,<span style=\"color:red\">还原</span>硫酸铜制备了纳米铜颗粒;利用TEM、XRD、FTIR研究了反应条件对纳米铜颗粒稳定性及粒径的影响.结果表明:在甲醇-水体系中,当壬基酚聚氧乙烯醚与硫酸铜数量(摩尔)比达到1:1时,能在纳米铜颗粒表面形成较紧密的吸附层,有助于提高纳米铜颗粒的稳定性,得到较小粒径(20 nm)的纳米颗粒.","authors":[{"authorName":"陈磊","id":"6e2715fa-c244-4509-a6b0-fdad3960513c","originalAuthorName":"陈磊"},{"authorName":"陈建敏","id":"616c80ce-7f5e-4f80-aead-b14c046e3d0a","originalAuthorName":"陈建敏"},{"authorName":"周惠娣","id":"970cafb0-c93b-4511-9ecd-d3cc5156efed","originalAuthorName":"周惠娣"},{"authorName":"贾均红","id":"4a00496f-0aa4-4075-9119-a4398b9c4180","originalAuthorName":"贾均红"},{"authorName":"皮珺","id":"0b45976a-16be-4a71-9275-348d4bfdb621","originalAuthorName":"皮珺"}],"doi":"10.3969/j.issn.1000-3738.2005.07.021","fpage":"65","id":"48133eeb-c4cb-426c-9465-c2165ba49c60","issue":"7","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"de21282f-824d-40db-986e-73f5efb05bfc","keyword":"纳米","originalKeyword":"纳米"},{"id":"150d0848-42d6-44c7-ba59-3503ef802cf9","keyword":"铜","originalKeyword":"铜"},{"id":"ddcb3265-6684-437e-8034-1535dfe4183e","keyword":"制备","originalKeyword":"制备"},{"id":"63ff7f86-23d0-4f03-a59a-b34e438f3646","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>","originalKeyword":"液相化学还原法"}],"language":"zh","publisherId":"jxgccl200507021","title":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>制备纳米铜颗粒的研究","volume":"29","year":"2005"},{"abstractinfo":"选用<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>,分别在以羧甲基纤维素钠(Carboxymethyl cellulose sodium,CMC)和葡萄糖为<span style=\"color:red\">还原</span>剂的体系下制备纳米银颗粒,并进行了对比分析.通过紫外分光光度计、X射线衍射和透射电镜等测试手段对其进行了表征.结果表明,用CMC体系制备的纳米银粉末平均粒径为20～30nm,为多晶结构；用葡萄糖体系制备的纳米银粉末平均粒径为25～35nm,为面心结构.利用抑菌圈<span style=\"color:red\">法</span>对纳米银的抗茵性能进行测试,结果显示2种体系下制备的纳米银对海洋芽孢杆菌都有很好的抑制作用.","authors":[{"authorName":"孔茉莉","id":"406a916d-23ee-444e-acc1-8efe426e59ff","originalAuthorName":"孔茉莉"},{"authorName":"高冠慧","id":"be331083-2022-4774-ab97-d0dcbd020fe9","originalAuthorName":"高冠慧"},{"authorName":"常雪婷","id":"5f83ad77-6259-43bc-858b-0b46c1d7278e","originalAuthorName":"常雪婷"},{"authorName":"尹衍升","id":"99dc052c-0dcd-45a1-9077-aeecbb72ce0b","originalAuthorName":"尹衍升"}],"doi":"","fpage":"51","id":"8eabb490-0b1b-4e35-9c72-b5b1dee1af6c","issue":"18","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"6f1eee15-611b-403d-8c8d-a675d2734160","keyword":"纳米银","originalKeyword":"纳米银"},{"id":"3cd972f4-2467-4d92-b15b-3b6e68c4c15f","keyword":"羧甲基纤维素钠","originalKeyword":"羧甲基纤维素钠"},{"id":"582dab3b-e79d-4e39-9326-525e9a71111b","keyword":"葡萄糖","originalKeyword":"葡萄糖"},{"id":"33fcd290-7380-47d0-a495-14fc5bdd48ce","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>","originalKeyword":"液相化学还原法"},{"id":"b95d051a-5080-4c9d-bed9-4041588ef47a","keyword":"抑菌性能","originalKeyword":"抑菌性能"}],"language":"zh","publisherId":"cldb201118014","title":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>制备纳米银及抗菌性能研究","volume":"25","year":"2011"},{"abstractinfo":"采用<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>制备出平均粒径为20～35nm的纳米银,并考察不同温度及PVP用量对纳米银性质的影响.结果表明:当硝酸银与PVP的质量比为1∶4、反应温度为30℃时,纳米银的平均粒径最小,为22.4nm,且其团聚程度最小,粒径分布最佳.在压力10MPa、温度200℃、保温30min的烧结条件下,利用制得的纳米银配制焊膏,连接纯度为99.9％的无氧紫铜板,通过扫描电镜(SEM)观察烧结接头截面形貌,可见烧结界面连接紧密,接头组织有孔隙存在.","authors":[{"authorName":"曹洋","id":"50157e60-406b-4fca-a396-f7314dad358e","originalAuthorName":"曹洋"},{"authorName":"刘平","id":"031501aa-abdb-4a91-af5c-b04839ba7bc1","originalAuthorName":"刘平"},{"authorName":"魏红梅","id":"e7ef6856-dd4b-4062-9ea6-e5e89b00ef2c","originalAuthorName":"魏红梅"},{"authorName":"林铁松","id":"f42a033e-cf8c-4eff-9d00-b4c27cc6d52b","originalAuthorName":"林铁松"},{"authorName":"何鹏","id":"74bdd187-3f23-4d70-a080-123ffb22caa9","originalAuthorName":"何鹏"},{"authorName":"顾小龙","id":"bd7f0db7-742d-44ca-a04c-4d1959d7150d","originalAuthorName":"顾小龙"}],"doi":"10.11868/j.issn.1001-4381.2015.04.014","fpage":"79","id":"cfb391a5-3a53-4b95-82aa-3cdcc6676505","issue":"4","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"7a109e1e-ccfb-4486-9602-833aab5c4e15","keyword":"纳米银","originalKeyword":"纳米银"},{"id":"308323fe-0b49-45aa-ae35-4be920484cb0","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>","originalKeyword":"液相化学还原法"},{"id":"8b6ea4f8-376c-404e-bc28-54d5008a89d7","keyword":"低温连接","originalKeyword":"低温连接"}],"language":"zh","publisherId":"clgc201504014","title":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>制备纳米银焊膏及其连接性","volume":"43","year":"2015"},{"abstractinfo":"片状纳米银是一种新型纳米材料,与球形纳米银相比具有更好的导电性、催化性、低温超导性等.近年来,国内外关于片状纳米银制备方法的研究较多,并探讨了<span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>中片状纳米银的形成机理.介绍片状纳米银的<span style=\"color:red\">化学</span>合成方法并分析其特点,概括了片状纳米银的生长机理和影响因素,并简要分析了其工业化生产的制约因素.","authors":[{"authorName":"王春霞","id":"085123f5-75af-47da-8a22-d0073eed0a0c","originalAuthorName":"王春霞"},{"authorName":"李英琳","id":"8791e4bf-e01b-4a48-91a0-41c8cbedc665","originalAuthorName":"李英琳"},{"authorName":"徐磊","id":"8a0e8dd5-cd35-404b-9d64-da08ae0eec88","originalAuthorName":"徐磊"},{"authorName":"周少波","id":"71c9e883-2195-4e4d-9e00-4216959c4b28","originalAuthorName":"周少波"}],"doi":"10.11896/j.issn.1005-023X.2014.23.024","fpage":"113","id":"ad1c2e4e-a072-403d-b8ae-309424b9bee5","issue":"23","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"a717a62e-d234-415b-b1b9-bd2ea42686e2","keyword":"片状纳米银","originalKeyword":"片状纳米银"},{"id":"906cb6b1-662a-489b-98be-25e9ae662ebd","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>","originalKeyword":"液相化学还原法"},{"id":"2320de59-748d-47b1-88db-78de98ec3ce9","keyword":"生长机理","originalKeyword":"生长机理"}],"language":"zh","publisherId":"cldb201423024","title":"片状纳米银的<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span>制备及研究进展","volume":"28","year":"2014"},{"abstractinfo":"采用<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>,在1,2-丙二醇体系中,分别使用吐温-80(Tween-80)、聚乙二醇-6000(PEG-6000)和十二烷基硫酸钠(SDS)与聚乙二醇-6000(PEG-6000)的混合物作为修饰剂,利用1,2-丙二醇<span style=\"color:red\">还原</span>相同母体醋酸镍,制备形貌分别为海绵体、纤维状、雪花状的多晶纳米镍;在水体系中,使用SDS为修饰剂,利用水合肼<span style=\"color:red\">还原</span>相同母体醋酸镍,制备球形多晶纳米镍.通过X射线衍射(XRD)、透射电子显微镜(TEM)、选区电子衍射(SAED)对纳米镍进行表征.利用傅立叶红外(FTIR)分析初步解释不同形貌纳米镍的形成机理.","authors":[{"authorName":"张锡凤","id":"b760a530-c419-4906-ae1b-66322fd1a739","originalAuthorName":"张锡凤"},{"authorName":"程晓农","id":"f2478c87-a27a-4fab-affa-fe0c7315b988","originalAuthorName":"程晓农"},{"authorName":"殷恒波","id":"90862029-d676-43cc-9535-438d5571fabd","originalAuthorName":"殷恒波"},{"authorName":"吴寅寅","id":"23a60e3c-ba7b-48b3-8f27-6c9f6a7e5ae4","originalAuthorName":"吴寅寅"}],"doi":"","fpage":"1700","id":"e36df7d4-b3a5-46ef-9639-b9c012992672","issue":"10","journal":{"abbrevTitle":"ZGYSJSXB","coverImgSrc":"journal/img/cover/ZGYSJSXB.jpg","id":"88","issnPpub":"1004-0609","publisherId":"ZGYSJSXB","title":"中国有色金属学报"},"keywords":[{"id":"5566c8e9-37ca-41e1-9234-71551bb3c90a","keyword":"纳米镍","originalKeyword":"纳米镍"},{"id":"366f1516-839d-44dc-8adc-079530338c0d","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原法</span>","originalKeyword":"液相还原法"},{"id":"9f8b3a5a-e5f3-44f0-9e1e-ea874518eba2","keyword":"吐温-80","originalKeyword":"吐温-80"},{"id":"2136f490-801c-4f76-88ed-0d3ef1ed9ee2","keyword":"聚乙二醇-6000","originalKeyword":"聚乙二醇-6000"},{"id":"f077df64-4bc6-4639-af10-3af97d040e8d","keyword":"十二烷基硫酸钠","originalKeyword":"十二烷基硫酸钠"}],"language":"zh","publisherId":"zgysjsxb200710025","title":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>制备不同形貌的多晶纳米镍","volume":"17","year":"2007"},{"abstractinfo":"以硫酸铜为铜源,水合肼为<span style=\"color:red\">还原</span>剂,聚乙烯吡咯烷酮(PVP)为保护剂,十六烷基三甲基溴化铵(CTAB)为分散剂,采用<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>制备纳米铜溶胶.通过单因素<span style=\"color:red\">法</span>考察了体系的反应温度、PVP用量、CTAB用量和水合肼浓度等对纳米铜溶胶合成的影响,获得制备高分散稳定纳米铜溶胶的适宜条件.纳米铜溶胶通过紫外-可见吸收光谱(UV-Vis)和透射电镜(TEM)表征,而铜纳米粒子(CuNPs)则通过红外光谱(FTIR)、X射线衍射(XRD)和热分析(TG)检测.研究结果表明:纳米铜溶胶具有较高的稳定性；CuNPs的粒径分布为10～30 nm,其表面吸附有少量的保护剂PVP,有利于防止CuNPs的团聚及氧化,使其具有良好的分散性.","authors":[{"authorName":"杨海君","id":"8c394d54-fa74-4893-8824-655c872f5b6f","originalAuthorName":"杨海君"},{"authorName":"田恐虎","id":"a068c1a2-4c4c-4977-badf-31ecaf89c0eb","originalAuthorName":"田恐虎"},{"authorName":"刘才林","id":"898c1ab7-d4f7-47ab-8b8a-1437a62e4735","originalAuthorName":"刘才林"},{"authorName":"任先艳","id":"302dcc87-65fe-495d-b141-947fc3f087af","originalAuthorName":"任先艳"},{"authorName":"邓永俊","id":"9db3310a-ffef-4c81-aa48-00001724d9fc","originalAuthorName":"邓永俊"}],"doi":"","fpage":"32","id":"5fd2e9fa-57b1-4ef6-a19f-a3f53c2734e9","issue":"8","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"99540201-a25d-4049-a532-ab92418bc26f","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原</span>","originalKeyword":"液相化学还原"},{"id":"f5b5b4f6-948e-4fa7-a5e3-79c5d32a5fb2","keyword":"铜纳米粒子","originalKeyword":"铜纳米粒子"},{"id":"28435eb8-25c9-41e2-9dae-c347b431ba26","keyword":"溶胶","originalKeyword":"溶胶"}],"language":"zh","publisherId":"cldb201308010","title":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>制备分散稳定的纳米铜溶胶","volume":"27","year":"2013"},{"abstractinfo":"研究了<span style=\"color:red\">化学</span><span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原</span>反应制备纳米铁粉过程中碱性介质加入对粒子晶化程度、大小、磁性能以及粒子聚集形态的影响.结果表明,加入碱性介质影响<span style=\"color:red\">还原</span>反应过程,在其它条件相同时,未加碱性介质所制得的纳米铁粉有一定程度的晶化,且粒子相对较大;而加入适当碱性介质所制得的纳米铁粉为非晶态,且粒子明显小于未加碱性介质时.晶化程度的差别导致两者的磁性能明显不同,并使两者粒子具有不同的微观聚集状态.","authors":[{"authorName":"刘颖","id":"9d62cb3d-f5fb-4e13-a63e-eed2945362eb","originalAuthorName":"刘颖"},{"authorName":"赵修臣","id":"ba51718d-8040-45be-a2c4-cbc3952129ba","originalAuthorName":"赵修臣"},{"authorName":"余智勇","id":"7f51b0a4-61fd-4dbd-a580-e8dc228b991d","originalAuthorName":"余智勇"},{"authorName":"邹鑫","id":"7361ac52-fcaf-473d-be90-fb89a21fb460","originalAuthorName":"邹鑫"},{"authorName":"程荆卫","id":"eaf1eafa-4d5d-4a63-9499-ffb4703afbea","originalAuthorName":"程荆卫"}],"doi":"10.3969/j.issn.1000-3738.2003.11.002","fpage":"4","id":"13cb9279-bddb-48bc-b05e-20690f09e24e","issue":"11","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"e18055b0-c020-4ab1-950c-097f4c416264","keyword":"纳米粒子","originalKeyword":"纳米粒子"},{"id":"f89be9b0-f8eb-483c-8ed5-4aea9e1098ab","keyword":"纯铁","originalKeyword":"纯铁"},{"id":"78a90991-f496-4344-bd93-56e83e453a75","keyword":"<span style=\"color:red\">化学</span>制备","originalKeyword":"化学制备"}],"language":"zh","publisherId":"jxgccl200311002","title":"添加碱性介质对用<span style=\"color:red\">化学</span><span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原法</span>制备纳米铁粉的影响","volume":"27","year":"2003"},{"abstractinfo":"以PVP为表面活性剂，甲酸铵为<span style=\"color:red\">还原</span>剂，采用<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原法</span>制备了纳米银颗粒。采用X射线衍射(XRD)、透射电子显微镜(TEM)和紫外-可见光吸收光谱(UV-Vis)对所制备样品进行表征。结果显示：当PVP与AgNO3的质量比为2.2：1，陈化时间24 h，得到立方块和六棱柱的银混合颗粒。","authors":[{"authorName":"王春霞","id":"d29e6d5b-74bc-4c01-a9e7-517fd0482d7f","originalAuthorName":"王春霞"},{"authorName":"李英琳","id":"94790c06-15cb-40a6-9a45-0bba3eff3ecd","originalAuthorName":"李英琳"},{"authorName":"徐磊","id":"c49892a5-bb29-4c33-a39c-fde493c39a93","originalAuthorName":"徐磊"}],"doi":"","fpage":"30","id":"963be70b-34c6-49f1-87b8-465207b6a4bf","issue":"4","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"b94eb968-00d2-4fd6-b0e0-6dc0572b07f3","keyword":"纳米<span style=\"color:red\">化学</span>","originalKeyword":"纳米化学"},{"id":"c0ec7c6f-4661-4694-9e7d-53d071b0ff89","keyword":"纳米银","originalKeyword":"纳米银"},{"id":"2ae3268d-229e-467b-bc4e-becee2cbf25b","keyword":"<span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>","originalKeyword":"化学还原法"},{"id":"5052ab40-c418-476f-b17f-046769daec84","keyword":"PVP","originalKeyword":"PVP"},{"id":"a90caa3c-be58-4fb1-a449-07b229870827","keyword":"陈化时间","originalKeyword":"陈化时间"}],"language":"zh","publisherId":"gjs201404007","title":"PVP保护下纳米银颗粒的<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">化学</span><span style=\"color:red\">还原法</span>制备及表征","volume":"","year":"2014"},{"abstractinfo":"用<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原法</span>制备纳米尺寸Ag-50Ni粉末而后热压制得其纳米块体合金,并与传统粉末冶金法制备的粗晶Ag-50Ni合金对比研究了它们在含Cl-介质中的腐蚀电<span style=\"color:red\">化学</span>行为.结果表明:合金粉末平均粒径约为45nm,真空热压后,晶粒有所长大,但仍为纳米尺度;随Cl-浓度增加,两种尺寸Ag-50Ni合金的腐蚀电流密度均增加,腐蚀速度加快;晶粒尺寸降低后,腐蚀电流密度略有增加,腐蚀速度变快;当极化电位增到某一程度后,两种尺寸Ag-50Ni合金均出现钝化;纳米尺寸Ag-50Ni合金在含0.02mol/L Cl-介质中的交流阻抗谱由双容抗弧组成,其余均由单容抗弧组成,腐蚀受电<span style=\"color:red\">化学</span>反应控制.","authors":[{"authorName":"曹中秋","id":"30f332e5-75da-4254-8f4b-7bd6a132d809","originalAuthorName":"曹中秋"},{"authorName":"祝溪明","id":"fd0fff5f-c201-4791-ac3a-268bfcadf6af","originalAuthorName":"祝溪明"},{"authorName":"代丽","id":"ab46dc83-149d-4262-9461-c28b9057a597","originalAuthorName":"代丽"},{"authorName":"付雅君","id":"e203bc60-0997-4617-99ef-2bb55125cff9","originalAuthorName":"付雅君"},{"authorName":"李凤春","id":"9b127073-8f4b-4bc0-8211-1394879a2073","originalAuthorName":"李凤春"}],"doi":"10.3969/j.issn.1002-6495.2009.02.028","fpage":"161","id":"aaaaf5af-b711-439a-b952-f718bc7025b3","issue":"2","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[{"id":"eabe3bf8-f3cd-4193-aee8-fd9cfd788409","keyword":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原</span>","originalKeyword":"液相还原"},{"id":"b74666fc-2aad-42d6-8899-0a738d86f46a","keyword":"Ag-Ni合金","originalKeyword":"Ag-Ni合金"},{"id":"0380e45b-b33b-491a-9b82-005e93aae0f5","keyword":"纳米晶","originalKeyword":"纳米晶"},{"id":"a5cb54ca-702a-44ea-9a78-fd27963a7354","keyword":"腐蚀电<span style=\"color:red\">化学</span>","originalKeyword":"腐蚀电化学"}],"language":"zh","publisherId":"fskxyfhjs200902028","title":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原法</span>并热压制备的纳米晶Ag·50Ni合金在含Cl-介质中腐蚀电<span style=\"color:red\">化学</span>行为研究","volume":"21","year":"2009"},{"abstractinfo":"在<span style=\"color:red\">液</span>相联氨<span style=\"color:red\">还原法</span>工艺基础上,对<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原法</span>制备纳米银粉的<span style=\"color:red\">还原</span>反应条件(体系温度、分散剂、反应物浓度)进行了研究,得到了优化的反应条件:反应体系温度70℃,反应物浓度[Ag[NH3]2+]=0.02 mol/1和特定的分散剂2#.且生产出平均粒径约为50 nm、大小均匀、灰白色的球状银粉.","authors":[{"authorName":"廖立","id":"473b91a5-6c47-49b3-b20c-05674f4f523c","originalAuthorName":"廖立"},{"authorName":"熊继","id":"4b3aeb53-01b1-4b35-a201-67a083ce3c77","originalAuthorName":"熊继"},{"authorName":"谢克难","id":"0b87850d-fe71-479c-8d45-1c3600c69e41","originalAuthorName":"谢克难"}],"doi":"","fpage":"558","id":"5ae9add9-6a7f-4644-a56c-9a1ccf5de688","issue":"5","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"4d586160-5de7-4497-b879-8f7eae764aa2","keyword":"纳米银","originalKeyword":"纳米银"},{"id":"b9e7e511-9241-42c6-9df1-8885867dd243","keyword":"水合联氨","originalKeyword":"水合联氨"},{"id":"849e59e7-85f1-49e3-9781-06a93d47d5f2","keyword":"<span style=\"color:red\">还原</span>","originalKeyword":"还原"},{"id":"a14bab58-1644-4dee-98b1-bcab3c10f709","keyword":"制备","originalKeyword":"制备"}],"language":"zh","publisherId":"xyjsclygc200405027","title":"<span style=\"color:red\">液</span><span style=\"color:red\">相</span><span style=\"color:red\">还原法</span>制备纳米银粉的研究","volume":"33","year":"2004"}],"totalpage":9423,"totalrecord":94224}