{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"用恒流<span style=\"color:red\">电解</span><span style=\"color:red\">相</span><span style=\"color:red\">萃取</span>技术成功地提取了NDG-2镍基耐磨堆焊合金中主要硬质<span style=\"color:red\">相</span>Cr7C3、NiCrWSi,用XRD、SEM分析观察了堆焊合金中各种硬质<span style=\"color:red\">相</span>结构及结晶立体形态,探讨了硬质相对合金耐磨性能的影响.","authors":[{"authorName":"线恒泽","id":"0ef23b7f-2377-4ae4-b071-a48487c55a18","originalAuthorName":"线恒泽"}],"doi":"","fpage":"2230","id":"d772daec-7dfb-44d8-acfa-0690c6e239c8","issue":"z1","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"bebbe1be-02ef-4a5e-b672-3b6e83138d74","keyword":"耐磨堆焊","originalKeyword":"耐磨堆焊"},{"id":"69a36cc9-9d05-43fc-b5fa-8ee9d2066d9c","keyword":"<span style=\"color:red\">电解</span><span style=\"color:red\">相</span><span style=\"color:red\">萃取</span>","originalKeyword":"电解相萃取"},{"id":"6346e4ef-506d-49f0-953c-f603520b53b6","keyword":"硬质<span style=\"color:red\">相</span>","originalKeyword":"硬质相"},{"id":"9f6d2a33-4cf1-401c-9f11-73b03ae24854","keyword":"镍基合金","originalKeyword":"镍基合金"}],"language":"zh","publisherId":"gncl2004z1619","title":"NDG-2镍基耐磨堆焊合金硬质<span style=\"color:red\">相</span>的研究","volume":"35","year":"2004"},{"abstractinfo":"通过对热处理态FGH95合金进行<span style=\"color:red\">电解</span><span style=\"color:red\">萃取</span>,组织形貌观察及XRD分析,研究了FGH95合金的<span style=\"color:red\">相</span>组成及γ′<span style=\"color:red\">相</span>的粒度分布.结果表明,经1140℃固溶和时效处理后,合金的组织结构由γ′,γ<span style=\"color:red\">相</span>,(Nb,Ti)C、( Nb,W)B2,Nb13B2和Cr23C6等碳、硼化物组成,其中合金中γ′,γ基体<span style=\"color:red\">相</span>的质量分数分别为47.8％和51.2％,其碳、硼化物的质量分数约为1％.合金中晶内为细小γ′<span style=\"color:red\">相</span>弥散分布,而粗大γ′相沿较宽的颗粒边界区域不连续析出；其中,在36～60nm之间的γ′<span style=\"color:red\">相</span>粒子质量分数为30.6％,在60～96nm之间的γ′<span style=\"color:red\">相</span>粒子质量分数为29.1％,γ′<span style=\"color:red\">相</span>的结构组成式为:(Ni0.896C00.055Cr0.017Fe0.031)3 (Ti0.224Nb0.134Al0.473Mo0.038W0.066 Cr0.064).","authors":[{"authorName":"李晶晶","id":"47f055a6-2f1c-48b5-8b04-f4aae35a43d6","originalAuthorName":"李晶晶"},{"authorName":"田素贵","id":"f85696be-3fb3-4fca-b195-5c7e18600ad3","originalAuthorName":"田素贵"},{"authorName":"谢君","id":"d9621530-e4e7-4f02-ba7f-265375a6b125","originalAuthorName":"谢君"},{"authorName":"周晓明","id":"46d0b243-7db1-41ad-a967-4a0e9d7d96db","originalAuthorName":"周晓明"}],"doi":"10.3969/j.issn.1001-4381.2010.z1.044","fpage":"206","id":"4c24abf0-32fa-4ac0-8d9c-82ceacafe0b9","issue":"z1","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"7df959ad-bbe6-4052-b688-73d3946ac037","keyword":"FGH95镍基合金","originalKeyword":"FGH95镍基合金"},{"id":"0a26320a-eb8d-4ebd-86ec-119fab4c30a7","keyword":"<span style=\"color:red\">电解</span><span style=\"color:red\">萃取</span>","originalKeyword":"电解萃取"},{"id":"3112ff8a-bbe8-4456-bfec-aa8993bb53a5","keyword":"相分析","originalKeyword":"相分析"},{"id":"bc3a41b8-42f6-417f-969b-449d528a67f8","keyword":"粒度分布","originalKeyword":"粒度分布"}],"language":"zh","publisherId":"clgc2010z1044","title":"FGH95镍基合金的<span style=\"color:red\">电解</span><span style=\"color:red\">萃取</span>及<span style=\"color:red\">相</span>组成与分布特征","volume":"","year":"2010"},{"abstractinfo":"固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>是基于<span style=\"color:red\">萃取</span>涂层与样品之间的吸附/溶解-解吸平衡而建立起来的集进样、<span style=\"color:red\">萃取</span>、浓缩功能于一体的技术。综述了固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>技术的最新发展动态,介绍了管内(in-tube)固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>、新型<span style=\"color:red\">萃取</span>头以及固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>与其他分析技术的联用情况。","authors":[{"authorName":"马继平","id":"2eb37d6d-66f1-42b2-b917-6da159add240","originalAuthorName":"马继平"},{"authorName":"王涵文","id":"c9e328e9-660b-4bdf-859b-82370a2979bf","originalAuthorName":"王涵文"},{"authorName":"关亚风","id":"18923469-e3f8-41bb-8f84-4b504b0ef2ee","originalAuthorName":"关亚风"}],"doi":"10.3321/j.issn:1000-8713.2002.01.004","fpage":"16","id":"5e233178-54a4-4b4f-ac53-f73a97e8dad8","issue":"1","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"61563703-5eaf-4e64-8bdc-4096e3b8a467","keyword":"固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>","originalKeyword":"固相微萃取"},{"id":"402eb729-fb30-4613-a30c-c71005bfde95","keyword":"样品预处理","originalKeyword":"样品预处理"},{"id":"31822e7b-e1bd-4d38-a549-673fe035d030","keyword":"吸附-脱附平衡","originalKeyword":"吸附-脱附平衡"},{"id":"c73d0651-3cf4-4bae-a903-14c0ee002710","keyword":"综述","originalKeyword":"综述"}],"language":"zh","publisherId":"sp200201004","title":"固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>新技术","volume":"20","year":"2002"},{"abstractinfo":"首次提出<span style=\"color:red\">电解</span>控制酸度<span style=\"color:red\">萃取</span>法,探讨了该法<span style=\"color:red\">萃取</span>反应机理.并用该法研究了HEH(EHP)从氯化稀土混合溶液中<span style=\"color:red\">萃取</span>La(Ⅲ)、Ce(Ⅲ)、Pr(Ⅲ)和Nd(Ⅲ)过程中各元素在HEH(EHP)-酸性<span style=\"color:red\">萃取</span>体系中的分离系数(β)、<span style=\"color:red\">萃取</span>速率(r)和电流效率(η1)等的变化规律.","authors":[{"authorName":"木合塔尔·依米提","id":"3daadc11-d27c-4016-9100-140516848388","originalAuthorName":"木合塔尔·依米提"},{"authorName":"孙都成","id":"ecf9c3e1-ecc8-4771-a49e-e9882de66f5a","originalAuthorName":"孙都成"},{"authorName":"夏熙","id":"c85e74a6-c2ef-419f-888f-fe4843edf507","originalAuthorName":"夏熙"},{"authorName":"帕提古丽·依明","id":"fa898c65-8a9f-452d-aa59-9647786dff86","originalAuthorName":"帕提古丽·依明"}],"doi":"10.3969/j.issn.1004-0277.2002.06.008","fpage":"27","id":"025edbcb-533d-4d53-9047-fd38976fb683","issue":"6","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"a3cbeaf6-99dd-4277-9f0f-9cb856d04df6","keyword":"<span style=\"color:red\">电解</span><span style=\"color:red\">萃取</span>","originalKeyword":"电解萃取"},{"id":"55275d62-5f77-457b-b45d-292db72f9200","keyword":"稀土","originalKeyword":"稀土"},{"id":"f04a9d05-efe8-4b81-8986-55e8e638a5c3","keyword":"HEH(EHP)","originalKeyword":"HEH(EHP)"}],"language":"zh","publisherId":"xitu200206008","title":"<span style=\"color:red\">电解</span>控制酸度<span style=\"color:red\">萃取</span>法研究HEH(EHP)从氯化稀土溶液中<span style=\"color:red\">萃取</span>La(Ⅲ)、Ce(Ⅲ)、Pr(Ⅲ)和Nd(Ⅲ)","volume":"23","year":"2002"},{"abstractinfo":"介绍了金<span style=\"color:red\">电解</span>与溶剂<span style=\"color:red\">萃取</span>两种工艺的原则流程;对两种工艺在原料的适应性、过程控制、工艺设备及配置、主要技术经济指标及投资等方面进行了比较分析.","authors":[{"authorName":"刘勇","id":"c8781cdc-5f22-45bb-bd37-36b500e5f561","originalAuthorName":"刘勇"},{"authorName":"阳振球","id":"9fed9d8c-a78c-4b09-bf7b-08955a85b983","originalAuthorName":"阳振球"},{"authorName":"杨天足","id":"baa1f977-5ba1-4bdc-9d88-911aa9775bc1","originalAuthorName":"杨天足"}],"doi":"10.3969/j.issn.1001-1277.2007.06.012","fpage":"42","id":"e726aea0-6b0c-4495-9e04-d26d97185ed9","issue":"6","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"e73cd504-f236-41f3-bdad-db1d60aeb5d5","keyword":"金","originalKeyword":"金"},{"id":"6932f3f3-8504-4fed-98ab-08deaa8ec8e7","keyword":"精炼","originalKeyword":"精炼"},{"id":"410411bf-94a4-48f7-b64f-9ebb5f2f99a2","keyword":"<span style=\"color:red\">电解</span>","originalKeyword":"电解"},{"id":"8d01e070-0d62-483a-8172-8cc10921d2d4","keyword":"溶剂<span style=\"color:red\">萃取</span>","originalKeyword":"溶剂萃取"}],"language":"zh","publisherId":"huangj200706012","title":"金<span style=\"color:red\">电解</span>与溶剂<span style=\"color:red\">萃取</span>精炼工艺比较分析","volume":"28","year":"2007"},{"abstractinfo":"对固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>(SPME)的固定相涂层的发展进行了综述。阐述了商品化和非商品化涂层的各自特点，并对涂层的选择性和SPME技术作了简单的介绍。","authors":[{"authorName":"黄悯嘉","id":"51f3bd2c-3725-4752-9b66-50f97db4394a","originalAuthorName":"黄悯嘉"},{"authorName":"游静","id":"31ee33d5-2414-480f-a1a5-a008351a2f08","originalAuthorName":"游静"},{"authorName":"梁冰","id":"44d5185b-a6dc-4736-86d3-54c2093f1048","originalAuthorName":"梁冰"},{"authorName":"欧庆瑜","id":"b1363e98-5df1-4db9-9bb5-00cc4e5d8267","originalAuthorName":"欧庆瑜"}],"doi":"10.3321/j.issn:1000-8713.2001.04.007","fpage":"314","id":"6fb45c05-6110-4407-9c53-ff5cae8ad88d","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"4c0c7d95-349e-45af-a52c-b37986791e4f","keyword":"固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>","originalKeyword":"固相微萃取"},{"id":"71fc5f8f-b598-42d9-96fb-553706c2ce78","keyword":"涂层","originalKeyword":"涂层"},{"id":"22230363-855d-457d-bbde-46378db90128","keyword":"进展","originalKeyword":"进展"}],"language":"zh","publisherId":"sp200104007","title":"固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>的涂层进展","volume":"19","year":"2001"},{"abstractinfo":"在阐述固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>的平衡理论及非平衡理论基础上,重点探讨了<span style=\"color:red\">萃取</span>头的制备技术和相关试验方法的进展.除了介绍商品化通用<span style=\"color:red\">萃取</span>头的制备技术外,还论述了溶胶-凝胶法、电沉积法、碳素基体吸附法、高温环氧树脂固定法等新的制备技术;探讨了固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>试验方法中<span style=\"color:red\">萃取</span>模式和<span style=\"color:red\">萃取</span>头的选择、<span style=\"color:red\">萃取</span>条件优化以及方法的灵敏度、精度、自动化等的评价;进一步总结了固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>的应用现状,对固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>的发展方向作了展望.","authors":[{"authorName":"徐溢","id":"f93fac3a-bc78-40c5-8200-2a977f12f35b","originalAuthorName":"徐溢"},{"authorName":"付钰洁","id":"0a286389-e502-4a10-a1c3-4b3dd4e74e99","originalAuthorName":"付钰洁"}],"doi":"10.3321/j.issn:1000-8713.2004.05.015","fpage":"528","id":"6c17af9c-8c0c-4adb-b77d-e6c0fd145b78","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"1d5fcafb-0e72-4e06-9907-3625b4e38ed7","keyword":"固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span>","originalKeyword":"固相微萃取"},{"id":"17841a09-21e3-42a2-bb37-94083ce57c4d","keyword":"<span style=\"color:red\">萃取</span>头制备","originalKeyword":"萃取头制备"},{"id":"1d6beafb-8d14-46a4-892d-cdee55450bd9","keyword":"试验方法","originalKeyword":"试验方法"}],"language":"zh","publisherId":"sp200405015","title":"固<span style=\"color:red\">相</span>微<span style=\"color:red\">萃取</span><span style=\"color:red\">萃取</span>头制备技术及试验方法的进展","volume":"22","year":"2004"},{"abstractinfo":"研究了基于与水互溶的普通有机溶剂的双水<span style=\"color:red\">相</span><span style=\"color:red\">萃取</span>体系，并考察了不同种类盐分相能力的差异及不同种类有机溶剂的分相情况.双水相分相受许多因素影响，包括溶剂、盐的类型及浓度.根据分相后有机溶剂<span style=\"color:red\">相</span>的体积变化，双水<span style=\"color:red\">相</span>体系存在3种分相类型：Ⅰ型(V始＜V终)、Ⅱ型(V始＞V终)和Ⅲ型(兼具Ⅰ、Ⅱ型).","authors":[{"authorName":"王志华","id":"e10eb94a-4611-4061-b16b-119362a82ad8","originalAuthorName":"王志华"},{"authorName":"马会民","id":"dfb7e9ca-8cec-4c16-9645-982192a04d84","originalAuthorName":"马会民"},{"authorName":"马泉莉","id":"e40673ad-0e9f-4595-aec0-29f90a90a892","originalAuthorName":"马泉莉"},{"authorName":"苏美红","id":"d0327f14-aacd-4179-9b95-96df6f839e48","originalAuthorName":"苏美红"},{"authorName":"梁树权","id":"77b5f07d-846f-4472-81b1-59fdf6ebbbf3","originalAuthorName":"梁树权"}],"doi":"10.3969/j.issn.1000-0518.2001.03.001","fpage":"173","id":"138c91c5-5bff-4e0e-8259-5def4328b4e5","issue":"3","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"ed2b154d-9826-413d-a12d-d760abd3724e","keyword":"有机溶剂","originalKeyword":"有机溶剂"},{"id":"2ddef27e-3ea5-4baf-9bbe-5270a51d0718","keyword":"双水<span style=\"color:red\">相</span><span style=\"color:red\">萃取</span>体系","originalKeyword":"双水相萃取体系"},{"id":"e48b356a-d21c-46d3-a6ac-d74d1f9a6061","keyword":"分相机理","originalKeyword":"分相机理"}],"language":"zh","publisherId":"yyhx200103001","title":"双水<span style=\"color:red\">相</span><span style=\"color:red\">萃取</span>体系的研究","volume":"18","year":"2001"},{"abstractinfo":"利用无孔脲醛树脂-ZrO2复合物微球表面的酰胺键与三嗪染料-活性艳蓝X-BR分子中三嗪环上的活泼氯反应,将染料键合到微球表面,合成了一种新型无孔染料配体固<span style=\"color:red\">相</span><span style=\"color:red\">萃取</span>剂.以牛血清白蛋白(BSA)为样品,考察了该<span style=\"color:red\">萃取</span>剂对BSA静态吸附的动力学和热力学性能.结果表明,该<span style=\"color:red\">萃取</span>剂对BSA的饱和<span style=\"color:red\">萃取</span>量达到34.5 mg/g,可以用Langmuir吸附等温方程进行描述;在pH=4.6时,BSA的<span style=\"color:red\">萃取</span>量达到最大;实验进行2 h后,BSA的<span style=\"color:red\">萃取</span>量达到最大值的80%,<span style=\"color:red\">萃取</span>的蛋白很容易用1 mol/L KSCN进行洗脱,洗脱率达93.5%,并且洗脱实验的重现性较好.由此可见,该<span style=\"color:red\">萃取</span>剂可用于生物大分子HPLC分析柱前干扰蛋白的除去和目标蛋白的富集.","authors":[{"authorName":"骆红琴","id":"02cb7e2a-414a-4dd9-add9-2206d735ba0b","originalAuthorName":"骆红琴"},{"authorName":"李乃瑄","id":"e86f4a8b-0394-4da2-9279-8f1c0eb8f51b","originalAuthorName":"李乃瑄"}],"doi":"10.3969/j.issn.1000-0518.2007.05.021","fpage":"585","id":"786cabb8-edfb-4b56-bb84-55609563bedb","issue":"5","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"08604709-ccb1-4a3d-ad16-e9666b864da9","keyword":"脲醛树脂-ZrO2复合微球","originalKeyword":"脲醛树脂-ZrO2复合微球"},{"id":"361968b6-57e8-49e0-8ae4-ed7ab97418e6","keyword":"染料配体","originalKeyword":"染料配体"},{"id":"3143553a-f41d-479c-bc27-eae2f00e13f3","keyword":"固<span style=\"color:red\">相</span><span style=\"color:red\">萃取</span>剂","originalKeyword":"固相萃取剂"}],"language":"zh","publisherId":"yyhx200705021","title":"染料配体固<span style=\"color:red\">相</span><span style=\"color:red\">萃取</span>剂的制备及<span style=\"color:red\">萃取</span>性能","volume":"24","year":"2007"},{"abstractinfo":"提出了模拟水<span style=\"color:red\">相</span>进料理想分馏<span style=\"color:red\">萃取</span>平衡态的极限法.只需给定原料组成和分离系数,极限法可以输出理想分馏<span style=\"color:red\">萃取</span>平衡态的组分分布、<span style=\"color:red\">萃取</span>段级数和洗涤段级数.极限法输出的平衡态组分分布特征,与其他方法的结果相一致.研究发现,理想分馏<span style=\"color:red\">萃取</span>的组分分布遵循递增规律、递减规律和中值规律.极限法输出的<span style=\"color:red\">萃取</span>段级数、洗涤段级数和总级数与串级<span style=\"color:red\">萃取</span>理论相吻合,级数误差不超过1级.","authors":[{"authorName":"钟学明","id":"c42716a1-1e75-4993-a521-d72482abbe6d","originalAuthorName":"钟学明"}],"doi":"10.3969/j.issn.1004-0277.2010.05.010","fpage":"48","id":"e851ad4d-7f06-4e7b-815b-ca4bc2c7d762","issue":"5","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"fb308987-ff95-4710-b565-6240fd107f4c","keyword":"分馏<span style=\"color:red\">萃取</span>","originalKeyword":"分馏萃取"},{"id":"1acdccbe-ed49-4c7f-9802-b6940fd5caea","keyword":"模拟","originalKeyword":"模拟"},{"id":"7e0144fb-98ec-4c4f-be6a-1fd4ba67ed3f","keyword":"极限法","originalKeyword":"极限法"},{"id":"1e5e94a4-13a8-46a1-b751-d10e24a513d0","keyword":"组分分布","originalKeyword":"组分分布"},{"id":"93a1a7ea-38a7-4ae3-af41-d6abd1138060","keyword":"级数","originalKeyword":"级数"}],"language":"zh","publisherId":"xitu201005010","title":"水<span style=\"color:red\">相</span>进料理想分馏<span style=\"color:red\">萃取</span>的模拟","volume":"31","year":"2010"}],"totalpage":4419,"totalrecord":44183}