{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"双水相<span style=\"color:red\">萃取</span>是一种新型的液-液<span style=\"color:red\">萃取</span>技术，具有方法简单，易操作，成本低，易放大，条件温和，可保持蛋白质活性等明显优势，特别适用于生物样品的前处理和组分分离。本文建立了15％ PEG-4000/8％ NaH 2 PO 4双水相体系，通过<span style=\"color:red\">两次</span>双水相<span style=\"color:red\">萃取</span>结合高效液相色谱法（HPLC）分离了唾液中的多种蛋白质。经过双水相<span style=\"color:red\">萃取</span>，对上、下<span style=\"color:red\">两</span>相中的蛋白质进行色谱的梯度洗脱分析。50 min 内蛋白质的色谱峰可分为10组，根据其在上、下<span style=\"color:red\">两</span>相的分配规律还可划分为6个组分区。结果表明，<span style=\"color:red\">两次</span>双水相<span style=\"color:red\">萃取</span>结合 HPLC 可以实现唾液中的蛋白质的选择性分离。该法为复杂生物样品中的蛋白质多维度、选择性分离和分析提供了新的思路。","authors":[{"authorName":"赵新颖","id":"1fce70d0-7cb0-427d-816c-cb9181a7e300","originalAuthorName":"赵新颖"},{"authorName":"屈锋","id":"629e95ee-7e4f-4da9-ad6a-e2f1588a7d8b","originalAuthorName":"屈锋"},{"authorName":"覃浩","id":"5ff8273d-f867-4aaf-a68e-1238cc02a354","originalAuthorName":"覃浩"},{"authorName":"罗爱芹","id":"0814f4f1-a8e0-47b5-8322-a9b66ca84b76","originalAuthorName":"罗爱芹"}],"doi":"10.3724/SP.J.1123.2014.03031","fpage":"600","id":"05872385-4eec-4c9b-b638-93c227092310","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"bf79492b-237d-436c-aebc-b9524e210ccb","keyword":"双水相<span style=\"color:red\">萃取</span>","originalKeyword":"双水相萃取"},{"id":"f9f770c8-de9c-4e05-8609-fbc07506e2e0","keyword":"<span style=\"color:red\">两次</span><span style=\"color:red\">萃取</span>","originalKeyword":"两次萃取"},{"id":"1f09f14c-192b-49d6-907d-9189c56867fc","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"17b66517-fcc4-4ff3-8b32-12ee0f2a2c5e","keyword":"唾液蛋白","originalKeyword":"唾液蛋白"}],"language":"zh","publisherId":"sp201406007","title":"<span style=\"color:red\">两次</span>双水相<span style=\"color:red\">萃取</span>结合高效液相色谱法选择性分离唾液蛋白质的初步研究","volume":"","year":"2014"},{"abstractinfo":"建立了液液<span style=\"color:red\">萃取</span>-气相色谱-质谱联用法测定动物组织中残留左旋咪唑的方法.在碱性溶液中将左旋咪唑盐酸盐转化为左旋咪唑,以乙酸乙酯进行提取；分别以HCl水溶液、氢氧化钾-二氯甲烷体系进行<span style=\"color:red\">两次</span>液液<span style=\"color:red\">萃取</span>净化,依次消除提取液中的脂溶性杂质和水溶性杂质,最后进入气相色谱-质谱系统,在选择离子监测模式下,以m/z148、176、204为定性离子,m/z 204为定量离子进行结构确证和定量检测.结果表明:左旋咪唑含量在0.25 ～3.0mg/L范围内方法的线性关系良好(相关系数为0 999)；定量限为5 μg/kg,低干当前国际最低限量标准；在鸡肝、鸭肝、兔肝和猪肝样品中的加标回收率在76％ ～ 106％范围内,相对标准偏差(RSD)小于9％.该法简便、稳定性好,无需对样品进行复杂的预处理即可实现对动物肝脏中左旋咪唑残留的快速准确测定.","authors":[{"authorName":"徐静","id":"8c203803-f3a1-4ab9-b28f-ac961ac3f151","originalAuthorName":"徐静"},{"authorName":"肖珊珊","id":"fa2e224c-cd0f-473f-9ac9-c1fa394f14f2","originalAuthorName":"肖珊珊"},{"authorName":"董伟峰","id":"86bfcd1d-5b36-4b3d-924b-fab816620a4c","originalAuthorName":"董伟峰"},{"authorName":"隋凯","id":"f8bc8bbb-d536-48c8-842d-d1212db5af8a","originalAuthorName":"隋凯"},{"authorName":"曹际娟","id":"45ce8d36-825f-4522-b02e-a9cabad63803","originalAuthorName":"曹际娟"},{"authorName":"刁文婷","id":"c719c26f-cbbd-4570-bf7c-e53861ef7a2e","originalAuthorName":"刁文婷"},{"authorName":"张静","id":"e4fc2ee8-a717-495a-a076-5f4f05508104","originalAuthorName":"张静"}],"doi":"10.3724/SP.J.1123.2012.04030","fpage":"922","id":"0f75b3bc-39d9-4b68-a0aa-e3798f3427cc","issue":"9","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"968de767-71c7-42de-87e2-7f9588da4a70","keyword":"液液<span style=\"color:red\">萃取</span>","originalKeyword":"液液萃取"},{"id":"6494a9d6-fc0a-419f-a3d7-ee819956a88b","keyword":"气相色谱","originalKeyword":"气相色谱"},{"id":"47a72bd7-e024-40cc-9dbc-1335f21de8ec","keyword":"质谱","originalKeyword":"质谱"},{"id":"c5c59aa4-0939-4ef6-904c-626ae1ac272b","keyword":"左旋咪唑","originalKeyword":"左旋咪唑"},{"id":"b19e83b3-bbe1-4230-840f-73d52aa745f9","keyword":"动物肝脏","originalKeyword":"动物肝脏"}],"language":"zh","publisherId":"sp201209011","title":"<span style=\"color:red\">两次</span>液液<span style=\"color:red\">萃取</span>-气相色谱-质谱联用法测定动物肝脏中左旋咪唑残留","volume":"30","year":"2012"},{"abstractinfo":"采用<span style=\"color:red\">两次</span>离心挂浆工艺制备出氮化硅网眼多孔陶瓷.与辊压法相比,用<span style=\"color:red\">两次</span>离心挂浆工艺制备的网眼多孔陶瓷的结构均匀性得到显著提高,抗弯强度提高了1倍左右.其相组成为β-Si3N4和O'-Sialon,晶粒发育较完善.","authors":[{"authorName":"蒲锡鹏","id":"b3d3a108-0ac1-4019-ba17-3890b28bc6b3","originalAuthorName":"蒲锡鹏"},{"authorName":"张大凤","id":"97e83bc8-819b-4ab4-bb5d-9f3b8f70e794","originalAuthorName":"张大凤"},{"authorName":"刘学建","id":"05bf9af0-04d8-40da-9e9f-7f5a06e0763b","originalAuthorName":"刘学建"}],"doi":"","fpage":"389","id":"2f694e29-e632-4f41-bcf2-2917072c8ee1","issue":"z2","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"50686d9c-0b99-4402-a74f-c9a5ca654fa0","keyword":"氮化硅","originalKeyword":"氮化硅"},{"id":"487dd181-b8a0-4146-a060-917901ba5bb0","keyword":"网眼多孔陶瓷","originalKeyword":"网眼多孔陶瓷"},{"id":"98df01e3-2f24-440b-a8b7-feb714c913fd","keyword":"<span style=\"color:red\">两次</span>离心","originalKeyword":"两次离心"}],"language":"zh","publisherId":"cldb2005z2122","title":"氮化硅网眼多孔陶瓷的制备及性能:(Ⅱ)<span style=\"color:red\">两次</span>离心工艺制备","volume":"19","year":"2005"},{"abstractinfo":"采用组织观察、成分检测、热力学计算和结构分析等方法研究了超高锰钢中<span style=\"color:red\">两次</span>匹配异质形核机制.结果表明:试样中的复合化合物主要由CaS,CeS和TiC组成;合金凝固时的形核顺序为CeS(CaS)→TiC→奥氏体;CeS及CaS的(100)晶面与TiC的(001)晶面、TiC的(100)晶面与奥氏体的(001)晶面匹配良好;CeS(CaS)凝固时可作为TiC的异质形核核心,而TiC又可作为奥氏体的形核核心.CeS(CaS)/TiC/奥氏体通过<span style=\"color:red\">两次</span>匹配的方式促进异质形核.","authors":[{"authorName":"吕宇鹏","id":"2cd7144d-f7c3-4940-806c-531ddb020146","originalAuthorName":"吕宇鹏"},{"authorName":"朱瑞富","id":"e1a9c8f1-d4fb-491c-a580-704b4c7e40c7","originalAuthorName":"朱瑞富"},{"authorName":"李士同","id":"661c0f3a-555f-4c2c-a484-c2f11b500439","originalAuthorName":"李士同"},{"authorName":"雷廷权","id":"6febd50d-74b2-49e1-8770-db52003416c5","originalAuthorName":"雷廷权"},{"authorName":"董玉平","id":"83088e5c-a129-4cbc-8979-848820edffbb","originalAuthorName":"董玉平"},{"authorName":"朝志强","id":"063aea75-df5d-48b4-b413-45e28d104c60","originalAuthorName":"朝志强"}],"doi":"","fpage":"44","id":"0cc2b6b3-8752-456f-9933-d52f85af64cb","issue":"3","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"22586e80-f4db-424d-a518-788c556955bc","keyword":"超高锰钢","originalKeyword":"超高锰钢"},{"id":"afac869e-9ceb-4ddb-a539-1eb76cdc6a9c","keyword":"<span style=\"color:red\">两次</span>匹配","originalKeyword":"两次匹配"},{"id":"d669cbf9-20f4-4f17-9a4f-154ec94c08ed","keyword":"异质形核","originalKeyword":"异质形核"}],"language":"zh","publisherId":"gtyjxb199903010","title":"超高锰钢中的<span style=\"color:red\">两次</span>匹配异质形核","volume":"11","year":"1999"},{"abstractinfo":"以具有三维网状结构和贯通气孔的聚氨酯泡沫体为载体,采用<span style=\"color:red\">两次</span>离心挂浆工艺制备了高气孔率、无堵孔且结构均匀可控的氮化硅网眼多孔陶瓷.借助TG-DSC分析了泡沫体的热分解过程,确定了排胶工艺.借助流变测量和光学显微镜观察了挂浆工艺及浆料粘度对泡沫体挂浆量和多孔结构的影响,并对制品材料的微观结构和性能进行了表征.结果表明,与传统辊压工艺相比,采用<span style=\"color:red\">两次</span>离心挂浆工艺后,改善了多孔结构的均匀性,显著提高了材料强度,为高强度、结构可控、网眼多孔陶瓷的制备提供了一个有效途径.","authors":[{"authorName":"蒲锡鹏","id":"48e0b4f0-2dad-46e5-a55c-a5c42a100280","originalAuthorName":"蒲锡鹏"},{"authorName":"邱发贵","id":"14b8bf75-e6b9-4196-a4d3-8726c0d74dde","originalAuthorName":"邱发贵"},{"authorName":"刘学建","id":"845a2b63-a50a-47ed-bfff-9be620815ce4","originalAuthorName":"刘学建"},{"authorName":"黄莉萍","id":"1de74cc0-7af3-4d9c-adae-a5823b2afafe","originalAuthorName":"黄莉萍"}],"doi":"10.3321/j.issn:1000-324X.2005.06.026","fpage":"1431","id":"ad2c6346-d5d0-4fb4-984b-fb241731842c","issue":"6","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"6bef5466-22e5-4f60-8c5f-be9e4776d394","keyword":"网眼多孔陶瓷","originalKeyword":"网眼多孔陶瓷"},{"id":"8f7297d2-bd86-4f2c-8998-7b65ce5a9ec2","keyword":"涂覆","originalKeyword":"涂覆"},{"id":"4213f05c-56b6-4ea3-ae11-a0cc4706c87b","keyword":"离心工艺","originalKeyword":"离心工艺"},{"id":"59d2b830-696c-4ec8-a305-ab33649bef95","keyword":"浆料","originalKeyword":"浆料"}],"language":"zh","publisherId":"wjclxb200506026","title":"<span style=\"color:red\">两次</span>离心挂浆工艺制备网眼多孔陶瓷","volume":"20","year":"2005"},{"abstractinfo":"采用<span style=\"color:red\">两次</span>碱一<span style=\"color:red\">次</span>回流法合成工艺代替一<span style=\"color:red\">次</span>法和<span style=\"color:red\">两次</span>碱法制备酚醛树脂胶黏剂,通过对酚醛比、反应时间、反应温度、回流时间等反应条件的考察得出:以n(苯酚)∶n(甲醛)=1∶2的比例,在70℃下反应40 min,80℃下反应20 min后升温回流反应45 min得到具有交联结构的酚醛树脂胶黏剂,产品相对分子质量及黏度适中,拉伸剪切强度可达到5 MPa以上,游离甲醛含量低于0.03％,稳定性较好.","authors":[{"authorName":"周太炎","id":"df2e31a9-653b-4faf-a370-212c1e10d24d","originalAuthorName":"周太炎"},{"authorName":"杜郢","id":"091a711e-d89b-438c-8b99-f4b96e5e2fde","originalAuthorName":"杜郢"},{"authorName":"王哲","id":"8a0297f5-2da4-4288-9bd4-7b8788f0eeb8","originalAuthorName":"王哲"},{"authorName":"左学明","id":"7323c850-8462-47ab-9286-6856ff7c4e84","originalAuthorName":"左学明"},{"authorName":"徐振宇","id":"2b58e1a3-ab68-425f-bc33-6c73baca6f6a","originalAuthorName":"徐振宇"}],"doi":"10.3969/j.issn.0253-4312.2012.02.017","fpage":"71","id":"08503d8b-9701-46cf-b352-7c4e7a447629","issue":"2","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"fba6b83d-4ba4-4a8a-9b05-d0d55c4f43ba","keyword":"水溶性酚醛树脂","originalKeyword":"水溶性酚醛树脂"},{"id":"b177d671-6f79-449a-92e4-6adf5e157121","keyword":"<span style=\"color:red\">两次</span>碱一<span style=\"color:red\">次</span>回流法","originalKeyword":"两次碱一次回流法"},{"id":"9fc26714-a010-4f6d-904f-15e7ce8c9466","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"tlgy201202017","title":"<span style=\"color:red\">两次</span>碱一<span style=\"color:red\">次</span>回流法合成水溶性酚醛树脂胶粘剂","volume":"42","year":"2012"},{"abstractinfo":"采用<span style=\"color:red\">两次</span>阳极氧化法在草酸溶液中制备多孔氧化铝(AAO),分别研究了电压、氧化时间及草酸溶液浓度对AAO孔洞特征的影响.结果表明,在第一<span style=\"color:red\">次</span>氧化过程中孔间距随氧化电压的提高而增大,氧化时间和草酸溶液浓度几乎没有影响;在第二<span style=\"color:red\">次</span>氧化过程中时间、电压及草酸溶液浓度对孔间距基本无影响,但是随着氧化电压的增大AAO孔径明显增大,孔洞呈六方阵列排布.此外,第二<span style=\"color:red\">次</span>氧化电压增大时孔洞形状由圆形到长条形、再到六边形变化;第二<span style=\"color:red\">次</span>氧化草酸溶液浓度增大至0.4 mol/L时所制备的AAO的相邻孔洞沿特定取向发生贯穿现象,甚至溶解,而孔洞整体分布有序性几乎不受影响.","authors":[{"authorName":"李鑫","id":"b33dd223-6819-460e-8a8d-41ea2e0e423e","originalAuthorName":"李鑫"},{"authorName":"李秉羲","id":"deb74d48-bc86-4435-ba3e-5144248bb2a3","originalAuthorName":"李秉羲"},{"authorName":"骆玉城","id":"714118be-c946-4ec7-99ab-d29aa6a29feb","originalAuthorName":"骆玉城"},{"authorName":"李阳平","id":"c6e94d71-3149-452e-8ba8-a97ee86ab404","originalAuthorName":"李阳平"}],"doi":"","fpage":"221","id":"8eae6a5c-2ce7-4c18-9580-6f2aca55552c","issue":"3","journal":{"abbrevTitle":"CLYJXB","coverImgSrc":"journal/img/cover/CLYJXB.jpg","id":"16","issnPpub":"1005-3093","publisherId":"CLYJXB","title":"材料研究学报"},"keywords":[{"id":"6be9cd81-5a77-4906-b840-2a448734f432","keyword":"无机非金属材料","originalKeyword":"无机非金属材料"},{"id":"98bdc0a6-f889-4565-83d1-7ab9f0ff6add","keyword":"多孔氧化铝","originalKeyword":"多孔氧化铝"},{"id":"8f481c37-4b86-405c-ae87-04fef131b6e8","keyword":"<span style=\"color:red\">两次</span>氧化法","originalKeyword":"两次氧化法"},{"id":"10f545e6-9c88-4c8d-aa46-b156ecb276df","keyword":"草酸溶液","originalKeyword":"草酸溶液"},{"id":"9b110c9c-153f-4312-87fc-10579e5b4e46","keyword":"孔洞特征","originalKeyword":"孔洞特征"}],"language":"zh","publisherId":"clyjxb201503009","title":"<span style=\"color:red\">两次</span>氧化条件对阳极氧化铝孔洞的影响","volume":"29","year":"2015"},{"abstractinfo":"用复合熔盐净化与循环过热相结合的方法,获得了最大210K过冷度,研究了DD3高温合金过冷熔体凝固组织的演化规律.在所获得的过冷度范围内,凝固组织的形态发生<span style=\"color:red\">两次</span>晶粒细化:发生第一<span style=\"color:red\">次</span>细化的过冷度为30～70K,因枝晶熟化、重熔,高度发达的树枝晶转变为第一类粒状晶;发生第二<span style=\"color:red\">次</span>细化的过冷度超过153K,凝固组织因枝晶碎断和再结晶而转变为第二类粒状晶.","authors":[{"authorName":"刘峰","id":"83a9000f-fd7c-4df8-a3f3-27b13caafe30","originalAuthorName":"刘峰"},{"authorName":"郭学锋","id":"7ba4fd9b-f177-42ff-b651-c78c8c524138","originalAuthorName":"郭学锋"},{"authorName":"杨根仓","id":"d50ff4f1-1b3c-4d05-8b24-4aab80720786","originalAuthorName":"杨根仓"}],"doi":"10.3321/j.issn:1005-3093.2001.03.002","fpage":"269","id":"04476c1f-a931-4fe1-a1c6-92395de252cd","issue":"3","journal":{"abbrevTitle":"CLYJXB","coverImgSrc":"journal/img/cover/CLYJXB.jpg","id":"16","issnPpub":"1005-3093","publisherId":"CLYJXB","title":"材料研究学报"},"keywords":[{"id":"f8dec1c5-78f2-4151-9cff-5d113d034e89","keyword":"DD3高温合金","originalKeyword":"DD3高温合金"},{"id":"7de750dc-6555-4669-9b08-495769c06d7b","keyword":"过冷","originalKeyword":"过冷"},{"id":"6ed3c88b-de13-464d-a3f8-c1af9e38bafd","keyword":"晶粒细化","originalKeyword":"晶粒细化"},{"id":"8d14a91d-e3de-427e-adf3-9ddfc95a4e77","keyword":"再结晶","originalKeyword":"再结晶"}],"language":"zh","publisherId":"clyjxb200103002","title":"深过冷DD3高温合金的<span style=\"color:red\">两次</span>细化机制","volume":"15","year":"2001"},{"abstractinfo":"利用装甲钢平头弹丸垂直侵彻Ti-6A1-4V合金靶板,分析相同弹道学条件下,<span style=\"color:red\">两次</span>侵彻同一靶板不同位置材料的微观组织与弹着点损伤演化特征.研究靶板<span style=\"color:red\">两次</span>侵彻损伤程度和一<span style=\"color:red\">次</span>侵彻对再次侵彻造成的影响.结果表明,<span style=\"color:red\">两次</span>侵彻形成的剪切带都萌发于靶板与受力方向成45°角方位.第1<span style=\"color:red\">次</span>侵彻形成的剪切带较短,剪切带有弯折与扭转,剪切带在与受力方向成45°角萌发后沿浅表面向30°角方向扩展.第2<span style=\"color:red\">次</span>侵彻形成的剪切带较长,剪切带内孔洞相连,剪切带在与受力方向成45°角方位形成后向平行于受力方向纵深发展.第2<span style=\"color:red\">次</span>剪切损伤大于第1<span style=\"color:red\">次</span>剪切损伤的主要原因是第1<span style=\"color:red\">次</span>侵彻过程中靶板局部区域形成了绝热剪切带,从而引起了靶板材料强度增高、残余应力呈不均匀分布以及笫2<span style=\"color:red\">次</span>侵彻过程中残余应力与应力叠加、局部应变硬化以及应变率硬化所致.","authors":[{"authorName":"李淑华","id":"3e86ae4f-262d-4536-8e81-6a9ce600181b","originalAuthorName":"李淑华"},{"authorName":"沈大为","id":"2ece68d1-0610-448c-8d94-fa7e0a60b13b","originalAuthorName":"沈大为"},{"authorName":"孙凯","id":"b46c35e4-96e9-4a9c-9edd-6186eefe3664","originalAuthorName":"孙凯"},{"authorName":"谭成文","id":"a19998e7-7ddb-485c-8c45-6ef73749865d","originalAuthorName":"谭成文"},{"authorName":"王富耻","id":"7251b074-f2f5-45b3-b94e-b99467c69307","originalAuthorName":"王富耻"},{"authorName":"冯顺山","id":"e2d99f3f-69ae-463b-8266-4997dbf914c3","originalAuthorName":"冯顺山"}],"doi":"","fpage":"1864","id":"766ddcbe-d972-4ab1-991f-bb19c9af34ca","issue":"9","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"f26ad10d-d7db-48cb-bd62-81763076bdc8","keyword":"<span style=\"color:red\">两次</span>侵彻","originalKeyword":"两次侵彻"},{"id":"73e1dc58-9ab1-4147-9760-00635945e057","keyword":"Ti-6A1-4V合金","originalKeyword":"Ti-6A1-4V合金"},{"id":"3d96a787-0561-4389-89f0-930a01ee7b3f","keyword":"绝热剪切带","originalKeyword":"绝热剪切带"},{"id":"d61d21f9-95ff-42b5-a2c1-212564a750d6","keyword":"损伤特征","originalKeyword":"损伤特征"}],"language":"zh","publisherId":"xyjsclygc201309020","title":"Ti-6Al-4V合金<span style=\"color:red\">两次</span>侵彻弹着点损伤及组织演化","volume":"42","year":"2013"},{"abstractinfo":"用纳米ZrO2(4Y)粉为原料,研究了单轴压片素坯成型特征.通过<span style=\"color:red\">两次</span>施压成型,降低了烧结致密温度,在1300℃常压烧结2小时,陶瓷体致密度达99.1%,烧结体晶粒长大减缓.片状烧结体1000℃和800℃时的电导率分别为4.23×10-2Ω-1cm-1和1.19×10-2Ω-1cm-1.","authors":[{"authorName":"袁望治","id":"c9c5f8cb-d185-46b6-b2b6-b6bcd595f6a0","originalAuthorName":"袁望治"},{"authorName":"劳令耳","id":"749c2917-19df-4aa8-bd70-4a20fdb4c910","originalAuthorName":"劳令耳"},{"authorName":"田卫","id":"9418873b-76ee-4f38-8bf4-488a907c8e22","originalAuthorName":"田卫"},{"authorName":"刘毅","id":"145a2e13-cc79-411d-9d56-2264e9e14d64","originalAuthorName":"刘毅"},{"authorName":"王大志","id":"d70fb646-9c3b-4492-adf2-206c253268e8","originalAuthorName":"王大志"},{"authorName":"姚琨","id":"18260c40-51cb-49f7-8a90-d1f85a873ac0","originalAuthorName":"姚琨"},{"authorName":"王正","id":"6b46924c-e753-46c0-b837-4ef4c9c4ee57","originalAuthorName":"王正"}],"doi":"10.3969/j.issn.1673-2812.2000.03.014","fpage":"57","id":"ddbaa445-1383-4c69-a24d-d564dd36191b","issue":"3","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"aec3ccdf-00db-4e27-b1a5-77d658961ea2","keyword":"ZrO2(4Y)","originalKeyword":"ZrO2(4Y)"},{"id":"de0ebc06-ba5f-4328-82fa-bcad4715940c","keyword":"纳米粉","originalKeyword":"纳米粉"},{"id":"e9d56bf4-b572-4e77-be5d-7fce723a78e4","keyword":"烧结","originalKeyword":"烧结"},{"id":"25e43653-b01d-4b92-9c4e-018bba46b888","keyword":"电导","originalKeyword":"电导"}],"language":"zh","publisherId":"clkxygc200003014","title":"纳米ZrO2(4Y)<span style=\"color:red\">两次</span>成型常压烧结致密特性及其电导率","volume":"18","year":"2000"}],"totalpage":3381,"totalrecord":33801}