{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"探索了用传统的电弧放电法、在现有的电弧放电装置中,通过改进放电工艺、添加催化剂制备<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>(Nano Onion-Iike Fullerenes <span style=\"color:red\">NOLFs</span>)的过程和工艺.用高分辨透射电镜(High Resolution Transmission Electron Microscope HRTEM)对生成的<span style=\"color:red\">NOLFs</span>进行了形貌、结构的观察与表征.分析结果表明<span style=\"color:red\">NOLFs</span>晶化程度很高,直径均匀(20～50nm).生成的<span style=\"color:red\">NOLFs</span>可分为两大类:(1)内包金属<span style=\"color:red\">纳米</span>微粒的<span style=\"color:red\">NOLFs</span>;(2)单体<span style=\"color:red\">NOLFs</span>.对<span style=\"color:red\">NOLFs</span>的生成机理及催化剂对其直径、收率的影响进行了讨论.据此建立的汽-液-固(Vapor-Liquid-Solid:VLS)生长模型可以解释实验中出现的一些现象.研究表明生成<span style=\"color:red\">NOLFs</span>的数量、直径分别与催化剂的活性及其尺寸有关.","authors":[{"authorName":"许并社","id":"378494dd-a37d-485f-bd69-db77341c91b7","originalAuthorName":"许并社"},{"authorName":"闫小琴","id":"e98801a8-90ce-4cfd-89f1-869e1f169078","originalAuthorName":"闫小琴"},{"authorName":"王晓敏","id":"63670061-5c35-47a4-8e3e-7f964651c5dd","originalAuthorName":"王晓敏"},{"authorName":"市野濑英喜","id":"b0217d75-9d3c-44ad-84dc-d91c10f7f242","originalAuthorName":"市野濑英喜"},{"authorName":"解思深","id":"a0add664-0a39-4a5e-90db-614142411c25","originalAuthorName":"解思深"}],"doi":"10.3969/j.issn.1009-6264.2001.04.003","fpage":"9","id":"98f6e8f9-842b-4f93-995b-d356a11ab70a","issue":"4","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"0f103508-9525-4c3d-8989-32ab08e722c0","keyword":"<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>(<span style=\"color:red\">NOLFs</span>)","originalKeyword":"纳米洋葱状富勒烯(NOLFs)"},{"id":"bf2ba747-d83f-4d81-8111-905f5b5964c6","keyword":"电弧放电","originalKeyword":"电弧放电"},{"id":"581839fa-52b9-4a73-acaf-c1cc015af978","keyword":"高分辨透射电镜(HRTEM)","originalKeyword":"高分辨透射电镜(HRTEM)"},{"id":"7a939df9-9795-4e23-98a4-adeb620c0de2","keyword":"汽-液-固生长模型","originalKeyword":"汽-液-固生长模型"}],"language":"zh","publisherId":"jsrclxb200104003","title":"电弧放电中<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>生成机理的研究","volume":"22","year":"2001"},{"abstractinfo":"采用金属Cu,Al微粒/石墨混合材料,用直流电弧放电方法制备了<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>.对两种产物进行了XRD、SEM、HRTEM和Raman结构表征.结果表明:两种<span style=\"color:red\">纳米</span>金属微粒均可催化得到<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>;所得产物中有单纯<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>和内包<span style=\"color:red\">纳米</span>金属微粒<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>,且石墨化程度都很高;<span style=\"color:red\">纳米</span>金属微粒尺寸大小不同决定<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的直径分布不均匀,从而造成其拉曼谱峰相对于石墨特征峰1582cm-1发生了频移;用汽-液-固(VLS)生长模型描述了<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>生长机理,解释了汽态碳原子通过在液态催化剂中扩散和析出,逐渐长大成形的现象.","authors":[{"authorName":"王晓敏","id":"63e2c729-5e37-4565-92e9-944d7b7658a8","originalAuthorName":"王晓敏"},{"authorName":"许并社","id":"636c341f-0fed-40e7-baaa-99055b066f44","originalAuthorName":"许并社"},{"authorName":"刘旭光","id":"0dbeddfd-9cbf-4faa-a352-a43237274d7f","originalAuthorName":"刘旭光"},{"authorName":"市野濑英喜","id":"4eafc35b-b579-4b0a-8a2d-c0f59437f7de","originalAuthorName":"市野濑英喜"}],"doi":"10.3969/j.issn.1007-8827.2004.03.009","fpage":"209","id":"6266d7cf-61ec-41a7-a834-da0a3925eba5","issue":"3","journal":{"abbrevTitle":"XXTCL","coverImgSrc":"journal/img/cover/XXTCL.jpg","id":"70","issnPpub":"1007-8827","publisherId":"XXTCL","title":"新型炭材料"},"keywords":[{"id":"e83f0ddc-1a4d-4ca5-a195-46f580634af4","keyword":"<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>","originalKeyword":"洋葱状富勒烯"},{"id":"cce4eac6-9656-462b-92be-d33c87b0ea34","keyword":"<span style=\"color:red\">纳米</span>金属微粒","originalKeyword":"纳米金属微粒"},{"id":"a75e60fc-1f42-4ef8-b636-99088ccc5dfb","keyword":"结构表征","originalKeyword":"结构表征"},{"id":"fd69e765-8b03-425f-9395-0750931a3e88","keyword":"VLS生长模型","originalKeyword":"VLS生长模型"}],"language":"zh","publisherId":"xxtcl200403009","title":"<span style=\"color:red\">纳米</span>金属微粒催化制备的<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的结构表征","volume":"19","year":"2004"},{"abstractinfo":"通过述评<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的结构、制备、生长机理、纯化、修饰及性能,指出:<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>具有独特的中空笼<span style=\"color:red\">状</span>及同心壳层结构,是<span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>家族的一个重要成员,具有许多特殊性能,有望在能源材料、高性能、高温耐磨材料、超导材料和生物医用材料等领域得到广泛的应用.","authors":[{"authorName":"许并社","id":"fadd2c76-720a-4780-b0c4-e2c2f5be4766","originalAuthorName":"许并社"}],"doi":"","fpage":"289","id":"7dc32fc9-0967-4346-a48e-39f6da13b789","issue":"4","journal":{"abbrevTitle":"XXTCL","coverImgSrc":"journal/img/cover/XXTCL.jpg","id":"70","issnPpub":"1007-8827","publisherId":"XXTCL","title":"新型炭材料"},"keywords":[{"id":"47b68eae-8eaf-4fc9-b525-0eb58e7c01c9","keyword":"<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>","originalKeyword":"纳米洋葱状富勒烯"},{"id":"f6634fbe-1d0f-4ec8-ace6-fe687b58d30d","keyword":"研究进展","originalKeyword":"研究进展"},{"id":"7d129ec7-9998-46ed-be6d-cde32d4762bc","keyword":"前景","originalKeyword":"前景"}],"language":"zh","publisherId":"xxtcl200804001","title":"<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的研究现状及前景","volume":"23","year":"2008"},{"abstractinfo":"评述了<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的研究发展过程和动向.论述了该物质的各种制备方法及其工艺,并对各种制备工艺进行了分析和探讨性研究,在此基础上比较论述了每种方法的优缺点.展望了<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>基础研究、宏量制备和应用研究的发展趋向.\n","authors":[{"authorName":"许并社","id":"adbfa5a2-f2a3-40c8-935b-c58d3932c9fd","originalAuthorName":"许并社"}],"doi":"","fpage":"45","id":"61ce958b-af0b-4c88-8fb8-25a6a130d64b","issue":"9","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"3238c13c-ae61-403e-8dde-3f6e8282284a","keyword":"<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>","originalKeyword":"纳米洋葱状富勒烯"},{"id":"1a048859-2a73-4ba6-8f85-b015108ac7e4","keyword":"电子束辐照","originalKeyword":"电子束辐照"},{"id":"64073178-486a-461d-bfaf-b309aa57b1b5","keyword":"电弧放电","originalKeyword":"电弧放电"},{"id":"0f234e8a-8bb5-4729-a49a-287e5b010735","keyword":"碳材料","originalKeyword":"碳材料"},{"id":"6e553d97-4502-4d57-bbd2-11090ef1bd7d","keyword":"<span style=\"color:red\">纳米</span>材料","originalKeyword":"纳米材料"}],"language":"zh","publisherId":"cldb200109014","title":"<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的研究进展及动向","volume":"15","year":"2001"},{"abstractinfo":"研究了相同电弧放电条件下,不同催化剂(Fe、Al)掺杂对<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>形成的影响.用高分辨透射电子显微镜(HRTEM)和X-射线衍射(XRD)对产物进行了观察与表征.结果表明,Fe作催化剂形成的<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>产量和质量都优于Al作催化剂的情况,Fe的催化活性较Al的高,是制备<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的一种更加有效的催化剂.","authors":[{"authorName":"章海霞","id":"ba74ef72-704d-4f2b-b5a7-55efcd596fb2","originalAuthorName":"章海霞"},{"authorName":"王晓敏","id":"ffe61e62-6efd-4dea-95ae-7b6deccaf6f3","originalAuthorName":"王晓敏"},{"authorName":"王海英","id":"1e8dd208-628e-4575-85e6-d9d642023bd6","originalAuthorName":"王海英"},{"authorName":"刘旭光","id":"ad4326ca-a9d9-4cc5-9e23-4283fad11c18","originalAuthorName":"刘旭光"},{"authorName":"许并社","id":"45183482-bcb2-4fa7-bb0d-90d1c65881b9","originalAuthorName":"许并社"}],"doi":"","fpage":"175","id":"a01642df-97a7-4128-b2c6-efa69a598bd0","issue":"z2","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"ffdef94b-040d-48b0-99d6-6077e29d6095","keyword":"催化剂","originalKeyword":"催化剂"},{"id":"8751c61d-d1a2-4c45-8436-f37c31a46f63","keyword":"<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>","originalKeyword":"纳米洋葱状富勒烯"},{"id":"fc1c537a-c9f9-438f-8d36-97419715c986","keyword":"影响","originalKeyword":"影响"},{"id":"129f5a23-7ae1-43db-823d-72d69cd41519","keyword":"电弧放电","originalKeyword":"电弧放电"}],"language":"zh","publisherId":"cldb2004z2053","title":"催化剂种类对<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>形成的影响","volume":"18","year":"2004"},{"abstractinfo":"运用<span style=\"color:red\">纳米</span>Bi2O3微粒作催化剂,在电弧放电条件下,进行了<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>大量合成的研究.并用透射电镜对产物的形貌、结构进行了观察与分析.结果表明:<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的石墨化程度很高,且直径均匀(约为25 nm),结构较完善;同时伴有单核<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>向多核<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的转变.为<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的宏量制备提供了有利线索.","authors":[{"authorName":"章海霞","id":"3dd357e1-c98d-45ba-bf87-4c5e6be54417","originalAuthorName":"章海霞"},{"authorName":"王晓敏","id":"35eaca3a-f471-4c5f-9ebd-3036f52456c2","originalAuthorName":"王晓敏"},{"authorName":"王海英","id":"eb60c029-f512-44be-83f0-7e6888af8a98","originalAuthorName":"王海英"},{"authorName":"刘旭光","id":"dd50e763-0ac7-4031-9c29-00b28d898a91","originalAuthorName":"刘旭光"},{"authorName":"许并社","id":"91f4d1bf-44ec-4b77-bc58-042168a9f8cc","originalAuthorName":"许并社"}],"doi":"10.3969/j.issn.1007-8827.2004.01.013","fpage":"61","id":"f60cc889-f5c7-4b8d-9af0-83d26b3dc654","issue":"1","journal":{"abbrevTitle":"XXTCL","coverImgSrc":"journal/img/cover/XXTCL.jpg","id":"70","issnPpub":"1007-8827","publisherId":"XXTCL","title":"新型炭材料"},"keywords":[{"id":"2b53d608-1466-4dba-a9bd-21c39a20b6c3","keyword":"催化剂","originalKeyword":"催化剂"},{"id":"41e38597-64e4-4723-b3e4-2259df88ed49","keyword":"电弧放电","originalKeyword":"电弧放电"},{"id":"68b44b37-b34d-46e5-b070-8fe7f7f82b0d","keyword":"<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>","originalKeyword":"纳米洋葱状富勒烯"}],"language":"zh","publisherId":"xxtcl200401013","title":"电弧法制备<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的工艺研究","volume":"19","year":"2004"},{"abstractinfo":"在射频等离子体条件下以煤为原料制备<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>(Nano-structured Onion-like Fullerenes:NSOFs).高分辨透射电镜(HRTEM)和X射线衍射(XRD)表征结果表明:以煤为原料可大量制备NSOFs,纯度较高,无碳<span style=\"color:red\">纳米</span>管伴随生成,外观呈准球状或多面体<span style=\"color:red\">状</span>,内中空,直径分布较均匀,石墨化程度很高,为低成本合成纯净的NSOFs提供了一条新途径.","authors":[{"authorName":"杜爱兵","id":"e56b4911-1427-412c-ad02-be3cef9928e7","originalAuthorName":"杜爱兵"},{"authorName":"刘旭光","id":"9a6ef9e0-b19e-402f-ad88-38a7be4cf8f2","originalAuthorName":"刘旭光"},{"authorName":"许并社","id":"d1315164-8abd-4f6a-923c-096af31bcca8","originalAuthorName":"许并社"}],"doi":"10.3321/j.issn:1000-324X.2005.04.002","fpage":"779","id":"00713be4-495f-434a-8bf9-e6865553d22e","issue":"4","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"0da4e199-90fd-436c-a573-aec24bc9e60b","keyword":"<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>","originalKeyword":"纳米洋葱状富勒烯"},{"id":"c148d964-749d-4d3f-aa2e-5400c75deb42","keyword":"射频等离子体","originalKeyword":"射频等离子体"},{"id":"8df800d1-6321-47c3-92bf-430227891efa","keyword":"煤","originalKeyword":"煤"},{"id":"08466b52-1675-4341-9381-0171642cd1a0","keyword":"HRTEM","originalKeyword":"HRTEM"}],"language":"zh","publisherId":"wjclxb200504002","title":"煤基<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>制备及其结构表征","volume":"20","year":"2005"},{"abstractinfo":"在金属微粒催化的条件下探索了用直流电弧放电法制备内包金属<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>(Onionlike Fullerenes OLFs)的过程和工艺.用扫描电镜(SEM)和高分辨透射电镜(HRTEM)等实验手段对生成的OLFs进行了形貌、结构的观察和表征.研究结果表明:调整工艺参数,并辅以催化剂掺杂可大量制备内包金属的OLFs;对个别工艺参数的影响进行了探讨.","authors":[{"authorName":"王海英","id":"1d82a58e-aa40-4e1e-a882-f882a0986d2f","originalAuthorName":"王海英"},{"authorName":"王晓敏","id":"326ee2d7-91c5-4c04-8ee5-ca4275dd8e8b","originalAuthorName":"王晓敏"},{"authorName":"章海霞","id":"cb0e6931-3325-4b4b-9594-24e9f38af229","originalAuthorName":"章海霞"},{"authorName":"许并社","id":"a834549f-ad88-4994-8f98-5dfd498b6b90","originalAuthorName":"许并社"}],"doi":"10.3969/j.issn.1009-6264.2003.04.009","fpage":"41","id":"a8fba1d8-927f-4c12-9f1d-a2c6912ffd9b","issue":"4","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"f1314450-82b3-43a7-abf5-f4d1717a64bd","keyword":"<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>(OLFs)","originalKeyword":"洋葱状富勒烯(OLFs)"},{"id":"53d7ec92-26f1-48fe-82d4-c458c57cd386","keyword":"电弧放电","originalKeyword":"电弧放电"},{"id":"e36193f7-bbee-4dd1-a202-faa99e7d1d57","keyword":"金属<span style=\"color:red\">纳米</span>微粒催化","originalKeyword":"金属纳米微粒催化"}],"language":"zh","publisherId":"jsrclxb200304009","title":"电弧放电制备内包金属<span style=\"color:red\">纳米</span><span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的研究","volume":"24","year":"2003"},{"abstractinfo":"采用CVD法制备了<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>(OLFs),研究了不同工艺条件对OLFs形成的影响,并通过硝酸回流法对得到的粗产品进行了提纯处理.研究结果表明,在相同的反应体系中,采用乙炔作碳源,氩气和氢气的混合气体作载气,制得的OLFs的纯度较高;硝酸处理可有效去除粗产品中碳<span style=\"color:red\">纳米</span>管、无定形炭和金属催化剂颗粒等杂质,使得OLFs的整体纯度得到提高.","authors":[{"authorName":"孙瑞平","id":"a138f7de-ae95-4354-a053-e5248a950547","originalAuthorName":"孙瑞平"},{"authorName":"刘光焕","id":"d889078a-fd4f-47db-82b7-5f4d3bd66ab6","originalAuthorName":"刘光焕"},{"authorName":"李天保","id":"27622a06-2944-401c-a194-5703364587a1","originalAuthorName":"李天保"},{"authorName":"韩培德","id":"995d2fe0-88ab-44eb-b364-7f919950c40b","originalAuthorName":"韩培德"},{"authorName":"刘旭光","id":"0c944ba1-2245-496f-97d0-71c1720f78e3","originalAuthorName":"刘旭光"},{"authorName":"许并社","id":"3d2f5ff4-f15b-497c-9bfb-2392192ea481","originalAuthorName":"许并社"}],"doi":"","fpage":"206","id":"46e294ec-9867-4811-ad61-6b8c1fadec1b","issue":"z1","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"eac3550f-7454-4d2e-87ff-ca4b62bc3e83","keyword":"<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>","originalKeyword":"洋葱状富勒烯"},{"id":"586f9655-6b43-4b44-b4c5-4ac377e78d87","keyword":"CVD","originalKeyword":"CVD"},{"id":"7dd73e9b-02b4-477d-b109-0dc28435596b","keyword":"回流","originalKeyword":"回流"},{"id":"538612a0-d68e-4bba-83fc-2e80fa3b5ada","keyword":"提纯","originalKeyword":"提纯"}],"language":"zh","publisherId":"cldb2006z1066","title":"<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的制备与提纯","volume":"20","year":"2006"},{"abstractinfo":"详细介绍和分析了<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>(OLFS)的各种制备、纯化和改性方法,概述了其性能和应用的最新研究进展.OLFS特有的力、电、光、磁、吸附、催化等物理及化学性能,使其在工程、电子信息、能源、生物医学、化学化工、国防等领域有着广阔的应用前景.为此,应进一步围绕OLFS类新型<span style=\"color:red\">纳米</span>碳材料的制备、表面修饰、功能化、实际应用等各个环节的物理与化学问题进行探索,为该类功能材料的实际应用提供参考依据.","authors":[{"authorName":"许并社","id":"6057a14e-f96f-44cc-bc05-e11970a620bf","originalAuthorName":"许并社"},{"authorName":"杨永珍","id":"05be18cc-db68-4e50-9883-2c80c2d88692","originalAuthorName":"杨永珍"},{"authorName":"张竹霞","id":"040a132e-9364-4370-9ee9-0ffff03648a6","originalAuthorName":"张竹霞"},{"authorName":"刘旭光","id":"50d0419e-db9f-423d-aad6-4c3a5139c00e","originalAuthorName":"刘旭光"}],"doi":"","fpage":"1","id":"531aade5-accb-400c-b491-af5fdf59e877","issue":"11","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"a855951c-c49b-448a-b358-2b197474e798","keyword":"新型碳材料","originalKeyword":"新型碳材料"},{"id":"b10864ac-ecc8-405d-9b0e-2734579095eb","keyword":"<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>","originalKeyword":"洋葱状富勒烯"},{"id":"c2cc200a-7657-4a0e-b9d8-2baa2856fab5","keyword":"制备与改性","originalKeyword":"制备与改性"}],"language":"zh","publisherId":"cldb200911001","title":"<span style=\"color:red\">洋葱</span><span style=\"color:red\">状</span><span style=\"color:red\">富</span><span style=\"color:red\">勒</span><span style=\"color:red\">烯</span>的研究进展","volume":"23","year":"2009"}],"totalpage":3344,"totalrecord":33438}