{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以250 μm大小的锑粉为原料,在添加相同含量蒸馏水和烷基酚聚氧乙烯醚的条件下,采用湿法机械球磨的方式制备出不同类型的锑基粉末.采用XRD、TEM及FT-IR对制备的锑基粉末的结构、形貌及粒径大小进行了表征分析,研究了球磨时间和球磨转速对锑粉制备的影响.结果表明:当锑粉原料中加入1 ml/g蒸馏水和0.2 ml/g OP-1O湿磨时,球磨转速为150r/min、球磨时间为18 h可制备出分散良好、粒径分布均匀、平均粒径约为10 nm的锑粉.","authors":[{"authorName":"徐建林","id":"4c5377ba-f00f-4bd7-86d3-e50240465f45","originalAuthorName":"徐建林"},{"authorName":"郭强","id":"10f406b2-2483-4e72-bb37-4abba1e8432e","originalAuthorName":"郭强"},{"authorName":"康昭","id":"ff696df4-2f79-4d75-a91c-6dbe2d9d4fdf","originalAuthorName":"康昭"},{"authorName":"<span style=\"color:red\">席</span><span style=\"color:red\">国强</span>","id":"2871122b-b050-4910-8ca9-609630615039","originalAuthorName":"席国强"}],"doi":"","fpage":"18","id":"001c90ba-9590-475f-a414-e5840fb3326d","issue":"6","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"548a3a1b-18e6-488f-a115-8ba994049dfe","keyword":"锑","originalKeyword":"锑"},{"id":"0c1393b9-e34c-4051-a787-dea7912c6336","keyword":"球磨","originalKeyword":"球磨"},{"id":"af60ecae-c5c1-4d76-b64a-3febc0534898","keyword":"纳米粉","originalKeyword":"纳米粉"}],"language":"zh","publisherId":"jsrclxb201306004","title":"球磨时间和转速对球磨法制备纳米锑粉的影响","volume":"34","year":"2013"},{"abstractinfo":"为了研究纳米锑颗粒作为润滑油添加剂的润滑摩擦学性能,充分发挥其减磨、抗磨效果,采用CFT-1型材料性能测试仪对比研究了不同载荷下纳米锑粒子作为液压油添加剂的摩擦学性能,通过SEM对试样摩擦表面进行了形貌分析,利用EDX进行了磨痕表面元素分析.结果表明:不同载荷下纳米锑颗粒在液压油中的最佳添加量不同,重载荷下纳米锑粒子表现出优良的抗磨减摩性能；纳米锑粒子在一定程度上可以提高液压油的抗磨减摩性能,这是由于磨痕表面形成了含锑元素的表面膜,起到良好的抗磨减摩效果.","authors":[{"authorName":"徐建林","id":"16877fc3-08fb-446f-87e6-a7e4d4d636ca","originalAuthorName":"徐建林"},{"authorName":"康昭","id":"8466ac95-5ff1-490c-9083-4097112371c1","originalAuthorName":"康昭"},{"authorName":"郭强","id":"fe46c1cb-0dcb-416f-ab1d-ee5d86f4b37f","originalAuthorName":"郭强"},{"authorName":"<span style=\"color:red\">席</span><span style=\"color:red\">国强</span>","id":"5c42cdc1-3f6b-4a8c-96f3-3a69e0d8b26e","originalAuthorName":"席国强"},{"authorName":"王佳","id":"716fe2a0-b6ae-482e-9b1d-ebca1ca7f095","originalAuthorName":"王佳"}],"doi":"","fpage":"24","id":"02b94c41-4d72-47fe-b2fa-ba37e518774f","issue":"1","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"aa3d38ba-587a-4646-9321-18986cebe8fc","keyword":"纳米颗粒","originalKeyword":"纳米颗粒"},{"id":"d528daef-89e9-4fab-b051-96a37ad628f8","keyword":"锑","originalKeyword":"锑"},{"id":"145dbf9d-1ca2-4e54-8dc2-880cb358666b","keyword":"摩擦磨损性能","originalKeyword":"摩擦磨损性能"},{"id":"9529f78a-a1f4-497b-9cb3-276db97aa7ec","keyword":"液压油","originalKeyword":"液压油"},{"id":"11cb09be-237f-4711-b6b8-830e7d0cb6e1","keyword":"添加剂","originalKeyword":"添加剂"}],"language":"zh","publisherId":"clkxygy201301005","title":"纳米锑颗粒作为液压油添加剂的摩擦学性能","volume":"21","year":"2013"},{"abstractinfo":"为探讨不同的球磨介质对球磨法制备纳米锑粉的影响,以250μm大小的锑粉为原料,采用干法机械球磨以及添加不同的球磨介质进行湿法机械球磨的方式制备出不同类型的锑基粉末.应用XRD、TEM及FT-IR对制备的锑基粉末的结构、形貌及粒径大小进行了表征分析.研究结果表明:不同的球磨介质对机械球磨法制备纳米锑粉的作用是不同的.采用于法机械球磨制备出的锑粉会产生氧化现象,采用湿法球磨可制备出纳米锑粉.当球磨介质为蒸馏水时,可有效防止纳米锑粉的氧化,但锑粉的分散性不佳；当球磨介质为蒸馏水和十二烷基硫酸钠时,可制备出分散均匀、粒径分布不均匀的纳米锑粉；当球磨介质为蒸馏水和OP-10时,可制备出分散均匀、粒径分布均匀纳米锑粉,锑粉的平均粒径约为20nm.","authors":[{"authorName":"徐建林","id":"c98eb2aa-1d2e-43e4-8676-b985a57f1585","originalAuthorName":"徐建林"},{"authorName":"郭强","id":"674c64ea-6ef5-4ec0-94b9-2b76dc109e31","originalAuthorName":"郭强"},{"authorName":"高威","id":"3f675278-cbb1-4e45-bd52-f36dcf3fc477","originalAuthorName":"高威"},{"authorName":"康昭","id":"9915f98d-3ced-49fc-8ab3-d37ee34f1ed3","originalAuthorName":"康昭"},{"authorName":"<span style=\"color:red\">席</span><span style=\"color:red\">国强</span>","id":"73130499-663d-49ed-af1f-9e82d611b55b","originalAuthorName":"席国强"},{"authorName":"张亮","id":"222a244d-cf4b-491d-84a0-03d2920d5ab3","originalAuthorName":"张亮"}],"doi":"10.3969/j.issn.1005-5053.2013.1.009","fpage":"50","id":"b56c89e9-270d-4b61-98c4-8b35a07a025b","issue":"1","journal":{"abbrevTitle":"HKCLXB","coverImgSrc":"journal/img/cover/HKCLXB.jpg","id":"41","issnPpub":"1005-5053","publisherId":"HKCLXB","title":"航空材料学报"},"keywords":[{"id":"2caacef4-351e-47d8-a0ba-40bbec72207b","keyword":"锑","originalKeyword":"锑"},{"id":"04a55789-ca4e-498f-a601-fcd3cf6c46d1","keyword":"球磨","originalKeyword":"球磨"},{"id":"4e77b339-78ae-4081-a9c0-d545b80cff2f","keyword":"纳米粉末","originalKeyword":"纳米粉末"}],"language":"zh","publisherId":"hkclxb201301009","title":"球磨介质对机械球磨法制备纳米锑粉影响的研究","volume":"33","year":"2013"},{"abstractinfo":"以对溴苯酚和苯甲酰氯为原料,经过酯化、Fries重排、缩合等一系列反应,合成了2-[(2-苯基亚氨基)苯甲基]-4-溴苯酚,该化合物分别与多种醛酮在不同条件下反应,得到了5种不对称双<span style=\"color:red\">席</span>夫碱和2种对称性双<span style=\"color:red\">席</span>夫碱.对<span style=\"color:red\">席</span>夫碱化合物的抑菌活性测定表明,大部分化合物具有较强的抗菌活性,其中含硫原子的<span style=\"color:red\">席</span>夫碱抑菌活性最强,最小抑菌浓度均为1×10-4 g/L.","authors":[{"authorName":"杨丰科","id":"6f13de68-ac01-4c93-8e9b-373e1b12e1cb","originalAuthorName":"杨丰科"},{"authorName":"韩健","id":"50c55067-3346-4038-9e5c-babd9c16da72","originalAuthorName":"韩健"},{"authorName":"王永春","id":"151d8543-fbd4-44f0-97f9-9cb7de3750be","originalAuthorName":"王永春"},{"authorName":"陈芳","id":"b8cbbd0c-0353-4f41-8a8f-a9d2337a4cc3","originalAuthorName":"陈芳"}],"doi":"10.11944/j.issn.1000-0518.2015.04.140286","fpage":"392","id":"9a31439f-1072-453a-b80e-c2ca9fad7ea9","issue":"4","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"73140970-7d63-4df7-a86d-5bd15e3fa4f4","keyword":"<span style=\"color:red\">席</span>夫碱","originalKeyword":"席夫碱"},{"id":"fc2f2b6a-ab1e-45d3-831d-5fcf6461f2af","keyword":"合成","originalKeyword":"合成"},{"id":"c79ef3d0-667d-4733-a567-1ffe50e2f2b8","keyword":"重排","originalKeyword":"重排"},{"id":"3b636a3c-8d87-4520-a247-5c8f007186cf","keyword":"抑菌活性","originalKeyword":"抑菌活性"}],"language":"zh","publisherId":"yyhx201504004","title":"<span style=\"color:red\">席</span>夫碱的合成及生物活性","volume":"32","year":"2015"},{"abstractinfo":"<span style=\"color:red\">席</span>夫碱及其盐类是一类新型功能材料,已在众多领域得到广泛应用.本文主要介绍了<span style=\"color:red\">席</span>夫碱的合成和性能及其在吸波材料和红外隐身材料中的研究现状与发展前景.","authors":[{"authorName":"张艳茹","id":"fd8d9fa5-9b1a-4fbb-af43-122a7cde7f5a","originalAuthorName":"张艳茹"},{"authorName":"王智勇","id":"caf76b14-1982-4e2c-b294-1b3571aca36d","originalAuthorName":"王智勇"}],"doi":"10.3969/j.issn.1001-4381.2008.z1.080","fpage":"366","id":"ccb00c2f-ae68-4b3e-83d7-615b522795de","issue":"z1","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"6ec25a27-956d-4055-affd-ba9eb7c2bf2b","keyword":"<span style=\"color:red\">席</span>夫碱","originalKeyword":"席夫碱"},{"id":"2b909aa2-2fa0-473b-b0d1-f4e7114003f0","keyword":"吸波材料","originalKeyword":"吸波材料"},{"id":"04860297-43a9-4ae4-a7e4-b46f2e20b4b5","keyword":"红外隐身材料","originalKeyword":"红外隐身材料"}],"language":"zh","publisherId":"clgc2008z1080","title":"<span style=\"color:red\">席</span>夫碱在隐身材料中的应用前景","volume":"","year":"2008"},{"abstractinfo":"咔唑经过亚硝基化后在醋酸溶液中用锌粉还原得到9-氨基咔唑,后者在弱酸催化下与不同取代芳醛反应,合成了9种新型的咔唑<span style=\"color:red\">席</span>夫碱,收率63%～87%.采用红外光谱、核磁共振谱、质谱和元素分析等测试技术确证了它们的结构.初步生物活性测试结果表明,目标化合物具有较好的抗菌活性,其中化合物3和化合物7对测试菌种的抑菌率高于85%.","authors":[{"authorName":"李中华","id":"142e4eeb-4954-41ac-89ea-a0514c353ff5","originalAuthorName":"李中华"},{"authorName":"李佳凤","id":"92ceaf29-7578-49da-85e5-fe8c93d7aeb7","originalAuthorName":"李佳凤"},{"authorName":"汪焱钢","id":"e4a82b1c-e5e3-4a88-a1b0-a67b35ff57b0","originalAuthorName":"汪焱钢"}],"doi":"10.3969/j.issn.1000-0518.2007.09.023","fpage":"1074","id":"4199da53-d5fc-4fcd-93cb-014b67baff1f","issue":"9","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"3f78747c-89d0-4bc2-85d4-1ecbef525fa2","keyword":"氨基咔唑","originalKeyword":"氨基咔唑"},{"id":"13426735-80f7-4316-af6b-18fbff7ffde3","keyword":"芳醛","originalKeyword":"芳醛"},{"id":"3dd820b0-30e2-45b4-8e4a-9912a4fd7aa8","keyword":"<span style=\"color:red\">席</span>夫碱","originalKeyword":"席夫碱"},{"id":"c6bdc804-cea7-42cc-bde1-ac72868e7922","keyword":"合成","originalKeyword":"合成"},{"id":"bd86a649-0ee4-4e86-a855-3d2a18220c1c","keyword":"抗菌活性","originalKeyword":"抗菌活性"}],"language":"zh","publisherId":"yyhx200709023","title":"咔唑<span style=\"color:red\">席</span>夫碱的合成及抗菌活性","volume":"24","year":"2007"},{"abstractinfo":"利用自组装技术使<span style=\"color:red\">席</span>夫碱在铜表面自组装成膜，用扫描电子显微镜（SEM）、交流阻抗法及量子化学法研究了<span style=\"color:red\">席</span>夫碱结构对Cu缓蚀作用的影响。结果表明:<span style=\"color:red\">席</span>夫碱类化合物在发挥其活性时应以接受电子为主，此类化合物的亚胺或甲亚胺特性基团（-RC=N—）和苯环上的-OH是该类化合物的主要活性区，<span style=\"color:red\">席</span>夫碱苯环的-H被给电子基团取代会提高对Cu的缓蚀效率，且取代基团越靠进-C=N-，形成的螯合物越稳定，缓蚀效率越高。","authors":[{"authorName":"陈玉红","id":"9d1df174-df9a-4ff9-afd8-58665ca47e3f","originalAuthorName":"陈玉红"},{"authorName":"唐致远","id":"fb43909a-a5a1-4cf7-9c3c-3ff18a8ea684","originalAuthorName":"唐致远"},{"authorName":"童汝亭","id":"f6e4fddc-361f-4982-9baf-e9f281788864","originalAuthorName":"童汝亭"}],"categoryName":"|","doi":"","fpage":"156","id":"4060c7a9-20ac-43ab-8eb9-959148929c44","issue":"3","journal":{"abbrevTitle":"ZGFSYFHXB","coverImgSrc":"journal/img/cover/中国腐蚀封面19-3期-01.jpg","id":"81","issnPpub":"1005-4537","publisherId":"ZGFSYFHXB","title":"中国腐蚀与防护学报"},"keywords":[{"id":"b1ece50c-c70b-4e91-921a-b1291877d635","keyword":"<span style=\"color:red\">席</span>夫碱","originalKeyword":"席夫碱"},{"id":"2a811f18-28f7-4e29-91da-8ae2991ebc26","keyword":"corrosion inhibitors","originalKeyword":"corrosion inhibitors"},{"id":"256d5b96-49a8-4828-b218-71c6eb33c7af","keyword":"Self-Assembled Monolayer (SAM)","originalKeyword":"Self-Assembled Monolayer (SAM)"}],"language":"zh","publisherId":"1005-4537_2007_3_4","title":"<span style=\"color:red\">席</span>夫碱结构对铜缓蚀作用的影响","volume":"27","year":"2007"},{"abstractinfo":"阐述了长链共轭<span style=\"color:red\">席</span>夫碱吸波材料的吸波机理,综述了<span style=\"color:red\">席</span>夫碱吸波材料的电性能、磁性能、吸渡性能的研究现状,展望了该类吸波材料的电性能、磁性能以及吸波性能的改善研究情况,可通过设计合成长链共轭结构的<span style=\"color:red\">席</span>夫碱、引选手性螺旋结构、利用过渡金属或稀土金属配位这3个方面来提高<span style=\"color:red\">席</span>夫碱吸波材料的电性能、磁性能以及吸波性能.","authors":[{"authorName":"刘辉林","id":"2d8c274a-ec3f-4436-bd58-591249e14ef7","originalAuthorName":"刘辉林"},{"authorName":"刘崇波","id":"209e412b-ba69-4b5d-befe-89dd0956898b","originalAuthorName":"刘崇波"},{"authorName":"陈园","id":"7900b00b-a7c1-4a31-8f5e-681b1de31213","originalAuthorName":"陈园"},{"authorName":"徐荣臻","id":"1f8f4ebe-725a-4e3c-ad67-aac37e0d3931","originalAuthorName":"徐荣臻"}],"doi":"","fpage":"89","id":"5ad36684-ab3c-4cd8-951a-c1cc379123d2","issue":"13","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"07439a59-b37f-4dab-ab56-3e4819b5ef36","keyword":"长链共轭<span style=\"color:red\">席</span>夫碱","originalKeyword":"长链共轭席夫碱"},{"id":"7e30d9a3-2f00-48fd-8970-c6ab8f6a8df1","keyword":"电性能","originalKeyword":"电性能"},{"id":"c8d6127d-ff73-44ef-8912-20b865b0b3d5","keyword":"磁性能","originalKeyword":"磁性能"},{"id":"993a1dfd-c291-42f4-982c-adaac32ae1f3","keyword":"吸波材料","originalKeyword":"吸波材料"}],"language":"zh","publisherId":"cldb201213018","title":"长链共轭<span style=\"color:red\">席</span>夫碱吸波材料的研究进展","volume":"26","year":"2012"},{"abstractinfo":"用自组装技术使<span style=\"color:red\">席</span>夫碱在cu表面自组装成膜,用扫描电子显微镜(SEM)、交流阻抗方法及量子化学法研究了<span style=\"color:red\">席</span>夫碱结构对Cu缓蚀作用的影响.结果表明:<span style=\"color:red\">席</span>夫碱类化合物在发挥其活性时应以接受电子为主,此类化合物的亚胺或甲亚胺特性基团(-RC=N-)和苯环上的-OH是该类化合物的主要活性区,<span style=\"color:red\">席</span>夫碱苯环的-H被给电子基团取代会提高对Cu的缓蚀效率,且取代基团越靠进-C=N-,形成的螯合物越稳定,缓蚀效率越高.","authors":[{"authorName":"陈玉红","id":"258d36c6-701f-4d9c-b0ca-ae839e26a0ce","originalAuthorName":"陈玉红"},{"authorName":"唐致远","id":"b6f5b28e-14ff-4f29-8bed-f6199437f796","originalAuthorName":"唐致远"},{"authorName":"童汝亭","id":"150dcd29-e507-4635-9610-93252b714ef8","originalAuthorName":"童汝亭"},{"authorName":"王庆飞","id":"d9d6a16c-c9dc-42b2-b036-3658cdc45d42","originalAuthorName":"王庆飞"}],"doi":"10.3969/j.issn.1005-4537.2007.03.007","fpage":"156","id":"d24e42af-5994-43cd-8929-28b904a4d823","issue":"3","journal":{"abbrevTitle":"ZGFSYFHXB","coverImgSrc":"journal/img/cover/中国腐蚀封面19-3期-01.jpg","id":"81","issnPpub":"1005-4537","publisherId":"ZGFSYFHXB","title":"中国腐蚀与防护学报"},"keywords":[{"id":"e33a0034-bbcb-4314-b12e-49d65d46db6b","keyword":"<span style=\"color:red\">席</span>夫碱","originalKeyword":"席夫碱"},{"id":"c5783526-4338-4f97-a114-af29aef19012","keyword":"缓蚀剂","originalKeyword":"缓蚀剂"},{"id":"b55723df-bc72-40ed-bc28-bbf938f6aa39","keyword":"自组装膜","originalKeyword":"自组装膜"}],"language":"zh","publisherId":"zgfsyfhxb200703007","title":"<span style=\"color:red\">席</span>夫碱结构对Cu缓蚀作用的影响","volume":"27","year":"2007"},{"abstractinfo":"分别合成了小分子共轭结构、长链非共轭结构和长链共轭结构三种不同结构<span style=\"color:red\">席</span>夫碱及其相应的铁盐,采用IR、GPC、DSC对合成产物进行表征并测定了三种不同结构<span style=\"color:red\">席</span>夫碱及其相应铁盐的电导率和红外发射率.结果表明,长链共轭结构<span style=\"color:red\">席</span>夫碱及其铁盐具有最高的电导率和最低的红外发射率,说明长链共轭结构<span style=\"color:red\">席</span>夫碱及其铁盐具有优良的红外隐身性能.","authors":[{"authorName":"胡映雪","id":"9855d217-db74-4292-be56-577c803bdca7","originalAuthorName":"胡映雪"},{"authorName":"庄海燕","id":"058b7baa-7921-46e6-839e-85d4ee500283","originalAuthorName":"庄海燕"},{"authorName":"徐国跃","id":"43230a12-db25-4fc1-b78e-80b395779959","originalAuthorName":"徐国跃"},{"authorName":"燕刘军","id":"d9bdbd06-9e79-44b2-ac76-3e2c7d095a05","originalAuthorName":"燕刘军"}],"doi":"","fpage":"55","id":"83b4f64b-8255-4b86-b345-6a6bae0f9f86","issue":"1","journal":{"abbrevTitle":"CLKFYYY","coverImgSrc":"journal/img/cover/CLKFYYY.jpg","id":"10","issnPpub":"1003-1545","publisherId":"CLKFYYY","title":"材料开发与应用"},"keywords":[{"id":"dd1e6fde-c81b-483a-b807-b3d835ecfccf","keyword":"<span style=\"color:red\">席</span>夫碱","originalKeyword":"席夫碱"},{"id":"f768574e-fe5f-4aaa-9379-de8ff8c14d24","keyword":"共轭结构","originalKeyword":"共轭结构"},{"id":"46798c68-51d0-44ac-8d24-40d85294ea17","keyword":"电导率","originalKeyword":"电导率"},{"id":"f4c0faea-e667-484a-9549-b5c24e4a1433","keyword":"红外发射率","originalKeyword":"红外发射率"}],"language":"zh","publisherId":"clkfyyy201601013","title":"不同结构<span style=\"color:red\">席</span>夫碱及其铁盐的合成与红外隐身性能研究","volume":"31","year":"2016"}],"totalpage":17,"totalrecord":170}