{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"在水／二甲基亚砜(DMSO)的混合溶液体系中,利用自组装方法,使5,10,15,20-四苯基卟琳铟(InTPP)分子聚集成纳米材料,并研究了其最优制备温度为50℃.通过场发射扫描电子显微镜(FE-SEM)对铟卟啉纳米材料的表面形貌进行了研究,可获得粒径为100～200nm的棒状铟卟啉纳米材料.利用紫外-可见光谱分析了铟卟啉单体与纳米材料光学性质的差别:在紫外-可见光谱中,铟卟啉纳米分散体系的Soret带吸收峰从原来的423nm分别红移到433和453nm,吸光值明显减小,峰形呈劈裂状且明显变宽.利用紫外-可见光谱对铟卟啉的光学检测性能进行了研究,将铟卟啉单体和纳米溶液体系对低浓度甲基膦酸二甲酯(DMMP)的检测效果进行了对比,结果显示铟卟啉纳米溶液体系的检测效果明显优于单体.","authors":[{"authorName":"侯长军","id":"b7445b76-a669-4f50-aaa8-561823d248db","originalAuthorName":"侯长军"},{"authorName":"刘琛","id":"d67962d7-f2af-41a9-8cee-2f952bc61f4e","originalAuthorName":"刘琛"},{"authorName":"霍丹群","id":"a571b653-2af2-493b-94af-078352a2d2ae","originalAuthorName":"霍丹群"},{"authorName":"法焕宝","id":"65883c03-8a52-4137-8eee-049dd0bcf9cd","originalAuthorName":"法焕宝"},{"authorName":"杨眉","id":"4dcee122-12ba-40a2-8d5c-8328e1e21bd5","originalAuthorName":"杨眉"},{"authorName":"<span style=\"color:red\">向</span><span style=\"color:red\">芸</span><span style=\"color:red\">颉</span>","id":"a82ff802-ecf5-491d-99cc-2d8457a500ff","originalAuthorName":"向芸颉"},{"authorName":"宋坤","id":"f628f161-fae6-4630-81b2-7ad522b9117d","originalAuthorName":"宋坤"},{"authorName":"陈泳池","id":"d93c69f0-8286-434e-a620-c7a57a70ecca","originalAuthorName":"陈泳池"},{"authorName":"卢中明","id":"c11c6f44-cb44-4589-a176-36ab5102cb92","originalAuthorName":"卢中明"}],"doi":"","fpage":"1155","id":"d1e34b99-ec3a-44ce-97c0-489969a28114","issue":"6","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"2c3a3a8b-ccf1-422c-8948-348023cb8778","keyword":"铟卟啉","originalKeyword":"铟卟啉"},{"id":"dc55bd49-3adb-43df-a01f-f0cc56cb3ac8","keyword":"纳米材料","originalKeyword":"纳米材料"},{"id":"8889647c-d1ae-4769-9856-9d865992198f","keyword":"检测","originalKeyword":"检测"},{"id":"e38f344d-b2f2-4846-a959-b12fab1d8706","keyword":"甲基膦酸二甲酯","originalKeyword":"甲基膦酸二甲酯"},{"id":"18a18529-956a-4410-8e82-e6d3df066d85","keyword":"光学性能","originalKeyword":"光学性能"}],"language":"zh","publisherId":"gncl201106050","title":"四苯基卟琳铟纳米材料的制备及其光学传感性能研究","volume":"42","year":"2011"},{"abstractinfo":"在水/乙醇混合溶液体系中,利用自组装方法,使5-对磺酸基苹基-10,15,20-三苯基卟啉(TPPS1)分子聚集成功能化卟啉纳米材料.利用AFM、SEM、FE-SEM对卟啉纳米材料表面形貌性质及样品处理条件进行了研究:可获得50～70nm不同粒径的卟啉纳米材料;通过控制、调节样品的处理条件,可实现纳米材料尺寸的可控.利用紫外可见光谱和荧光光谱分析自组装卟啉与卟啉单体光学性质的差别:在紫外-可见光谱中,自组装卟啉Soret带吸收峰从原来的412nm分别蓝移和红移到361和451nm,呈现明显的劈裂状,且峰形变宽.以上特征性变化预示了卟啉纳米材料的形成;在荧光光谱中,纳米卟啉的荧光强度以及荧光量子产率分别约为未纳米化TPPS1单体的4和3倍,体现出良好的光敏性能,可作优良的光敏元件及光敏材料.","authors":[{"authorName":"侯长军","id":"736cb153-23c8-4374-9b62-8db5cd760b8c","originalAuthorName":"侯长军"},{"authorName":"<span style=\"color:red\">向</span><span style=\"color:red\">芸</span><span style=\"color:red\">颉</span>","id":"472481b7-e22c-4a6f-b860-c15c48463ad4","originalAuthorName":"向芸颉"},{"authorName":"法焕宝","id":"056e6a40-1556-435a-a074-aa2483e5e338","originalAuthorName":"法焕宝"},{"authorName":"霍丹群","id":"b5f98bb9-e605-4513-ae43-f928cc0ac943","originalAuthorName":"霍丹群"},{"authorName":"罗小刚","id":"2e010593-7031-44bf-8854-5eebecedc982","originalAuthorName":"罗小刚"},{"authorName":"杨军","id":"d4ca59bc-0749-4853-acb4-0a02862d750f","originalAuthorName":"杨军"},{"authorName":"侯冰峰","id":"4ee9801e-5cbd-4153-aad6-7f8b3086f85b","originalAuthorName":"侯冰峰"}],"doi":"","fpage":"1425","id":"c9b29f25-bb1a-4f80-bd29-639a0f40a0db","issue":"9","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"9d22a516-62e2-417b-8e7e-66c338ca4c6d","keyword":"卟啉","originalKeyword":"卟啉"},{"id":"c1d6ea29-e0a6-4057-a10a-2b99fc565f08","keyword":"自组装","originalKeyword":"自组装"},{"id":"d756f69d-9c97-4b60-ae83-18518cf4e066","keyword":"纳米材料","originalKeyword":"纳米材料"},{"id":"cbbbfc8a-33d8-4dda-8e4f-cac37a9619fe","keyword":"表面形貌","originalKeyword":"表面形貌"},{"id":"3ab14c31-2d30-4375-8e63-3b613c97b0c2","keyword":"光学性质","originalKeyword":"光学性质"}],"language":"zh","publisherId":"gncl200909004","title":"新型自组装卟啉纳米材料及其光学性质研究","volume":"40","year":"2009"},{"abstractinfo":"利用φ映射方法得出了计算<span style=\"color:red\">向</span>错线自由能公式和<span style=\"color:red\">向</span>错强度为m=±1的<span style=\"color:red\">向</span>错点自由能公式,从而弥补了挖掉奇异区域来估算自由能的不足.研究结果表明,液晶在有<span style=\"color:red\">向</span>错线的结构中指向矢场更多地出现正的<span style=\"color:red\">向</span>错强度状态.随着k24的增大,m=+1的<span style=\"color:red\">向</span>错点的自由能将降低,而m=-1的<span style=\"color:red\">向</span>错点的自由能将增大.","authors":[{"authorName":"王玉生","id":"053c83a3-3887-4a77-8575-8454349afb86","originalAuthorName":"王玉生"},{"authorName":"宋纳红","id":"b19130ea-203a-45f7-b7ad-157cdd6503dc","originalAuthorName":"宋纳红"}],"doi":"10.3969/j.issn.1007-2780.2008.03.001","fpage":"261","id":"ed511536-4fcb-44c2-b271-be179d20e381","issue":"3","journal":{"abbrevTitle":"YJYXS","coverImgSrc":"journal/img/cover/YJYXS.jpg","id":"72","issnPpub":"1007-2780","publisherId":"YJYXS","title":"液晶与显示   "},"keywords":[{"id":"d2294ae8-fdf7-4f77-8306-063386c66b68","keyword":"指向矢","originalKeyword":"指向矢"},{"id":"a9151462-827f-4277-8dff-4643f9165c69","keyword":"<span style=\"color:red\">向</span>错线","originalKeyword":"向错线"},{"id":"2e906500-cb21-41b2-ad6c-a858ce0a1b3e","keyword":"自由能","originalKeyword":"自由能"}],"language":"zh","publisherId":"yjyxs200803001","title":"<span style=\"color:red\">向</span>列相液晶中<span style=\"color:red\">向</span>错线和<span style=\"color:red\">向</span>错点自由能的计算","volume":"23","year":"2008"},{"abstractinfo":"高炉冶炼过程中炉温是影响技术经济指标的关键参数，保持合理的炉温是高炉稳定顺行的关键因素。采用某炼铁厂在线采集的数据，通过核主元分析对建模数据进行预处理，根据相关系数选定模型参数，确定参数对炉温的滞后时间，基于支持向量机建立了高炉<span style=\"color:red\">向</span>凉、<span style=\"color:red\">向</span>热预测诊断模型。通过实例验证，该模型具有很高的精度。","authors":[{"authorName":"崔桂梅，鄢常亮，关英辉","id":"740c5bca-7d7c-402a-84f2-660f7318cabc","originalAuthorName":"崔桂梅，鄢常亮，关英辉"}],"categoryName":"|","doi":"","fpage":"18","id":"278e0281-8164-4137-8988-a748ae05bf7c","issue":"7","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"25f73097-f2c9-4d30-b5e4-6686e52d901b","keyword":"高炉 ","originalKeyword":"高炉 "},{"id":"9303b771-83e7-4d60-b648-a789337fd7aa","keyword":" SVM ","originalKeyword":" SVM "},{"id":"e4aaa5dd-8ef5-4a50-8dc7-76d9fecf58f8","keyword":" KPCA ","originalKeyword":" KPCA "},{"id":"b89ff7d3-c84f-45fb-bc5c-77383dee3099","keyword":" prediction of furnace temperature","originalKeyword":" prediction of furnace temperature"}],"language":"zh","publisherId":"1001-0963_2011_7_14","title":"基于支持向量机的高炉<span style=\"color:red\">向</span>凉、<span style=\"color:red\">向</span>热炉况预测","volume":"23","year":"2011"},{"abstractinfo":"高炉冶炼过程中炉温是影响技术经济指标的关键参数，保持合理的炉温是高炉稳定顺行的关键因素。采用某炼铁厂在线采集的数据，通过核主元分析对建模数据进行预处理，根据相关系数选定模型参数，确定参数对炉温的滞后时间，基于支持向量机建立了高炉<span style=\"color:red\">向</span>凉、<span style=\"color:red\">向</span>热预测诊断模型。通过实例验证，该模型具有很高的精度。","authors":[{"authorName":"崔桂梅","id":"e2188a10-9e27-4aa7-bbad-f11690034f91","originalAuthorName":"崔桂梅"},{"authorName":"鄢常亮","id":"8b1f8f58-1329-4316-ab61-8355b4f954ef","originalAuthorName":"鄢常亮"},{"authorName":"关英辉","id":"a7294aed-9e02-4a0b-99cd-b9a1eeba8bb6","originalAuthorName":"关英辉"}],"doi":"","fpage":"18","id":"fc5b88e8-e5c6-4f4d-80b1-faeab607d30c","issue":"7","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"983c3d17-c23a-44ff-a689-ec98b6ff05d1","keyword":"高炉","originalKeyword":"高炉"},{"id":"bc6ee7ba-8fd8-4583-8a5b-62fc6459f7a2","keyword":"支持向量机","originalKeyword":"支持向量机"},{"id":"5aefe48c-6f83-4d3b-8aad-6ad9c8b58e2e","keyword":"核主元分析","originalKeyword":"核主元分析"},{"id":"0755a096-b9d0-46d7-b56b-7082b0f3e186","keyword":"炉温预测","originalKeyword":"炉温预测"}],"language":"zh","publisherId":"gtyjxb201107005","title":"基于支持向量机的高炉<span style=\"color:red\">向</span>凉、<span style=\"color:red\">向</span>热炉况预测","volume":"23","year":"2011"},{"abstractinfo":"为评估三<span style=\"color:red\">向</span>碳/碳材料的烧蚀性能,在北京空气动力研究所研制的FD-04F电弧加热器上对三<span style=\"color:red\">向</span>碳/碳材料进行了滑行试验,测出了三<span style=\"color:red\">向</span>碳/碳材料的转捩压力.试验结果表明:滑行试验在测量转捩压力方面是有效的,并给出了三<span style=\"color:red\">向</span>碳/碳模型的转捩压力数据和最终外形形状.","authors":[{"authorName":"张骞","id":"5abb8c81-8d09-42b1-88dc-ebfd60d5ab7f","originalAuthorName":"张骞"},{"authorName":"陆兴煜","id":"13a231be-12cb-4518-ad69-d3e109da8b41","originalAuthorName":"陆兴煜"},{"authorName":"程淑芬","id":"2920e07f-1f9b-4a68-a811-f1eac97571a2","originalAuthorName":"程淑芬"}],"doi":"10.3969/j.issn.1007-2330.2003.02.014","fpage":"58","id":"69039f4e-2398-44dd-b95a-fe3740d66548","issue":"2","journal":{"abbrevTitle":"YHCLGY","coverImgSrc":"journal/img/cover/YHCLGY.jpg","id":"77","issnPpub":"1007-2330","publisherId":"YHCLGY","title":"宇航材料工艺   "},"keywords":[{"id":"1e39c8c3-6697-49c9-9181-c1482bd3ee03","keyword":"烧蚀性能","originalKeyword":"烧蚀性能"},{"id":"dc791042-1799-458c-ba36-9e5234cae600","keyword":"滑行试验","originalKeyword":"滑行试验"},{"id":"3c7660e6-b2c6-4a68-8818-6d595f306a6e","keyword":"转捩压力","originalKeyword":"转捩压力"}],"language":"zh","publisherId":"yhclgy200302014","title":"三<span style=\"color:red\">向</span>碳/碳材料转捩压力的测量","volume":"33","year":"2003"},{"abstractinfo":"采用一种金相和RO-XRD相结合的方法,快速、准确地测定Mo-Nb合金单晶的晶<span style=\"color:red\">向</span>,并对晶<span style=\"color:red\">向</span>品质做出精确的表征.所测Mo合金单晶,其(111)晶面衍射角的测试值与计算值基本一致,其晶<span style=\"color:red\">向</span>偏离角分别为0.73°和0.91°,与电子背散射衍射法测试的结果一致,晶<span style=\"color:red\">向</span>分散度仅为1°左右.","authors":[{"authorName":"胡忠武","id":"a5388297-9eee-4014-8254-072dfb769f78","originalAuthorName":"胡忠武"},{"authorName":"李中奎","id":"31d6fd7e-454b-426b-bd41-f3f315932d39","originalAuthorName":"李中奎"},{"authorName":"郭林江","id":"f5c9cc1b-5241-4ae8-87b8-56f48a2be8bf","originalAuthorName":"郭林江"},{"authorName":"殷涛","id":"fe5746fe-9b0c-4435-a37d-882c003e26cd","originalAuthorName":"殷涛"},{"authorName":"郭振祺","id":"68282c87-701d-4ebb-bd0c-b2a4d6abcd8c","originalAuthorName":"郭振祺"}],"doi":"","fpage":"2006","id":"fafc98f9-b445-46bd-8461-6de7863fd719","issue":"11","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"9540e06e-ad7c-469d-8845-b3d8d329d898","keyword":"单晶","originalKeyword":"单晶"},{"id":"24c87c68-7b76-42cc-abf3-220985989c6b","keyword":"RO-XRD法","originalKeyword":"RO-XRD法"},{"id":"125673d5-5034-458e-858f-9765d1be57cc","keyword":"金相","originalKeyword":"金相"},{"id":"2263b0e4-0137-4fe7-81aa-577d157a2551","keyword":"晶<span style=\"color:red\">向</span>偏离角","originalKeyword":"晶向偏离角"}],"language":"zh","publisherId":"xyjsclygc201111027","title":"Mo-Nb合金单晶晶<span style=\"color:red\">向</span>测定和表征","volume":"40","year":"2011"},{"abstractinfo":"研究了1Cr21Ni5Ti双相不锈钢γ相在0℃以下的马氏体相变,着重测试和分析了相邻板条马氏体间位<span style=\"color:red\">向</span>关系.结果表明:马氏体与母相奥氏体之间的位<span style=\"color:red\">向</span>关系(K-S或N-W关系)决定了相邻板条马氏体间的位<span style=\"color:red\">向</span>关系,K-S或N-W关系条件下板条马氏体变态使得相邻板条马氏体间呈多种位<span style=\"color:red\">向</span>关系.交替排列的互为孪晶的马氏体板条间不存在残留奥氏体,这是马氏体自协调形成的结果,这一孪晶位<span style=\"color:red\">向</span>关系与K-S关系马氏体变态的孪晶关系不同.","authors":[{"authorName":"杨卓越","id":"bbcc2943-0327-4671-b01b-3f06377e377d","originalAuthorName":"杨卓越"},{"authorName":"陈嘉砚","id":"772ac9c2-208a-4f67-86af-f8b32462360e","originalAuthorName":"陈嘉砚"},{"authorName":"苏杰","id":"cc203fda-9c30-41f8-9784-ecca77663f38","originalAuthorName":"苏杰"},{"authorName":"张永权","id":"11fb9949-8cf9-430f-9169-857b9b024a65","originalAuthorName":"张永权"}],"doi":"10.3969/j.issn.1009-6264.2004.06.009","fpage":"35","id":"9a782b40-9cd5-4ced-8fb9-0e120652080c","issue":"6","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"75122f53-59e9-4e84-ae1a-db945e20b97d","keyword":"双相不锈钢","originalKeyword":"双相不锈钢"},{"id":"a4a8d9cb-6c3e-4d87-93c7-cb7b2910644d","keyword":"马氏体相变","originalKeyword":"马氏体相变"},{"id":"e199f506-ab58-454a-9c81-cce35afc108c","keyword":"位<span style=\"color:red\">向</span>关系","originalKeyword":"位向关系"},{"id":"06063bce-aadb-41e2-8692-da2fb7d71da1","keyword":"K-S关系","originalKeyword":"K-S关系"},{"id":"13228e2a-1189-4253-b5ab-4f2e4bcb0343","keyword":"N-W关系","originalKeyword":"N-W关系"}],"language":"zh","publisherId":"jsrclxb200406009","title":"相邻板条马氏体间位<span style=\"color:red\">向</span>关系的TEM研究","volume":"25","year":"2004"},{"abstractinfo":"取向硅钢成品的晶粒尺寸非常大,其易磁化方向[001]晶<span style=\"color:red\">向</span>对于轧<span style=\"color:red\">向</span>的偏差角度对其磁性能影响极大.本文介绍了取向硅钢二次再结晶后成品晶粒位<span style=\"color:red\">向</span>的几种测定方法,包括侵蚀法、劳厄法、OIM法、极图法和非对称X射线衍射法等,并对这几种测量方法进行了比较.","authors":[{"authorName":"张贞贞","id":"6b5b308b-c8d3-4ff6-b8af-83138d62b9d4","originalAuthorName":"张贞贞"},{"authorName":"任卫","id":"8ec64ff3-e2e7-42a1-822c-15a0d5ce191f","originalAuthorName":"任卫"},{"authorName":"方建锋","id":"c9c13f97-5a9e-4565-a4d3-57f9ecbb6f38","originalAuthorName":"方建锋"}],"doi":"","fpage":"6","id":"76e358b3-775e-493e-8c65-c14e0af2f329","issue":"4","journal":{"abbrevTitle":"JSGNCL","coverImgSrc":"journal/img/cover/JSGNCL.jpg","id":"46","issnPpub":"1005-8192","publisherId":"JSGNCL","title":"金属功能材料"},"keywords":[{"id":"78cc7b9d-5465-4eab-bc18-c6f952667d17","keyword":"取向硅钢","originalKeyword":"取向硅钢"},{"id":"4fee412f-4c6f-412d-a9d2-f610390a2fa5","keyword":"[001]晶<span style=\"color:red\">向</span>","originalKeyword":"[001]晶向"},{"id":"2f1b953d-47d8-4928-a63e-1f8e72699871","keyword":"位<span style=\"color:red\">向</span>测定","originalKeyword":"位向测定"}],"language":"zh","publisherId":"jsgncl201104002","title":"取向硅钢成品晶粒的位<span style=\"color:red\">向</span>测定方法","volume":"18","year":"2011"},{"abstractinfo":"针对RPM管环<span style=\"color:red\">向</span>拉伸强度测试中采用板条状试样所存在的问题,理论分析和试验研究表明通过改变试样形状和尺寸可明显改善测试结果.","authors":[{"authorName":"周仕刚","id":"25e1dccf-f4ca-4985-9ee9-a9d2409754c8","originalAuthorName":"周仕刚"},{"authorName":"付强","id":"48c506a8-d15f-4670-b25d-3f6dbe98bd2a","originalAuthorName":"付强"}],"doi":"10.3969/j.issn.1003-0999.2004.06.001","fpage":"3","id":"20ca2e1a-4260-4788-91e8-03bc231574ef","issue":"6","journal":{"abbrevTitle":"BLGFHCL","coverImgSrc":"journal/img/cover/BLGFHCL.jpg","id":"6","issnPpub":"1003-0999","publisherId":"BLGFHCL","title":"玻璃钢/复合材料"},"keywords":[{"id":"59348e22-bdd0-453b-b57b-cc32da9380dc","keyword":"RPM管","originalKeyword":"RPM管"},{"id":"2ea48636-3a62-4645-957d-a9b862131c44","keyword":"环<span style=\"color:red\">向</span>拉伸强度","originalKeyword":"环向拉伸强度"},{"id":"725aaab8-fcb5-43f3-8a36-22381108fbec","keyword":"测试方法","originalKeyword":"测试方法"}],"language":"zh","publisherId":"blgfhcl200406001","title":"RPM管环<span style=\"color:red\">向</span>拉伸强度的测试","volume":"","year":"2004"}],"totalpage":775,"totalrecord":7743}