{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"建立了溶剂型涂料中三氯苯3种同分异构体(1,3,5-三氯苯、1,2,4-三氯苯、1,2,3-三氯苯)的气相色谱-质谱检测方法.研究了丙酮、正己烷、四氢呋喃和乙酸乙酯4种溶剂对涂料中三氯苯的提取以及分离效果.配制三氯苯浓度分别为1 mg/L、5 mg/L、10 mg/L、20 mg/L、50 mg/L、100 mg/L的标准溶液,以选择离子(SIM)模式进行定性及定量分析.以三氯苯提取m/z=180.0离子峰面积为横坐标,以对应的三氯苯浓度(mg/L)为纵坐标,绘制标准曲线.3种同分异构体对应曲线的相关系数均大于0.999,在1～100 mg/L浓度范围内线性良好;样品平均回收率为95.9％ ～ 107.6％;相对标准偏差(RSD,n=6)在1.44％～4.33％之间.样品中1,3,5-三氯苯、1,2,4-三氯苯、1,2,3-三氯苯检出限(LOD,S/N=3)分别为2 mg/kg、2 mg/kg、2 mg/kg.","authors":[{"authorName":"魏宇锋","id":"47d69a13-cf02-4297-947e-c8c296def3a2","originalAuthorName":"魏宇锋"},{"authorName":"王文青","id":"94cb86ca-6d56-498d-94a9-1f187ff67c95","originalAuthorName":"王文青"},{"authorName":"邱丰","id":"82ad6531-9417-448c-9d69-b6635a1090ae","originalAuthorName":"邱丰"},{"authorName":"<span style=\"color:red\">费</span><span style=\"color:red\">旭</span><span style=\"color:red\">东</span>","id":"d83a7668-9a05-4bba-8391-ebc5f5a9857e","originalAuthorName":"费旭东"},{"authorName":"张继<span style=\"color:red\">东</span>","id":"9bcc21f5-0bec-4392-8cf7-ba4172f5aa13","originalAuthorName":"张继东"}],"doi":"","fpage":"52","id":"338ece07-60f9-4981-aac2-855e4037ea85","issue":"1","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"212b7281-0142-472d-be53-4b16df0e594f","keyword":"溶剂型涂料","originalKeyword":"溶剂型涂料"},{"id":"ca1cef57-d6ad-450d-9ca6-7f9323ecd53d","keyword":"三氯苯","originalKeyword":"三氯苯"},{"id":"b318053f-7880-41f9-9af0-f58c6ff546b6","keyword":"气相色谱-质谱法","originalKeyword":"气相色谱-质谱法"},{"id":"f53b6b25-4074-4b1d-a198-edcc2491d65f","keyword":"检测","originalKeyword":"检测"}],"language":"zh","publisherId":"tlgy201401011","title":"气相色谱-质谱法测定溶剂型涂料中三氯苯的含量","volume":"44","year":"2014"},{"abstractinfo":"","authors":[{"authorName":"蒋海宁","id":"55ee14c6-5291-4fe0-bec5-59d86d4ed0b8","originalAuthorName":"蒋海宁"},{"authorName":"吴雄英","id":"41702405-fb40-46fc-8351-ecdf5860a2f1","originalAuthorName":"吴雄英"},{"authorName":"杨娟","id":"f196431f-ceba-4315-ab82-68331d2c218c","originalAuthorName":"杨娟"},{"authorName":"<span style=\"color:red\">费</span><span style=\"color:red\">旭</span><span style=\"color:red\">东</span>","id":"5400d7f9-cc9a-4684-83d7-95958007265b","originalAuthorName":"费旭东"},{"authorName":"施黎","id":"fb5cdfea-acc9-454e-8968-bebb68a9a3d4","originalAuthorName":"施黎"},{"authorName":"唐敏峰","id":"a525877f-41ab-491e-a5aa-dc13df661854","originalAuthorName":"唐敏峰"}],"doi":"10.3321/j.issn:1000-8713.2006.03.029","fpage":"321","id":"8f6461ab-f924-449d-89c7-d2da9ff1647c","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"9d4c80c3-918d-46eb-a7f4-44d17a914a91","keyword":"毛细管气相色谱法(CGC)","originalKeyword":"毛细管气相色谱法(CGC)"},{"id":"dca880ec-bfaf-423d-85ea-12e3cac92bcd","keyword":"有机磷杀虫剂(organophosphorus pesticide)","originalKeyword":"有机磷杀虫剂(organophosphorus pesticide)"},{"id":"806435e6-240b-41ae-9237-58ba164b8d81","keyword":"含脂羊毛(greasy wool)","originalKeyword":"含脂羊毛(greasy wool)"},{"id":"a282a740-56bd-41e9-9c66-9ec3b57c15ed","keyword":"残留(residues)","originalKeyword":"残留(residues)"}],"language":"zh","publisherId":"sp200603029","title":"气相色谱法测定含脂羊毛中有机磷杀虫剂的残留量","volume":"24","year":"2006"},{"abstractinfo":"建立了离子色谱-抑制型电导检测同时测定食品级润滑油中C1-、NO3-、sO4-3种代表性无机阴离子的方法.样品经50％ (v/v)甲醇水溶液超声提取,离心后所得下层水相用0.22 μm混合纤维过滤膜净化,以15 mmoL/LKOH溶液为淋洗液,采用抑制型电导检测器进行检测,外标法定量.在上述条件下,C1-、NO3-、SO24-3种无机阴离子在0.10～20.00 mg/L范围内具有良好的线性关系(R2＞0.999);检出限(S/N=3)为0.01～0.03 mg/kg;在1.00、5.00、10.00 mg/kg添加水平下,实际样品中3种阴离子的加标回收率为90.0％ ～ 103.6％,相对标准偏差为2.8％～5.7％.结果表明,该方法无需燃烧、灰化油相基质等繁琐耗时的前处理过程,可以快速、准确定量测定食品级润滑油中C1-、NO3-、SO24-3种无机阴离子的含量,适用于润滑油等油品中痕量无机阴离子的同时分离与测定.","authors":[{"authorName":"张丽媛","id":"b1e67171-1f3b-439d-a517-a243303f90ac","originalAuthorName":"张丽媛"},{"authorName":"<span style=\"color:red\">费</span><span style=\"color:red\">旭</span><span style=\"color:red\">东</span>","id":"8cc04595-4d02-4ffe-a9db-fe5b7904df33","originalAuthorName":"费旭东"},{"authorName":"邱丰","id":"c1765f5c-378b-4a3c-8c19-986db2b77f9f","originalAuthorName":"邱丰"},{"authorName":"林苗","id":"e76fa4fa-1967-4cd5-8c8c-381a1e2ca809","originalAuthorName":"林苗"}],"doi":"10.3724/SP.J.1123.2014.10009","fpage":"164","id":"2c65cd6f-08b5-41e2-8a94-dd0cd536b7e7","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"7d8377d5-2db1-492c-ab16-c976f13371f1","keyword":"离子色谱","originalKeyword":"离子色谱"},{"id":"44d2a85c-0dc1-4fa5-b59e-59bae937c73d","keyword":"抑制型电导检测","originalKeyword":"抑制型电导检测"},{"id":"04ec9497-633a-4779-824b-c49360c03c19","keyword":"无机阴离子","originalKeyword":"无机阴离子"},{"id":"6e1c7292-e356-4a98-a50b-073a671bfb90","keyword":"食品级润滑油","originalKeyword":"食品级润滑油"}],"language":"zh","publisherId":"sp201502010","title":"离子色谱-抑制型电导检测法同时测定食品级润滑油中的3种无机阴离子","volume":"33","year":"2015"},{"abstractinfo":"班公湖-怒江成矿带跨班公湖-怒江缝合带两侧，是近年来发现的一条重要的多金属成矿带。商<span style=\"color:red\">旭</span>金矿床位于班公湖-怒江缝合带中段，主要矿体呈透镜状或脉状产于中-下侏罗统木嘎岗日群浅变质海相复理石建造中，受近东西向断裂构造控制。矿石类型以石英脉型为主，其次为蚀变岩型，近矿围岩蚀变较弱，蚀变类型包括硅化、绢云母化、绿泥石化、碳酸盐化等。矿石中金属矿物主要为自然金、黄铁矿及方铅矿；脉石矿物以石英、方解石以及黏土矿物为主。初步研究表明，该矿床主要受地层及构造因素控制，成因类型为造山型金矿床。在此基础上，初步总结了矿区的主要找矿标志，包括岩性及构造标志、蚀变标志、硫化物标志、化探异常及古采矿遗迹标志等，并认为区域上存在找到商<span style=\"color:red\">旭</span>式金矿床的可能。","authors":[{"authorName":"肖万峰","id":"1d451ac3-887c-4617-a0ca-158b639eee34","originalAuthorName":"肖万峰"},{"authorName":"李光明","id":"a43a9f64-db4e-4ae7-a4db-ad6b5c6fdf01","originalAuthorName":"李光明"},{"authorName":"黄瀚霄","id":"4bd70593-6e2d-4a4a-a476-a8499e8e8141","originalAuthorName":"黄瀚霄"},{"authorName":"马<span style=\"color:red\">东</span>","id":"62242f64-8b3e-453d-90b4-3cdd52646587","originalAuthorName":"马东"},{"authorName":"张智林","id":"4e3ebf94-f1d0-409d-a4e6-f99d952597d4","originalAuthorName":"张智林"},{"authorName":"曲扎","id":"e0763d49-69d4-429c-ba6a-eba9484badf0","originalAuthorName":"曲扎"}],"doi":"10.11792/hj20131005","fpage":"17","id":"64eb054f-8d90-414b-8571-cdbe479e8b5b","issue":"10","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"e38f1f96-a61b-4a64-b5d5-cf076ed042d1","keyword":"商<span style=\"color:red\">旭</span>金矿床","originalKeyword":"商旭金矿床"},{"id":"222c536e-17cf-4583-ac2e-eb9910f27ce7","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"84cc3253-435b-48e9-8036-2a247c1b10b7","keyword":"控矿因素","originalKeyword":"控矿因素"},{"id":"e472e283-83a4-4b15-bdbe-041026cc787a","keyword":"矿床成因","originalKeyword":"矿床成因"},{"id":"55fa1374-bf4f-4361-8758-6b26fa5c71d1","keyword":"找矿标志","originalKeyword":"找矿标志"},{"id":"b817b4f3-ad9b-4e53-b2d3-2fafe0695a73","keyword":"藏北","originalKeyword":"藏北"}],"language":"zh","publisherId":"huangj201310007","title":"藏北商<span style=\"color:red\">旭</span>金矿床控矿因素及其找矿标志","volume":"","year":"2013"},{"abstractinfo":"简要介绍了西气<span style=\"color:red\">东</span>输工程中水土腐蚀勘测的方法,给出了郑州至郸城高桥段水土腐蚀性勘测结果.","authors":[{"authorName":"阳光","id":"98eff96a-396f-44f7-8d60-a5b3a6f7cbc0","originalAuthorName":"阳光"},{"authorName":"罗心","id":"72bc340f-c870-42a0-8132-5ccb0128ac80","originalAuthorName":"罗心"},{"authorName":"高立群","id":"c4dcadc0-888b-4c91-aa15-736f24084f59","originalAuthorName":"高立群"}],"doi":"10.3969/j.issn.1005-748X.2003.01.008","fpage":"29","id":"1ec632dd-cb44-4bc0-9cbc-966f105209e7","issue":"1","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"c60892dc-9c4f-495c-8b15-af91b337bc52","keyword":"西气<span style=\"color:red\">东</span>输","originalKeyword":"西气东输"},{"id":"8fab1792-4cb9-4c17-a0e8-24806345f8aa","keyword":"腐蚀调查","originalKeyword":"腐蚀调查"},{"id":"45a2bd96-ff07-4711-b717-257888340e1f","keyword":"土壤","originalKeyword":"土壤"}],"language":"zh","publisherId":"fsyfh200301008","title":"西气<span style=\"color:red\">东</span>输沿线水土腐蚀勘测方法","volume":"24","year":"2003"},{"abstractinfo":"叙述了<span style=\"color:red\">东</span>坪金矿两步骤回采嗣后充填采矿法充填工艺,介绍了充填过程中的技术措施,并提出了进一步改进设想.","authors":[{"authorName":"米继武","id":"17a1ce88-4af7-4cab-b90d-f822327087fa","originalAuthorName":"米继武"},{"authorName":"王爱民","id":"dfbb35af-93fa-4566-9fe7-78d2f5297007","originalAuthorName":"王爱民"}],"doi":"10.3969/j.issn.1001-1277.2004.12.009","fpage":"26","id":"ecd72cec-bb85-430a-b6a2-7c9fd7bb030d","issue":"12","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"6e7f5db8-d8f2-4289-8cb9-f0315a0d8e52","keyword":"<span style=\"color:red\">东</span>坪金矿","originalKeyword":"东坪金矿"},{"id":"db07539b-6a4e-4661-b197-296901eb3435","keyword":"充填采矿法","originalKeyword":"充填采矿法"},{"id":"5b1d27ca-bb43-4b8a-9cdf-f570050726ff","keyword":"块石胶结充填","originalKeyword":"块石胶结充填"},{"id":"02f22f37-93c9-4b7f-8680-c503ae819fcd","keyword":"充填设施","originalKeyword":"充填设施"}],"language":"zh","publisherId":"huangj200412009","title":"<span style=\"color:red\">东</span>坪金矿充填采矿法充填工艺的实践","volume":"25","year":"2004"},{"abstractinfo":"水相<span style=\"color:red\">费</span>托合成可以在远低于传统温度下实现,其低温高效的特点使其具有重要的应用潜力.本文制备了水相稳定且可循环利用的Co纳米粒子并应用于水相<span style=\"color:red\">费</span>托反应,150 ℃下活性为7.4× 10-7 molco gco-1 s-1,C5+选择性接近40％,是目前纯钴水相<span style=\"color:red\">费</span>托合成的最好结果,而其它方法合成的催化剂在150 ℃时活性低下.对催化剂进行了粒径、结构、成分测定和原位红外光谱检测,研究了催化剂在反应中的重构过程和B掺杂效应.","authors":[{"authorName":"王航","id":"664e2d40-3fd6-466f-aa67-14883a611499","originalAuthorName":"王航"},{"authorName":"寇元","id":"21d0781c-3e0e-4716-a7f4-31bbc7a331c2","originalAuthorName":"寇元"}],"doi":"10.1016/S1872-2067(12)60674-3","fpage":"1914","id":"8d98a207-3dd9-4e4b-81b8-4ae593b3f44b","issue":"10","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报   "},"keywords":[{"id":"c3189787-6708-4a29-8a90-15f5dd9876ae","keyword":"水相<span style=\"color:red\">费</span>托合成","originalKeyword":"水相费托合成"},{"id":"b3183333-a1cc-4a58-97d3-cd2c99de8839","keyword":"钴纳米粒子","originalKeyword":"钴纳米粒子"},{"id":"82aa261a-ffaa-4080-9e21-1f6b9b336f7e","keyword":"硼掺杂","originalKeyword":"硼掺杂"},{"id":"87ac1b12-9e09-4cbe-8fef-1a67d894fc28","keyword":"原位红外光谱","originalKeyword":"原位红外光谱"}],"language":"zh","publisherId":"cuihuaxb201310017","title":"钴纳米粒子催化水相<span style=\"color:red\">费</span>托合成","volume":"34","year":"2013"},{"abstractinfo":"为了调查川气<span style=\"color:red\">东</span>送管道内的腐蚀状况，根据相关标准 NACE SP0110-2010对管道的内腐蚀环境参数进行了调查，并对管道内积水来源、水露点、管道临界角和清管作业进行了主要的分析。结果表明，川气<span style=\"color:red\">东</span>送管道已经发生了内腐蚀。","authors":[{"authorName":"尹恒","id":"92e5b1b7-04e7-40be-a0ed-2a210f9e2ec3","originalAuthorName":"尹恒"},{"authorName":"董华清","id":"821dbb6a-2984-4873-8a0e-16eb18a8a6af","originalAuthorName":"董华清"},{"authorName":"原徐杰","id":"7487eb97-7086-4d5f-a18f-360c7a2b035d","originalAuthorName":"原徐杰"},{"authorName":"陈维","id":"fab1dfb0-ad98-468b-8fcc-e6769a546d4d","originalAuthorName":"陈维"},{"authorName":"王方","id":"9380b86c-6eee-4597-bcb8-bc9e59fd84a8","originalAuthorName":"王方"},{"authorName":"李爱莲","id":"162c8942-42db-409c-a640-48e718514852","originalAuthorName":"李爱莲"}],"doi":"","fpage":"1051","id":"ec2028c9-9c90-493e-9173-f079691f2421","issue":"10","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"c20bb445-2097-4bb4-bb54-2060934d0144","keyword":"天然气管道","originalKeyword":"天然气管道"},{"id":"5afc5d61-8f48-4d2e-b43e-23fa50ae4a50","keyword":"内腐蚀","originalKeyword":"内腐蚀"},{"id":"004b4715-631b-4fc8-bba8-f4120a5c35f9","keyword":"水露点","originalKeyword":"水露点"},{"id":"a827f9d4-85be-46b6-805f-7fe7efd45726","keyword":"管道临界角","originalKeyword":"管道临界角"}],"language":"zh","publisherId":"fsyfh201410026","title":"川气<span style=\"color:red\">东</span>送管道内腐蚀调查分析","volume":"","year":"2014"},{"abstractinfo":"利用电化学方法对塔里木解放渠<span style=\"color:red\">东</span>油田采出水的腐蚀及点蚀特性进行研究,指出了控制腐蚀的主要因素,并有针对性地筛选出适宜的缓蚀剂.","authors":[{"authorName":"韩霞","id":"675e61dd-8962-4c96-a374-069c6c8eeaeb","originalAuthorName":"韩霞"},{"authorName":"刘娜","id":"ba522445-cf95-467f-a5ea-74ea77687ff5","originalAuthorName":"刘娜"}],"doi":"10.3969/j.issn.1005-748X.2000.03.004","fpage":"107","id":"738c9eb3-d0e0-495b-aadd-09e4ee8dc8bc","issue":"3","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"361bca07-bcb3-4068-84a3-6f4c1cb32606","keyword":"油田采出水","originalKeyword":"油田采出水"},{"id":"99fe1df9-b06b-4160-9928-e5be5e96c6b1","keyword":"腐蚀特性","originalKeyword":"腐蚀特性"},{"id":"3e3df87e-9946-46f6-8642-d2cc1191c973","keyword":"腐蚀控制","originalKeyword":"腐蚀控制"}],"language":"zh","publisherId":"fsyfh200003004","title":"塔里木解放渠<span style=\"color:red\">东</span>油田采出水腐蚀特性研究","volume":"21","year":"2000"},{"abstractinfo":"简要介绍了低温<span style=\"color:red\">费</span>托合成产物的分布；概述了低温<span style=\"color:red\">费</span>托合成产品中α-烯烃的分离技术，以及分离馏分制备Ⅳ类基础油PAO的研究；另外，对低温<span style=\"color:red\">费</span>托合成产品生产高端Ⅲ类基础油的研究现状进行了简要介绍。","authors":[{"authorName":"刘素丽","id":"3dfa113c-22a6-4aaa-ac7f-0731e55b0042","originalAuthorName":"刘素丽"},{"authorName":"殷志宝","id":"e6ab5c18-4d77-439a-8d82-e9c0e4ead181","originalAuthorName":"殷志宝"},{"authorName":"梁雪美","id":"e7cfb768-b722-4a04-b237-310ca0252b12","originalAuthorName":"梁雪美"},{"authorName":"袁炜","id":"932203c9-782a-40fd-9e8e-a22e89027331","originalAuthorName":"袁炜"},{"authorName":"罗春桃","id":"2b9d0e4e-2836-4bf2-aa77-ca4660021b04","originalAuthorName":"罗春桃"}],"doi":"","fpage":"98","id":"9fe61280-90ed-45e7-9af5-60ebf764f972","issue":"6","journal":{"abbrevTitle":"HCCLLHYYY","coverImgSrc":"journal/img/cover/HCCLLHYYY.jpg","id":"42","issnPpub":"1671-5381","publisherId":"HCCLLHYYY","title":"合成材料老化与应用"},"keywords":[{"id":"20bc1e39-f715-4d53-9c70-6b8f299ad4c0","keyword":"低温<span 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