{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用Li2B4O7和LiNO3为熔剂,LiBr作脱膜剂,熔融法制备样品;运用干扰曲线法通过迭次校正Ba,Ti,V,Cr,Mn各元素谱线重叠干扰,理论α系数法校正基体效应,<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法(XRF)分析了复杂体系炉渣中Na2O,MgO,Al2O3,SiO2,P2O5,K2O,CaO,TiO2,V2O5,Cr2O3,MnO,TFe,BaO 13种组分.该方法与化学法测定结果符合较好,10次制样测量各组分,相对标准偏差在0.15%～3.79%范围内.","authors":[{"authorName":"童晓民","id":"15ac4890-0d5c-48a1-b103-3eb8f8504413","originalAuthorName":"童晓民"},{"authorName":"赵宏风","id":"f058c702-7d03-42bc-8d2d-99fe937f011f","originalAuthorName":"赵宏风"},{"authorName":"黄春燕","id":"34b96eab-c0e2-41cf-aed0-a5ab22b981bb","originalAuthorName":"黄春燕"},{"authorName":"赵一波","id":"55077f9b-658a-4ef3-9f89-00e4376934be","originalAuthorName":"赵一波"}],"doi":"10.3969/j.issn.1000-7571.2005.06.004","fpage":"12","id":"f508acee-e01b-4a05-96e7-e07bfc65aecb","issue":"6","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"c729c143-d1c2-4dab-92ca-e303c25867b9","keyword":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>","originalKeyword":"X-射线荧光"},{"id":"3880f647-cc69-4300-bffe-a38529e6f72a","keyword":"炉渣","originalKeyword":"炉渣"},{"id":"9b3e7e0a-753e-4c62-a216-c515970e90bc","keyword":"干扰曲线法","originalKeyword":"干扰曲线法"},{"id":"324850c1-cdc9-422c-9fce-59abad57c059","keyword":"迭次校正法","originalKeyword":"迭次校正法"}],"language":"zh","publisherId":"yjfx200506004","title":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定炉渣中13种组分","volume":"25","year":"2005"},{"abstractinfo":"探讨了应用能量色散型<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱仪测定生铁中硅和磷的炉前快速分析方法.该方法所得测定结果与化学法测定结果或标样认定值相吻合,相对标准偏差小于1.3%,与化学法相比,硅和磷的测定时间由15 min缩短到2 min.","authors":[{"authorName":"甄洪香","id":"0f6c07e3-5413-4c35-908d-1d09d255379f","originalAuthorName":"甄洪香"},{"authorName":"徐增芹","id":"1456aa41-7722-47e2-99a5-2afdf23edc89","originalAuthorName":"徐增芹"},{"authorName":"葛镧","id":"e7d9a9ba-a105-44cb-aa45-df4b0c8ea95d","originalAuthorName":"葛镧"}],"doi":"10.3969/j.issn.1000-7571.2005.04.011","fpage":"41","id":"2f4e6c15-5dca-489f-a0d9-3fc58dc2efa7","issue":"4","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"b1a18da4-5b5a-45fd-8cf2-99295ed8731b","keyword":"偏振式能量色散型<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱仪","originalKeyword":"偏振式能量色散型X-射线荧光光谱仪"},{"id":"cce21349-0b3c-4fe3-99e2-05267f011299","keyword":"生铁","originalKeyword":"生铁"},{"id":"4aa6f72c-c8bf-427e-8d60-c89d6c6cf50f","keyword":"次级靶","originalKeyword":"次级靶"}],"language":"zh","publisherId":"yjfx200504011","title":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定生铁中硅和磷","volume":"25","year":"2005"},{"abstractinfo":"本文介绍了用偏硼酸锂(33%)和四硼酸锂(67%)混合助熔剂熔融制样,加补钴粉做内标,采用<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法定量测定铁矿石中的TFe,SiO2,CaO,MgO,Al2O3,P,S含量,经大量实践数据证明,完全符合误差要求,精密度高,准确度可靠,不仅大大缩短了分析时间,提高了工作效率,而且降低了劳动强度.","authors":[{"authorName":"肖文忠","id":"44b3697c-bac8-4200-ad0a-8c50efb5c982","originalAuthorName":"肖文忠"},{"authorName":"苏峥","id":"b225c29a-fdc0-4432-b385-908e99057a69","originalAuthorName":"苏峥"},{"authorName":"马建平","id":"65632b58-3d32-4704-811e-6ce4451f92c8","originalAuthorName":"马建平"},{"authorName":"刘尚英","id":"84734798-bbe7-42f9-a8b3-de972be17bab","originalAuthorName":"刘尚英"}],"doi":"10.3969/j.issn.1000-7571.2004.z1.068","fpage":"232","id":"8bd7e412-cbf5-4cf8-aac3-e32ec58731d8","issue":"z1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"38b2f6b5-4f8c-4742-bb8b-3ed95421e837","keyword":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱","originalKeyword":"X-射线荧光光谱"},{"id":"177e23a0-d075-46ed-8b6c-fa61f91df231","keyword":"铁矿石","originalKeyword":"铁矿石"},{"id":"caa4faef-f47a-4ce2-a563-c6481e289963","keyword":"熔融法","originalKeyword":"熔融法"}],"language":"zh","publisherId":"yjfx2004z1068","title":"利用<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱仪分析铁矿石中若干元素","volume":"24","year":"2004"},{"abstractinfo":"采用硅石标准样品及其复配标准样品作为校准样品,建立了熔融制样<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定硅石中SiO2,Fe2O3,Al2O3,CaO,MgO,K2O,TiO2,MnO,P2O5主次成分的方法.采用熔融法为试料片和校准片的制备方法,通过试验选择四硼酸锂-偏硼酸锂混合熔荆(12:22,m/m)为助熔剂、1.00 mLz LiBr溶液为脱模剂、稀释比为1:20、熔融时间30 min.采用可变理论α系数对基体效应进行校正.对同一硅石样品进行测定的相对标准偏差(RSD)小于8%,对不同硅石样品进行测定,本法的测定结果与标准方法的测定结果相吻合,偏差在允许范围内,t检验合格.","authors":[{"authorName":"蒋晓光","id":"f7a95486-d473-4430-8225-4c708557a43d","originalAuthorName":"蒋晓光"},{"authorName":"林忠","id":"ce5602b6-db63-4be3-b30d-25c048835ba5","originalAuthorName":"林忠"},{"authorName":"李卫刚","id":"fc5bef97-4b01-40e9-92aa-e892155d248d","originalAuthorName":"李卫刚"}],"doi":"10.3969/j.issn.1000-7571.2008.10.008","fpage":"31","id":"fe182907-9ae6-4424-a410-cecd9cab202c","issue":"10","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"7c3f1cc3-d2fa-4ffb-9ef7-c4ebbbb7da96","keyword":"硅石","originalKeyword":"硅石"},{"id":"5bae5d23-4352-4614-9c51-37ee83c01747","keyword":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法","originalKeyword":"X-射线荧光光谱法"},{"id":"6fe6f7d0-fa3e-4018-8e66-f95ebc535a2a","keyword":"主次成分","originalKeyword":"主次成分"},{"id":"090af213-c0a9-4a8f-9c0d-8a9e64868c04","keyword":"熔融制样","originalKeyword":"熔融制样"}],"language":"zh","publisherId":"yjfx200810008","title":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定硅石中主次成分","volume":"28","year":"2008"},{"abstractinfo":"将凹精研磨至过120目,与混合熔剂混匀,熔融成片,用Philips PW1606<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱仪测定其中铝、钒、钛.结果准确,稳定,满足生产测定要求.","authors":[{"authorName":"邢华宝","id":"d4dc7c6a-5e79-4eef-8440-b05343c8389e","originalAuthorName":"邢华宝"},{"authorName":"胡正阳","id":"00045362-03de-4c82-b3f2-5ddb7304b004","originalAuthorName":"胡正阳"},{"authorName":"史厚义","id":"aec80c2a-e965-4d23-bb03-1fb0c25a35bd","originalAuthorName":"史厚义"},{"authorName":"孙雪松","id":"00fa7949-6d46-4890-88aa-ad5ccc7f0493","originalAuthorName":"孙雪松"}],"doi":"10.3969/j.issn.1000-7571.2004.z1.056","fpage":"198","id":"aca29c4c-eac0-4800-bd1c-dd82b0ab99cc","issue":"z1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"ab944b90-665a-476d-97d2-b246ce41f1a6","keyword":"凹精","originalKeyword":"凹精"},{"id":"bbdf3ad6-39da-40a0-abf3-ac2b457bb42e","keyword":"熔融","originalKeyword":"熔融"},{"id":"29abb581-9c61-42a3-b832-a0e145e48604","keyword":"<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱","originalKeyword":"X射线荧光光谱"}],"language":"zh","publisherId":"yjfx2004z1056","title":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱熔融法测定凹精中铝钒钛","volume":"24","year":"2004"},{"abstractinfo":"使用<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱仪,国产电熔融炉熔片法,消除固体样品的基体晶相效应,建立了铁矿石中主元素铁及其他元素含量的测定方法.研究了熔样方法、光谱条件.测定范围Fe2O3的质量分数为40%～70%,绝对误差小于+0.3%,所测试样结果与化学值对比,符合性很好.","authors":[{"authorName":"刘启新","id":"36e4283a-4bb6-4dc1-a1b7-8a0c0f4e1b69","originalAuthorName":"刘启新"},{"authorName":"陈会兴","id":"b269d60e-d36d-464b-99ac-3eefdcade6de","originalAuthorName":"陈会兴"}],"doi":"10.3969/j.issn.1000-7571.2004.z1.057","fpage":"200","id":"8511efb3-6dcb-42f8-bd8a-4fdce3e75981","issue":"z1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"856b1469-db90-4762-826e-d15effd1af54","keyword":"铁","originalKeyword":"铁"},{"id":"b8517f0a-6556-4846-b79e-aad4b81fa31c","keyword":"铁矿石","originalKeyword":"铁矿石"},{"id":"003cd2b0-3d50-4696-b7b1-48fbd43f1c21","keyword":"<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法","originalKeyword":"X射线荧光光谱法"}],"language":"zh","publisherId":"yjfx2004z1057","title":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定铁矿中铁含量的研究","volume":"24","year":"2004"},{"abstractinfo":"利用<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱仪测定转炉渣中的TFe,SiO2,CaO,MgO,MnO,P2O5,Al2O3等主要化学成分的含量,采用自制标样绘制工作曲线,利用光谱干扰校正系数和基体效应校正系数消除光谱干扰和基体效应.实验表明:该方法简便快速,有良好的精密度和准确度,所得结果与湿法化学分析结果一致.","authors":[{"authorName":"宋兆华","id":"1044b580-9964-49dd-afbf-faae5a93e08e","originalAuthorName":"宋兆华"},{"authorName":"武映梅","id":"a813e198-e374-4474-8cb9-426b0cd69b90","originalAuthorName":"武映梅"},{"authorName":"谢桂龙","id":"1bcd8705-7fdc-4fca-84a5-e1ab1fa096ea","originalAuthorName":"谢桂龙"}],"doi":"10.3969/j.issn.1000-7571.2004.z1.054","fpage":"190","id":"d76b5d89-a4b8-478a-a042-d4feeaf79d99","issue":"z1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"91f41770-6cd6-4b14-9440-99f3d223e1e7","keyword":"<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱","originalKeyword":"X射线荧光光谱"},{"id":"0e3b6723-450f-4134-9da5-1b0aab76191f","keyword":"光谱干扰","originalKeyword":"光谱干扰"},{"id":"0810fc68-1035-4212-9be9-7c5de1228c46","keyword":"基体效应","originalKeyword":"基体效应"},{"id":"44cf997f-208b-47e6-a2f7-e2e21b5dcd9b","keyword":"渣","originalKeyword":"渣"}],"language":"zh","publisherId":"yjfx2004z1054","title":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定转炉渣主要成分","volume":"24","year":"2004"},{"abstractinfo":"介绍了用<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定高炉渣中的Al2O3,试样采用粉末压片制成.该方法简便、快速、准确、可靠.","authors":[{"authorName":"宋兆华","id":"ec4800b4-59da-4a90-9981-1602628aa179","originalAuthorName":"宋兆华"},{"authorName":"武映梅","id":"7f2f75f8-b09a-4596-8bf9-6323eabaeb28","originalAuthorName":"武映梅"}],"doi":"10.3969/j.issn.1000-7571.2004.z1.059","fpage":"208","id":"65ffff00-478f-49c7-9555-b70871fcc59b","issue":"z1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"703af166-fee8-4cdc-a0e1-0fd6e8f696c7","keyword":"<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法","originalKeyword":"X射线荧光光谱法"},{"id":"638b70cb-1149-4778-994b-98139c92edad","keyword":"粉末压片","originalKeyword":"粉末压片"},{"id":"529a497e-8cc9-4f1f-a04a-09f8878bdb48","keyword":"渣","originalKeyword":"渣"},{"id":"af091843-21fe-4f1a-b1b8-e3a1b3cae7d5","keyword":"Al2O3","originalKeyword":"Al2O3"}],"language":"zh","publisherId":"yjfx2004z1059","title":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定高炉渣中的Al2O3","volume":"24","year":"2004"},{"abstractinfo":"用<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱仪,测定中,低合金钢中Si,Mn,P,S,Cr,Ni,Cu,V,Ti,Mo,As等12个化学元素.给出了各元素的干扰校正系数和基体效应校正系数.方法准确,灵敏,稳定性好,速度快.","authors":[{"authorName":"武映梅","id":"34e5d5a2-a6d5-4e29-8b32-7809d0df763a","originalAuthorName":"武映梅"},{"authorName":"宋兆华","id":"6a0858ec-2711-4edc-a1cd-7adc16aab16f","originalAuthorName":"宋兆华"},{"authorName":"邢文青","id":"32299e6f-12cd-4ce6-925e-83104db47413","originalAuthorName":"邢文青"}],"doi":"10.3969/j.issn.1000-7571.2004.z1.058","fpage":"203","id":"0af226ce-c5d7-4eba-9d2b-2767f231a3a8","issue":"z1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"7f387a06-1048-4633-9226-3e1f2c912b6d","keyword":"<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱","originalKeyword":"X射线荧光光谱"},{"id":"fe3763c9-97a8-4286-8ec4-d3757dd98041","keyword":"中、低合金钢","originalKeyword":"中、低合金钢"},{"id":"eccb9400-6527-4406-954a-adba961a34ed","keyword":"元素分析","originalKeyword":"元素分析"}],"language":"zh","publisherId":"yjfx2004z1058","title":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱法测定中、低合金钢中的12个元素","volume":"24","year":"2004"},{"abstractinfo":"建立了熔融制备的玻璃样片,用<span style=\"color:red\">X</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱分析(XRF)天然高岭土组分以及利用仪器所配(<span style=\"color:red\">X</span>40)软件包汇编程序,在程序中专门设定外加通道,反复输入烧失的近似数据,多次测量试样,直接测定烧失量的方法.解决了由于天然高岭土样品细散压片制备样品而引起的颗粒度效应和烧失量严重而影响测量归一化的问题.省略了预先做样品灼烧、恒重和称量等繁琐的操作,实现了天然高岭土组分的XRF光谱快速、准确和自动化程度高的分析.","authors":[{"authorName":"张志峰","id":"bfbe174a-dfe9-4bba-8ad2-55c84c679b85","originalAuthorName":"张志峰"},{"authorName":"刘子瑜","id":"e5a3f15e-6a3c-4feb-b7df-759d6a65fc3f","originalAuthorName":"刘子瑜"},{"authorName":"牛素琴","id":"82fc5ccc-fbe9-4af6-992c-25c3a8aa09e6","originalAuthorName":"牛素琴"},{"authorName":"王蓍茜","id":"6f49254e-18e8-4898-be9e-7b2e8f551f11","originalAuthorName":"王蓍茜"},{"authorName":"温铁丽","id":"6a36617e-1325-4b95-9796-368f79b1479b","originalAuthorName":"温铁丽"}],"doi":"10.3969/j.issn.1004-244X.2007.04.018","fpage":"64","id":"50837e34-1cde-4fd5-932d-8a9f0a22edf8","issue":"4","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程   "},"keywords":[{"id":"8193c370-20ef-43d8-9a88-a86a91c9dcf6","keyword":"<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>谱","originalKeyword":"X-射线荧光谱"},{"id":"820fd2f6-f006-45d2-8e5d-3b7449e9b7e2","keyword":"颗粒度效应","originalKeyword":"颗粒度效应"},{"id":"c6736478-5624-4109-b309-9daa2be343d8","keyword":"弥散型天然高岭土","originalKeyword":"弥散型天然高岭土"},{"id":"28799d17-4591-4583-980e-b1724744ae3e","keyword":"烧失量","originalKeyword":"烧失量"},{"id":"8cad6005-99f3-4852-a1b8-b6ff70444082","keyword":"外加通道","originalKeyword":"外加通道"}],"language":"zh","publisherId":"bqclkxygc200704018","title":"烧失量严重(15%～25%)弥散型天然高岭土的<span style=\"color:red\">X-</span><span style=\"color:red\">射线</span><span style=\"color:red\">荧光</span>光谱分析","volume":"30","year":"2007"}],"totalpage":3152,"totalrecord":31515}