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PREPARATION OF SILICA MOLECULAR SIEVE MEMBRANE FOR HYDROGEN SEPARATION

B.Q. Jiang , L. Gu , W.L. Zhang , Y.S. Sun and F. Lin Chemical Engineering Department of Nanchang University , Nanchang 330029 , China

金属学报(英文版)

A ceramic tube supported γ alumina silica inorganic composite membrane was made by modifying a ceramic tube supported γ alumina film with a silica sol using sol gel method. The thickness of the silica thin film was 750? and the pore diameter was less than 5?.The prepared silica molecular sieve membrane displayed a high hydrogen permeability and high selectivities of H 2/N 2 and H 2/CO 2 gas mixtures. This composite membrane can be used to separate high purity hydrogen of more than 99 5% from various kinds of industrial waste gas mixtures containing hydrogen.

关键词: silica , null , null , null

STUDY ON PREPARATION OF TUBULAR CERAMIC MICRO FILTRATION MEMBRANE

B.Q. Jiang , W.L. Zhang , Y.S. Sun , F. Lin and L. Gu Chemical Engineering Dpartment of Nanchang University , Nanchang 330029 , China

金属学报(英文版)

A tubular micro filtration membrane was prepared with α alumina powder and ceramic tube support using dip coating method. The prepared membrane was characterized by SEM, mercury porosimetry and permeability measurement. The effects of the suspension properties and the preparation conditions on the structure and the membrane properties were discussed. The membrane was made with a top layer thickness of 50 μm , an average pore diameter of 0 45 μm , a porosity of 42% and a water flux of 6 5×10 -2 l/(m 2 h Pa). The membrane has a narrow pore distribution and good strength without crack forming, which can be used in industrial micro filtration process.

关键词: ceramic membrane , null , null , null

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