{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以十六烷基三甲基溴化铵(CTAB)为模板剂,采用水热法制备了介孔TiO_2,对制得的样品进行了XRD、TEM、N2吸附-解吸表征,并探究了不同吸附条件对样品吸附性能的影响.结果表明,所得样品为窄孔道分布,其比表面积为161.2m~2/g,最可几孔径为5.2nm;与非介孔TiO_2相比,介孔TiO_2对氟离子的吸附性能明显优越,其对氟离子的吸附速率符合Bangham吸附速率方程,吸附量随氟离子浓度的增大而增大,而且吸附符合Langmuir等温吸附方程,属于放热吸附.","authors":[{"authorName":"<span style=\"color:red\">周</span><span style=\"color:red\">新</span><span style=\"color:red\">革</span>","id":"af48fb97-83f3-4085-a072-4abb5be6e940","originalAuthorName":"周新革"},{"authorName":"赵斯琴","id":"e43c9415-a671-49b3-af38-1a38fa4abb2f","originalAuthorName":"赵斯琴"},{"authorName":"长山","id":"961c8a19-033f-4b95-a478-a0fe923485b7","originalAuthorName":"长山"}],"doi":"","fpage":"476","id":"6057759e-5dbb-43a4-a069-9e08221ebbed","issue":"3","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"a019b63a-5faa-4216-ab47-fcf803a414d5","keyword":"水热法","originalKeyword":"水热法"},{"id":"488e978a-2c7a-4e4a-8ff5-b0f2ed61bb7e","keyword":"介孔TiO_2","originalKeyword":"介孔TiO_2"},{"id":"6eaca67a-d59e-4e5c-9a5b-3860a38a0b43","keyword":"氟离子","originalKeyword":"氟离子"},{"id":"c60e7052-a051-4a4c-9231-d8496f2655b7","keyword":"吸附","originalKeyword":"吸附"}],"language":"zh","publisherId":"gncl201003032","title":"介孔TiO_2的合成及其对氟离子的吸附性能研究","volume":"41","year":"2010"},{"abstractinfo":"通过316L钢在420℃环境下应力控制的低<span style=\"color:red\">周</span>疲劳实验, 基于连续损伤力学,\n提出一种<span style=\"color:red\">新</span>的低<span style=\"color:red\">周</span>疲劳损伤模型, 采用间接反映循环塑性应变能的应力--位移\n曲线面积的变化作为损伤变量, 实验结果与该模型显示的疲劳损伤演变规律符\n合较好.","authors":[{"authorName":"陈凌","id":"8e04eedc-ebba-4190-813a-8c292b03991e","originalAuthorName":"陈凌"},{"authorName":"蒋家羚","id":"48c4cffa-e84d-4a09-ac33-a76c8dae9b54","originalAuthorName":"蒋家羚"}],"categoryName":"|","doi":"","fpage":"157","id":"2546ed29-646a-4806-989b-3e0b04aa1d2a","issue":"2","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"da88a416-1cac-4d95-bd49-4aacd0c7d330","keyword":"低<span style=\"color:red\">周</span>疲劳","originalKeyword":"低周疲劳"},{"id":"9ea619c5-e668-4d09-8ab1-42a0b36f1d44","keyword":"null","originalKeyword":"null"},{"id":"86940e2f-d95e-4d16-8f23-a65aeb331a33","keyword":"null","originalKeyword":"null"}],"language":"zh","publisherId":"0412-1961_2005_2_11","title":"一种<span style=\"color:red\">新</span>的低<span style=\"color:red\">周</span>疲劳损伤模型及实验验证","volume":"41","year":"2005"},{"abstractinfo":"通过316L钢在420℃环境下应力控制的低<span style=\"color:red\">周</span>疲劳实验,基于连续损伤力学,提出一种<span style=\"color:red\">新</span>的低<span style=\"color:red\">周</span>疲劳损伤模型,采用间接反映循环塑性应变能的应力-位移曲线面积的变化作为损伤变量,实验结果与该模型显示的疲劳损伤演变规律符合较好.","authors":[{"authorName":"陈凌","id":"184993d7-8a94-43cd-b2db-d02681ff71fe","originalAuthorName":"陈凌"},{"authorName":"蒋家羚","id":"c02ab1a4-997c-4595-91ad-1b8abd2b6285","originalAuthorName":"蒋家羚"}],"doi":"10.3321/j.issn:0412-1961.2005.02.009","fpage":"157","id":"9cdaaf16-bbae-4aa9-9c31-1b0c6e4cdd8f","issue":"2","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"0a1bea72-6d08-4a8d-b652-dfebd3f90932","keyword":"低<span style=\"color:red\">周</span>疲劳","originalKeyword":"低周疲劳"},{"id":"1a276644-d3ff-429d-8744-b74246b71c30","keyword":"连续损伤力学","originalKeyword":"连续损伤力学"},{"id":"181867de-af83-4675-afb5-1c315994441e","keyword":"塑性应变能","originalKeyword":"塑性应变能"},{"id":"969ab198-750f-4bd5-8bee-2033a627c681","keyword":"应力-位移曲线","originalKeyword":"应力-位移曲线"},{"id":"759a497c-cc9a-40a7-aef9-08ee77c16eed","keyword":"损伤变量","originalKeyword":"损伤变量"}],"language":"zh","publisherId":"jsxb200502009","title":"一种<span style=\"color:red\">新</span>的低<span style=\"color:red\">周</span>疲劳损伤模型及实验验证","volume":"41","year":"2005"},{"abstractinfo":"生活中人们仅从外观上很难鉴别聚氨酯(PU)、聚氯乙烯(PVC)两种人造<span style=\"color:red\">革</span>.试验利用傅立叶红外光谱(ATR)法对送检的两件手提包人造<span style=\"color:red\">革</span>样品的材质进行快速鉴别.结果表明,傅立叶红外光谱(ATR)分析技术作为人造<span style=\"color:red\">革</span>有机结构分析的一个重要工具,具有快速、简便、样品用量少、结果准确可靠等优点.","authors":[{"authorName":"<span style=\"color:red\">周</span>洪涛","id":"3299fcd5-3735-4892-baff-708f7bcb772e","originalAuthorName":"周洪涛"},{"authorName":"李洪","id":"6d4e9acf-3fdc-4f11-b49c-93606a7ce9a6","originalAuthorName":"李洪"},{"authorName":"孙琳琳","id":"ef8b5ee3-36d0-495c-9af2-16f805d81bda","originalAuthorName":"孙琳琳"},{"authorName":"冷爱平","id":"0c775b64-44c7-4718-98cc-233d5f20b8cc","originalAuthorName":"冷爱平"},{"authorName":"孙献国","id":"be99732a-3c5a-4613-9510-8b2bc732c3b5","originalAuthorName":"孙献国"}],"doi":"","fpage":"45","id":"f445dcdf-a1d5-4a8c-acd7-748d7681ff6d","issue":"3","journal":{"abbrevTitle":"HCCLLHYYY","coverImgSrc":"journal/img/cover/HCCLLHYYY.jpg","id":"42","issnPpub":"1671-5381","publisherId":"HCCLLHYYY","title":"合成材料老化与应用"},"keywords":[{"id":"509ebe10-4c0e-4df0-9b13-9daeb298dbf8","keyword":"聚氨酯","originalKeyword":"聚氨酯"},{"id":"516b4b69-5827-4d7a-ac9f-36f2cf4e9659","keyword":"聚氯乙烯","originalKeyword":"聚氯乙烯"},{"id":"95a31e79-f36c-4809-90ed-f09d9d964cbf","keyword":"红外光谱","originalKeyword":"红外光谱"},{"id":"27b23470-68d0-4d54-8708-9413e2a3a11c","keyword":"ATR","originalKeyword":"ATR"},{"id":"b4559a7a-f39c-41b4-b0b8-f3725089f9c4","keyword":"波数","originalKeyword":"波数"}],"language":"zh","publisherId":"hccllhyyy201603011","title":"傅立叶红外光谱(ATR)法鉴别聚氨酯和聚氯乙烯<span style=\"color:red\">革</span>","volume":"45","year":"2016"},{"abstractinfo":"本文简要地介绍合成蜡剂在绵羊皮薄型服装<span style=\"color:red\">革</span>涂饰后水洗处理过程中的实际应用,以及有关问题探讨.","authors":[{"authorName":"蒋元源","id":"f259fcff-ea90-4d7e-ad49-67c9732fec78","originalAuthorName":"蒋元源"},{"authorName":"孙华","id":"baecb8db-abd4-4101-9a18-91fa0a039ff2","originalAuthorName":"孙华"}],"doi":"10.3969/j.issn.1671-5381.2011.03.011","fpage":"48","id":"9174060c-45cc-49f4-933d-5ff94c9412a5","issue":"3","journal":{"abbrevTitle":"HCCLLHYYY","coverImgSrc":"journal/img/cover/HCCLLHYYY.jpg","id":"42","issnPpub":"1671-5381","publisherId":"HCCLLHYYY","title":"合成材料老化与应用"},"keywords":[{"id":"4254568f-d0d1-4cc4-80c9-c788153e094f","keyword":"绵羊皮","originalKeyword":"绵羊皮"},{"id":"e77ab194-87f9-456e-8e6e-72b7a64f823e","keyword":"涂饰","originalKeyword":"涂饰"},{"id":"14a4e393-ccbe-45b3-971f-4db7c3a03f27","keyword":"蜡剂","originalKeyword":"蜡剂"},{"id":"ae46c5fd-8287-4761-a760-6586805ac743","keyword":"水洗","originalKeyword":"水洗"}],"language":"zh","publisherId":"hccllhyyy201103011","title":"合成蜡剂在羊皮水洗服装<span style=\"color:red\">革</span>中的应用","volume":"40","year":"2011"},{"abstractinfo":"微晶纤维素（MCC）可作为PU合成<span style=\"color:red\">革</span>湿法生产中优良的微孔剂和增稠剂使用,并能赋予合成<span style=\"color:red\">革</span>良好的手感和弹性,但国内外生产合成<span style=\"color:red\">革</span>用MCC多以棉浆粕和木浆粕为原料,资源少,成本高。以漂白麦草浆为原料,通过化学处理、生物酶处理和机械处理等工艺过程制备出了麦草MCC。重点探讨了酸处理工艺条件与产品性能的关系,并优化确定了最佳酸处理工艺。并利用SEM、XRD、TGA等手段分别对麦草MCC的微观形貌、结晶结构和热稳定性等性能进行了表征。研究结果表明,麦草MCC性能指标达到《合成<span style=\"color:red\">革</span>用微晶纤维素》行业标准要求,可以替代目前棉浆粕和木浆粕为原料生产的PU合成<span style=\"color:red\">革</span>用MCC产品。","authors":[{"authorName":"李金宝","id":"27b9795c-c032-4898-b268-f611292c5585","originalAuthorName":"李金宝"},{"authorName":"张美云","id":"6c5ac974-1121-41e3-a0bc-aa08fbd0b6f8","originalAuthorName":"张美云"},{"authorName":"刘银山","id":"21b28778-3771-44c0-95a0-6ec324224666","originalAuthorName":"刘银山"},{"authorName":"张云","id":"b32e0589-d18b-4f55-8041-ab8454817d88","originalAuthorName":"张云"}],"doi":"","fpage":"1606","id":"e39952c4-36d9-4f45-94ed-996d7749766d","issue":"9","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"3aeaba4a-eea7-4d20-9436-446f535a52f1","keyword":"微晶纤维素","originalKeyword":"微晶纤维素"},{"id":"a18308e6-d258-432f-825e-ea6fe0fe6d2f","keyword":"麦草浆","originalKeyword":"麦草浆"},{"id":"0352261d-21b4-48a8-97f5-b88b81cdb6fb","keyword":"PU合成<span style=\"color:red\">革</span>","originalKeyword":"PU合成革"}],"language":"zh","publisherId":"gncl201109017","title":"合成<span style=\"color:red\">革</span>用麦草微晶纤维素的制备及其表征","volume":"42","year":"2011"},{"abstractinfo":"将改性纳米TiO2添加到聚氨酯预聚体中,制备出具有良好稳定性的改性纳米TiO2/水性聚氨酯(WPU)复合材料;以其作为成膜剂,采用干法移膜法制备超细纤维合成<span style=\"color:red\">革</span>.通过对超细纤维合成<span style=\"color:red\">革</span>卫生性能、耐用性能等指标的测定,考察了复合材料的应用性能.结果表明:加入改性纳米TiO2可提高WPU的抗静电性且对涂层表面平整度无影响,当添加量为3％(质量分数)时,超细纤维合成<span style=\"color:red\">革</span>的透气性提高了40％,透水汽性提高了64％,其耐磨、耐折性也得到明显改善.","authors":[{"authorName":"罗晓民","id":"6177e90e-a06d-426d-809a-b9b9702fc99d","originalAuthorName":"罗晓民"},{"authorName":"刘蕊","id":"8d6b78b1-52f0-4a40-8648-e5003275cdfd","originalAuthorName":"刘蕊"},{"authorName":"冯见艳","id":"fdfc6a91-6b11-45de-a749-a019b99deb37","originalAuthorName":"冯见艳"},{"authorName":"杨菲菲","id":"8217a4fe-771c-4f4b-bec3-c221ce0cf902","originalAuthorName":"杨菲菲"},{"authorName":"张鹏","id":"ed3d85e1-4e1e-4f93-9674-fcb9d5d27226","originalAuthorName":"张鹏"}],"doi":"","fpage":"65","id":"a6d7ac77-c937-4ec2-b511-24ec918eac5e","issue":"6","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"e59b28a8-d54a-48e8-a217-751fc7e7eb8c","keyword":"纳米TiO2","originalKeyword":"纳米TiO2"},{"id":"6bdb735e-2cac-4b0a-908f-cf87c71070ab","keyword":"水性聚氨酯","originalKeyword":"水性聚氨酯"},{"id":"4788816e-3a53-45b5-9e2f-1150c7e69490","keyword":"超细纤维合成<span style=\"color:red\">革</span>","originalKeyword":"超细纤维合成革"}],"language":"zh","publisherId":"cldb201406017","title":"改性纳米TiO2/WPU复合材料在超细纤维合成<span style=\"color:red\">革</span>上的应用","volume":"28","year":"2014"},{"abstractinfo":"针对传统聚氨酯色浆中色基与聚氨酯结合力弱(分子间力),导致成品<span style=\"color:red\">革</span>色牢度差、色迁移严重等技术难题,本文设计合成了一种反应型彩色二元醇:在四氢呋喃介质中,控制n(对苯二胺)∶n(乙酸酐)=1.00∶0.95, 0~5 ℃下,用乙酸酐将对苯二胺单酰化反应15 h,得到对氨基乙酰苯胺(产率85%),经重氮化,与过量摩尔分数为5% N-苯基二乙醇胺偶合制得了一种含两个端羟甲基的偶氮化合物4-乙酰基胺基-4'-N,N-二羟乙氨基偶氮苯(产率82%);将其与聚酯二元醇?聚醚二元醇以不同比例混合,与双异氰酸酯预聚?扩链后形成红色聚氨酯树脂色浆,在离型纸上铺展成膜,其断裂增长率443畅0%,断裂相对强度125畅5 g,色迁移量21畅4 μg,进口同类产品形成膜后的断裂增长率?断裂相对强度与色迁移量分别为442畅2%?125畅3 g 和29畅2 μg.合成产品优于同类进口产品?","authors":[{"authorName":"尹志刚","id":"cd88d471-0829-4189-9de3-aae4ea781ff8","originalAuthorName":"尹志刚"},{"authorName":"刘珍珍","id":"8f90c1ee-314f-4feb-98ba-5627b79f9681","originalAuthorName":"刘珍珍"},{"authorName":"钱恒玉","id":"9ee9f3e1-1f23-4446-83f4-9b631ad17f32","originalAuthorName":"钱恒玉"},{"authorName":"WANG Zaifeng","id":"c1f6b1ef-2523-4bfe-9ab4-ef47f52f965c","originalAuthorName":"WANG Zaifeng"},{"authorName":"赵喜乐","id":"3a805d0a-117b-475e-a470-a49b242f6cd6","originalAuthorName":"赵喜乐"},{"authorName":"彭丽芳","id":"71d855cd-3be9-413f-932b-0eee75a9c366","originalAuthorName":"彭丽芳"},{"authorName":"袁奇","id":"57794fb8-44b1-484c-91c5-22c443de108e","originalAuthorName":"袁奇"}],"doi":"10.11944/j.issn.1000-0518.2017.06.160394","fpage":"649","id":"89050428-0d99-40b9-acef-9b626cc8fb2c","issue":"6","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"19521e97-7afc-4ec3-ad86-0f6587c1df1a","keyword":"对苯二胺","originalKeyword":"对苯二胺"},{"id":"15679abd-941e-4ae3-ad56-5fb9822d4118","keyword":"乙酰化","originalKeyword":"乙酰化"},{"id":"d80c5c8a-8048-4cd0-96ba-497ba774672e","keyword":"重氮化偶合反应","originalKeyword":"重氮化偶合反应"},{"id":"fdea5c98-6337-4fbf-b1d2-a74a96193ac9","keyword":"偶氮化合物","originalKeyword":"偶氮化合物"},{"id":"c5ae501e-2bea-48ca-9d5e-21bb8ea82b8a","keyword":"红色聚氨酯","originalKeyword":"红色聚氨酯"},{"id":"3a8255a3-4628-4a20-acc1-c860c8bcb4e8","keyword":"色迁移","originalKeyword":"色迁移"}],"language":"zh","publisherId":"yyhx201706006","title":"一种反应型染料的合成及其在聚氨酯<span style=\"color:red\">革</span>染色中的应用","volume":"34","year":"2017"},{"abstractinfo":"建立了超高效液相色谱-静电场轨道阱高分辨质谱(UPLC-Orbitrap HRMS)同时测定合成<span style=\"color:red\">革</span>中8种异氰酸酯残留的方法.样品中残留的异氰酸酯经二氯甲烷超声萃取后,用9-甲氨基甲基蒽(MAMA)进行衍生,衍生产物浓缩定容后进行UPLC-Orbitrap HRMS分析,外标法定量.衍生产物在Hypersil GOLD色谱柱(100 mm×2.1 mm,1.9 μm)上进行分离,流动相为乙腈-0.1％ (v/v)甲酸水溶液,采用电喷雾正离子(ESI+)模式电离,以保留时间和准分子离子精确质量数定性,以提取离子色谱峰面积定量.各组分的定量限均为0.2 μg/kg,在3个加标浓度水平下,方法的平均加标回收率为85.41％ ～95.53％,相对标准偏差(RSD)为2.55％ ～ 6.87％.应用该方法对市售合成<span style=\"color:red\">革</span>产品进行监测,结果在1个样品中检出了异佛尔酮二异氰酸酯.该方法定性准确,定量限低,灵敏度高,可用于合成<span style=\"color:red\">革</span>中异氰酸酯残留的测定.","authors":[{"authorName":"王成云","id":"2a263370-2bee-451d-b555-1e75df8d3eb7","originalAuthorName":"王成云"},{"authorName":"李丽霞","id":"4289170f-fb89-4912-be79-370bec38cf3e","originalAuthorName":"李丽霞"},{"authorName":"林君峰","id":"ba535c42-8f4a-4463-8183-349c2904e113","originalAuthorName":"林君峰"},{"authorName":"诸乃清","id":"0343addf-fb8d-4146-9b2f-98693ce0d4a7","originalAuthorName":"诸乃清"},{"authorName":"谢堂堂","id":"361abe52-2f53-4b5f-85f1-f33382f3ab95","originalAuthorName":"谢堂堂"}],"doi":"10.3724/SP.J.1123.2016.04037","fpage":"888","id":"52885107-53f5-405a-af72-2a578e76e2e2","issue":"9","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"d20f9e7a-0fdd-4c2c-afa2-e3d0d6d44c19","keyword":"超高效液相色谱","originalKeyword":"超高效液相色谱"},{"id":"dfd6d7e2-492a-4504-96ce-9ab52dcaa43d","keyword":"静电场轨道阱高分辨质谱","originalKeyword":"静电场轨道阱高分辨质谱"},{"id":"4cf17c89-766a-44b2-8759-4716f4627b70","keyword":"异氰酸酯","originalKeyword":"异氰酸酯"},{"id":"44b301eb-b0db-4504-a458-a8612cacdede","keyword":"合成<span style=\"color:red\">革</span>","originalKeyword":"合成革"}],"language":"zh","publisherId":"sp201609008","title":"超高效液相色谱-静电场轨道阱高分辨质谱法同时测定合成<span style=\"color:red\">革</span>中8种异氰酸酯残留","volume":"34","year":"2016"},{"abstractinfo":"从熵守恒定律和能量守恒定律出发, 推导出一个<span style=\"color:red\">新</span>的低<span style=\"color:red\">周</span>疲劳寿命预测能量模型,并以该模型为基础, 对线性累积损伤法则进行了探讨. 通过316L钢420℃环境下应力控制的低<span style=\"color:red\">周</span>疲劳实验, 用该模型及基于该模型的线性累积损伤法则进行了低<span style=\"color:red\">周</span>疲劳寿命和剩余寿命的预测, 预测结果与实测结果符合较好.","authors":[{"authorName":"陈凌","id":"695f86f0-91a6-4ba5-93d5-e371ea8660d3","originalAuthorName":"陈凌"},{"authorName":"蒋家羚","id":"eb22a3a5-22c2-4b58-9e8d-3b14bdbb5667","originalAuthorName":"蒋家羚"},{"authorName":"范志超","id":"010233d7-3bf7-4247-93ec-d829ba5780c6","originalAuthorName":"范志超"},{"authorName":"陈学东","id":"5a317cb0-30e5-4085-9daf-79fe85bd317f","originalAuthorName":"陈学东"},{"authorName":"杨铁成","id":"70bbb9b8-2e7a-4f77-af7e-3082fba36ca1","originalAuthorName":"杨铁成"}],"categoryName":"|","doi":"","fpage":"195","id":"401c4f27-f2e2-4eb0-a811-939232103b71","issue":"2","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"549c7c96-bf0a-41bc-ab3c-9f94f2a78987","keyword":"低<span style=\"color:red\">周</span>疲劳","originalKeyword":"低周疲劳"},{"id":"48765748-ffa9-47de-a6de-657fe389fdcc","keyword":"entropy conservation","originalKeyword":"entropy conservation"},{"id":"d21b5bfc-c665-41dd-b850-c4518877b842","keyword":"energy conservation","originalKeyword":"energy conservation"},{"id":"1c278480-4141-409b-bfe5-4a72bcc790ee","keyword":"strain energy","originalKeyword":"strain energy"}],"language":"zh","publisherId":"0412-1961_2006_2_22","title":"低<span style=\"color:red\">周</span>疲劳寿命预测的能量模型探讨","volume":"42","year":"2006"}],"totalpage":807,"totalrecord":8063}