{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"称取一定量的载<span style=\"color:red\">金</span>炭进行<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>配料,经过熔炼、灰吹得到金银合粒,使用硝酸分金得到<span style=\"color:red\">金</span>粒,再通过计算得到载<span style=\"color:red\">金</span>炭中银含量,从而建立了<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>重量法测定载<span style=\"color:red\">金</span>炭中银含量的方法.经过试验,确定了<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>配料中试样量、氧化铅加入量、灰吹温度等最佳试验条件.根据目前国内载<span style=\"color:red\">金</span>炭的生产水平,在载<span style=\"color:red\">金</span>炭国家标准物质加入一定量的共存元素,进行了银量测定的干扰试验,结果表明载<span style=\"color:red\">金</span>炭中共存元素(Cu、Fe、Pb、Cd、Zn、Bi、Cr、Ca、Mg、As)对银测定无影响.将方法用于3个载<span style=\"color:red\">金</span>炭国家标准物质中银的测定,测定值与认定值基本吻合,相对标准偏差(RSD,n=11)为0.82%~4.2%.","authors":[{"authorName":"夏珍珠","id":"ae2def66-61f8-4a33-8789-5dec712b132d","originalAuthorName":"夏珍珠"}],"doi":"10.13228/j.boyuan.issn1000-7571.010052","fpage":"54","id":"4b8246f5-46d3-4c21-add1-aec3ad1a51f6","issue":"2","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"47d546ce-8dc2-4590-a95d-577be2bda394","keyword":"载<span style=\"color:red\">金</span>炭","originalKeyword":"载金炭"},{"id":"d39a523e-9fce-4000-9dc3-679e231f7a0a","keyword":"银","originalKeyword":"银"},{"id":"4fe9ac55-04a7-4da9-9b38-d814d71ea793","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"}],"language":"zh","publisherId":"yjfx201702011","title":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>重量法测定载<span style=\"color:red\">金</span>炭中银","volume":"37","year":"2017"},{"abstractinfo":"研究了铅扣中铜对钯灰吹时的影响及铅扣中铜、氧化铅和硅酸度(K)三者间的关系.提出了对粗铜样品不经预先分离铜而直接进行<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>,连续测定样品中的金和钯量.方法准确,精密度高.","authors":[{"authorName":"林海山","id":"0b885736-1497-475f-9911-bc7cebb939ef","originalAuthorName":"林海山"}],"doi":"10.3969/j.issn.1000-7571.2002.01.020","fpage":"53","id":"2315ff49-3b90-40b7-a5b2-1a9030c429c8","issue":"1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"58627cbd-6788-497b-aba2-7e3baf6aafac","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"2935a686-14d6-421e-8658-d7872a47202e","keyword":"粗铜","originalKeyword":"粗铜"},{"id":"d0d0d571-57f9-46b7-a47d-00d06bf48c7b","keyword":"<span style=\"color:red\">试</span><span style=\"color:red\">金</span>配料","originalKeyword":"试金配料"},{"id":"013a59d4-5140-41e5-82cf-d77e31008e95","keyword":"<span style=\"color:red\">金</span>","originalKeyword":"金"},{"id":"54344541-ab47-4cbc-b6c7-e92e20441e37","keyword":"钯","originalKeyword":"钯"}],"language":"zh","publisherId":"yjfx200201020","title":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>法测定粗铜中金和钯","volume":"22","year":"2002"},{"abstractinfo":"采用加Au的方法解决<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>测Ag时灰吹合粒\"开花\"的问题,讨论了Au的加入量与Ag回收率的关系,此法测Ag快速和简便准确.","authors":[{"authorName":"管有祥","id":"4d86f294-dd88-450f-8db6-4f225df5fa6e","originalAuthorName":"管有祥"}],"doi":"10.3969/j.issn.1004-0676.1999.01.010","fpage":"42","id":"19d9b7c4-6131-476e-8f4c-1eceb3b36c33","issue":"1","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"a2f1d50d-e12e-428d-bf37-a7a693185f19","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"e4f5151b-d8a8-4c7e-a659-9458fa2c8ad9","keyword":"\"开花\"","originalKeyword":"\"开花\""},{"id":"3bd95d8c-f3e0-4194-96a4-0785bc68d6f3","keyword":"加Au","originalKeyword":"加Au"}],"language":"zh","publisherId":"gjs199901010","title":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>灰吹合粒\"开花\"的讨论","volume":"","year":"1999"},{"abstractinfo":"建立了样品焙烧处理—<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>重量法测定载<span style=\"color:red\">金</span>炭中的<span style=\"color:red\">金</span>量;经过了一系列条件实验,分别确定了称样量范围、焙烧温度、配料、熔样温度、分金时间、分金酸度及金银质量比例等最佳实验条件.在最佳实验条件下,该方法加入标准物质的回收率为99.85 ％～100.1％,与原子吸收光谱法对比,体现了更好的重复性和再现性.在载<span style=\"color:red\">金</span>炭交易中,该方法被推荐为仲裁分析方法.","authors":[{"authorName":"马丽军","id":"6768dfdb-3530-488a-9d93-1f0ab30c47fa","originalAuthorName":"马丽军"},{"authorName":"陈永红","id":"5ac59b89-d7d2-4dea-9c22-e5e9e2151d26","originalAuthorName":"陈永红"},{"authorName":"腾飞","id":"6d20e110-9155-40fb-9f55-e990679138be","originalAuthorName":"腾飞"},{"authorName":"芦新根","id":"1ce113b3-6ebb-4ed5-b1b0-d68573b7c776","originalAuthorName":"芦新根"}],"doi":"10.11792/hj20131118","fpage":"68","id":"031dab89-a481-4201-bcbf-680191560ad2","issue":"11","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"27a49c13-1b1f-40cb-8b6d-4d6a1cac9063","keyword":"载<span style=\"color:red\">金</span>炭","originalKeyword":"载金炭"},{"id":"fe57d337-dd21-4f75-b6f6-8d875f4cc7fc","keyword":"<span style=\"color:red\">金</span>","originalKeyword":"金"},{"id":"cd477d2b-4419-4c19-97b5-7ef553f579a0","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"13f56eb7-08cc-46f3-96e9-e3789e6a9687","keyword":"重量法","originalKeyword":"重量法"}],"language":"zh","publisherId":"huangj201311018","title":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>重量法测定载<span style=\"color:red\">金</span>炭中的<span style=\"color:red\">金</span>量","volume":"34","year":"2013"},{"abstractinfo":"针对高铁高硫砷<span style=\"color:red\">金</span>精矿<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>分析测定方法在配料上进行了研究探讨.在一硅酸度时,适当降低氧化铅的用量、加大碳酸钠和玻璃粉的用量,并根据硫、砷的含量进行配料,不仅节约试剂,防止坩埚腐蚀,而且测定方法简便、快速,分析结果重现性好.","authors":[{"authorName":"张广盛","id":"645ef7ec-9e38-435b-ab4e-bde5cc6f830a","originalAuthorName":"张广盛"}],"doi":"10.3969/j.issn.1001-1277.2009.05.015","fpage":"49","id":"0e7f42cc-9f4e-41fb-8c27-a905f9ae01cc","issue":"5","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"37b5175c-1340-468d-8eb0-89d73e3ada4b","keyword":"高铁高硫砷<span style=\"color:red\">金</span>精矿","originalKeyword":"高铁高硫砷金精矿"},{"id":"c132a779-42c4-4964-bceb-4e7e8b48f38f","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"d3f380e9-53ea-4742-9664-b3ed935f476e","keyword":"硅酸度","originalKeyword":"硅酸度"},{"id":"553019ab-3557-4487-ba02-78f62e964539","keyword":"配料","originalKeyword":"配料"}],"language":"zh","publisherId":"huangj200905015","title":"高铁高硫砷<span style=\"color:red\">金</span>精矿<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>法配料的探讨","volume":"30","year":"2009"},{"abstractinfo":"研究了样品经<span style=\"color:red\">试</span><span style=\"color:red\">金</span>炉熔炼、灰吹后,除去锡、铅和锑,用硝酸分金,重量法测<span style=\"color:red\">金</span>的方法.样品相对标准偏差0.369%,加标回收率大于99%,结果令人满意.","authors":[{"authorName":"管有祥","id":"03346d63-2270-4b89-a770-fe6b79d57ca3","originalAuthorName":"管有祥"},{"authorName":"甘建壮","id":"69aa2c63-1777-4e45-ab77-a2ca2290b309","originalAuthorName":"甘建壮"},{"authorName":"温结胜","id":"edd65609-b8a6-4e40-a33e-63db82756c3d","originalAuthorName":"温结胜"},{"authorName":"段颖","id":"94f6ddf2-1eb1-4a26-b56f-ff9a6cc47785","originalAuthorName":"段颖"}],"doi":"10.3969/j.issn.1000-7571.2004.z1.089","fpage":"303","id":"cd9586df-9286-4d82-b2f5-b93e41072fa8","issue":"z1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"5ffb83ba-fdac-4b1a-9768-f04038d43c85","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"04fd2c91-ddf6-4607-b8dc-a13c23535c98","keyword":"合金","originalKeyword":"合金"},{"id":"76eadfa2-900d-480a-8788-6dc578929d27","keyword":"锡铅<span style=\"color:red\">金</span>锑","originalKeyword":"锡铅金锑"}],"language":"zh","publisherId":"yjfx2004z1089","title":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>测定锡铅<span style=\"color:red\">金</span>锑合金中<span style=\"color:red\">金</span>含量","volume":"24","year":"2004"},{"abstractinfo":"研究了杂质元素对火<span style=\"color:red\">试</span><span style=\"color:red\">金</span>重量法测定粗<span style=\"color:red\">金</span>中<span style=\"color:red\">金</span>量的影响,并通过一系列实验分别确定了粗<span style=\"color:red\">金</span>中铜、铁、锌、镍、铂、钯、硒、碲、锑、铋、钛、钨12种杂质元素适用于该方法的上限量值,及杂质元素超上限量值时所采取的措施,保证了方法的适用性,对指导黄金冶炼企业准确测定粗<span style=\"color:red\">金</span>中<span style=\"color:red\">金</span>量具有重要的意义.","authors":[{"authorName":"马丽军","id":"1aea492a-f1cb-4f25-8870-494fbdfac084","originalAuthorName":"马丽军"},{"authorName":"李正旭","id":"bcdcac60-868f-43b0-8ff7-5fd18fdde2ed","originalAuthorName":"李正旭"},{"authorName":"钟英楠","id":"14b7df8e-fde7-400f-9b4c-11ba54563283","originalAuthorName":"钟英楠"},{"authorName":"阚春海","id":"69aab5c5-c343-4999-85bc-aa8f1fab723b","originalAuthorName":"阚春海"},{"authorName":"肖千鹏","id":"4124895c-f61b-457e-b3e1-a05be5a61792","originalAuthorName":"肖千鹏"},{"authorName":"赵可迪","id":"129b9416-e5e1-4289-b9ef-588bfdc3fb62","originalAuthorName":"赵可迪"}],"doi":"10.11792/hj20170419","fpage":"73","id":"46f9af80-ca46-483c-8fe4-9e040e33c937","issue":"4","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"479a91d0-1aef-4dcc-a898-ec7584f07b9c","keyword":"粗<span style=\"color:red\">金</span>","originalKeyword":"粗金"},{"id":"a0e8154d-ba09-4767-a2e9-43c4bda89609","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"83e6efb9-971b-4ca5-80bd-f897fba9014b","keyword":"重量法","originalKeyword":"重量法"},{"id":"5050a2e1-8206-4f61-b38a-326d6b9a783b","keyword":"杂质","originalKeyword":"杂质"},{"id":"938185a1-80ab-4ccd-8a9f-c89967d97758","keyword":"增量","originalKeyword":"增量"}],"language":"zh","publisherId":"huangj201704019","title":"杂质元素对火<span style=\"color:red\">试</span><span style=\"color:red\">金</span>重量法测定粗<span style=\"color:red\">金</span>中<span style=\"color:red\">金</span>量影响的探讨","volume":"38","year":"2017"},{"abstractinfo":"建立了用<span style=\"color:red\">金</span>作保护剂,铅<span style=\"color:red\">试</span><span style=\"color:red\">金</span>一步富集汽车尾气净化催化剂中铂钯铑的方法.研究了<span style=\"color:red\">金</span>保护剂的条件,对比了不同方法的富集效果.结果表明:加入20～ 40 mg<span style=\"color:red\">金</span>作保护剂,<span style=\"color:red\">试</span><span style=\"color:red\">金</span>配料硅酸度为1.0,进炉温度900℃,1130℃恒温10 min,熔炼时间50 ～ 60 min,灰吹温度910℃,可完全富集500μg铂钯铑.方法富集效果好,操作简便,适用于汽车尾气净化催化剂、熔炼渣以及日常样品中0.x～ xxxx g/t铂钯铑的分析.","authors":[{"authorName":"管有祥","id":"b0f7c617-4374-48e9-ac1b-e5543c3dbab3","originalAuthorName":"管有祥"},{"authorName":"徐光","id":"39cf43f2-ad50-4d30-ac4f-239fa6575552","originalAuthorName":"徐光"},{"authorName":"王应进","id":"364dbff3-800d-4814-b201-7ebe98bb3aeb","originalAuthorName":"王应进"},{"authorName":"吴晓峰","id":"506c53d8-aa33-4b89-b0f4-16c0bccc9468","originalAuthorName":"吴晓峰"},{"authorName":"刘霞","id":"a6d43bdb-fd7d-428b-b475-46e5fa82aba1","originalAuthorName":"刘霞"},{"authorName":"朱利亚","id":"e995cf97-b478-40d5-8dc1-ea1b253de82f","originalAuthorName":"朱利亚"},{"authorName":"刘云杰","id":"bb0401c2-ca57-4d03-82d6-ca2119e555d8","originalAuthorName":"刘云杰"},{"authorName":"马媛","id":"e9e251d8-de8a-4793-b4d2-0ffc8e727a51","originalAuthorName":"马媛"},{"authorName":"安中庆","id":"6f53b089-1695-4ad4-9cf5-383a4a4c2c5d","originalAuthorName":"安中庆"},{"authorName":"甘建壮","id":"de84c5c9-b144-4e8f-b0db-a59c2cb0056e","originalAuthorName":"甘建壮"}],"doi":"10.3969/j.issn.1004-0676.2011.02.014","fpage":"67","id":"edceddc9-97ff-4e9c-9d8f-1c6a27505d8c","issue":"2","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"887eaaec-a071-4b50-8303-d651061265f6","keyword":"分析化学","originalKeyword":"分析化学"},{"id":"4fc2d847-7727-441e-8d10-da729841383f","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"3beb7811-462b-462d-9be2-d0b91387091d","keyword":"催化剂","originalKeyword":"催化剂"},{"id":"d392bc6d-7c5c-45de-a364-ba1b9f536b8c","keyword":"<span style=\"color:red\">金</span>保护剂","originalKeyword":"金保护剂"},{"id":"5c0f78e6-47ac-4ce3-9796-a39f24a55c6b","keyword":"铂钯铑","originalKeyword":"铂钯铑"}],"language":"zh","publisherId":"gjs201102014","title":"用<span style=\"color:red\">金</span>作保护剂铅<span style=\"color:red\">试</span><span style=\"color:red\">金</span>富集汽车尾气净化催化剂中铂钯铑的研究","volume":"32","year":"2011"},{"abstractinfo":"将等离子体光谱法和X荧光光谱法应用于贵金属湿法冶炼物料中<span style=\"color:red\">金</span>的测定.通过对多种不同组成物料的测定及与经典<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>法进行的大量对照试验,拟定了测定金的新方法.光谱法具有测定快速、线性范围宽、准确度好、精密度高等优点,完全能满足生产控制及科研的需要.","authors":[{"authorName":"傅俊卫","id":"ef8a0fc0-2e80-4bc9-b0e6-8521c7d73135","originalAuthorName":"傅俊卫"},{"authorName":"夏珍珠","id":"0144e130-5550-40e2-bb18-e2d54d10aedb","originalAuthorName":"夏珍珠"}],"doi":"10.3969/j.issn.1000-7571.2003.03.017","fpage":"48","id":"08cb4a7b-a4d6-4171-b136-2cb16b4fc37c","issue":"3","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"9d1a481b-4add-42a9-98aa-4a820a0d9c6c","keyword":"湿法冶炼","originalKeyword":"湿法冶炼"},{"id":"7c170beb-efd1-4f11-aeb8-0b93506a8b22","keyword":"<span style=\"color:red\">金</span>","originalKeyword":"金"},{"id":"33f24545-73fa-4b51-919e-ec19a7ed27f0","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>","originalKeyword":"火试金"},{"id":"3520cf1f-94a9-4585-9777-a2fa704bfb44","keyword":"ICP-AES","originalKeyword":"ICP-AES"},{"id":"46d5c274-5eb3-44dd-9e87-b0197780f84b","keyword":"半定量分析","originalKeyword":"半定量分析"}],"language":"zh","publisherId":"yjfx200303017","title":"光谱法测定贵金属湿法冶炼物料中的<span style=\"color:red\">金</span>","volume":"23","year":"2003"},{"abstractinfo":"采用样品与试剂混合, 直接在灰皿中进行熔融、灰吹,合粒用硝酸分解,<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>法测定树脂中的<span style=\"color:red\">金</span>.实验结果表明,该方法对测定树脂中的<span style=\"color:red\">金</span>具有较好的准确度,相对标准偏差为1.27 %.","authors":[{"authorName":"李小玲","id":"b12237c4-4d34-445c-b77f-18d61ac74404","originalAuthorName":"李小玲"}],"doi":"10.3969/j.issn.1001-1277.2010.04.015","fpage":"54","id":"e10aef27-91ba-40dc-b6e0-852bef8a2b4f","issue":"4","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"0a96019f-9436-44b9-9da4-e15ec8bce2d1","keyword":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>法","originalKeyword":"火试金法"},{"id":"3bf169fe-5d80-47b4-8de5-b27501454c8d","keyword":"树脂","originalKeyword":"树脂"},{"id":"e554c720-bf1e-47a1-ba42-5a3891e30487","keyword":"<span style=\"color:red\">金</span>","originalKeyword":"金"}],"language":"zh","publisherId":"huangj201004015","title":"<span style=\"color:red\">火</span><span style=\"color:red\">试</span><span style=\"color:red\">金</span>法测定树脂中的<span style=\"color:red\">金</span>","volume":"31","year":"2010"}],"totalpage":332,"totalrecord":3315}