{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用光学显微镜、透射电子显微镜和X射线衍射仪研究<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>增强镁基复合材料的铸态组织及<span style=\"color:red\">Mg2B2O5</span>/AZ91D界面反应产物.结果表明:<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>具有孪<span style=\"color:red\">晶</span>结构,其孪生面和晶体生长方向分别为(202)和[010];部分<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>中存在MgB4<span style=\"color:red\">O</span>7颗粒相;在基体<span style=\"color:red\">晶</span>界与<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>之间存在等轴状<span style=\"color:red\">Mg2</span>Si相;<span style=\"color:red\">Mg2B2O5</span>/AZ91D界面处存在厚度不均匀的MgO和MgB<span style=\"color:red\">2</span>相界面层.尽管<span style=\"color:red\">Mg2B2O5</span>、MgO和MgB<span style=\"color:red\">2</span>之间没有确定的晶体学位相关系,但在特定<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>表面观察到(202)<span style=\"color:red\">Mg2B2O5</span>//(002)MgO,[010]<span style=\"color:red\">Mg2B2O5</span>//[110]MgO(002)Mgo//(0001)MgB<span style=\"color:red\">2</span>,[110]MgO//[<span style=\"color:red\">2</span>(11)0]MgB<span style=\"color:red\">2</span>取向关系.最后,讨论<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>对复合材料组织结构和性能的影响.","authors":[{"authorName":"陈善华","id":"c98fef32-9c49-4f56-87b5-8ae99cb32f5d","originalAuthorName":"陈善华"},{"authorName":"金培鹏","id":"a1a05382-4315-460a-976d-00646cfa0088","originalAuthorName":"金培鹏"},{"authorName":"","id":"e0d61888-f350-4f4f-8cd4-1ec959c2419d","originalAuthorName":""}],"doi":"","fpage":"106","id":"070a89ee-0f58-45d4-94ec-bde1f94306f8","issue":"1","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"11e5fd87-549c-493e-ba18-da375f77c45d","keyword":"<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>","originalKeyword":"Mg2B2O5晶须"},{"id":"cc006179-5ca7-4802-a062-044b2ead574c","keyword":"镁合金复合材料","originalKeyword":"镁合金复合材料"},{"id":"d2c92ad4-65d8-4d6c-b49d-e2938c51995a","keyword":"组织","originalKeyword":"组织"},{"id":"745983a4-3ee7-4ed6-9f4b-c9b26a109f1a","keyword":"界面","originalKeyword":"界面"}],"language":"zh","publisherId":"xyjsclygc201101023","title":"<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>增强镁基复合材料的组织与界面结构研究","volume":"40","year":"2011"},{"abstractinfo":"采用溶胶-凝胶法制备的CuO涂覆<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>改善了<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>增强镁基复合材料的界面.利用X射线衍射仪、扫描电镜和透射电子显微镜对CuO涂覆<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>和镁基复合材料分别进行物相分析、形貌观察和界面结构分析.结果表明:CuO成功地涂覆在了<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>上,CuO涂覆<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>增强镁基复合材料的界面相为MgCu<span style=\"color:red\">2</span>和MgO相,来源于CuO和基体的界面反应产物;基体析出相MgZn<span style=\"color:red\">2</span>在<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>两侧平行生长,在特定位置和<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>具有一定的晶体学位向关系:[001]<span style=\"color:red\">Mg2B2O5</span>//[5143] MgZn<span style=\"color:red\">2</span>和(100)<span style=\"color:red\">Mg2B2O5</span>//(0111)MgZn<span style=\"color:red\">2</span>;CuO涂覆<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>增强镁基复合材料的抗拉强度和伸长率分别提高了37.6％和35.7％.","authors":[{"authorName":"韩丽","id":"34084e25-e987-440a-a365-1da848a9ca6e","originalAuthorName":"韩丽"},{"authorName":"金培鹏","id":"cca99c1e-d670-4406-802c-7b807f70cd8b","originalAuthorName":"金培鹏"},{"authorName":"陈善华","id":"1c6834b6-b702-4d76-b13b-5e095167bbcb","originalAuthorName":"陈善华"},{"authorName":"王金辉","id":"2082e375-4482-4943-931c-1d8c71c4888d","originalAuthorName":"王金辉"}],"doi":"","fpage":"1221","id":"5e208921-6172-43ab-9d25-15d5bdb6ba3b","issue":"6","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"8ef8106f-9f95-436d-aa74-4fc8d9315e55","keyword":"溶胶-凝胶","originalKeyword":"溶胶-凝胶"},{"id":"02238629-8918-4d29-ad94-492852c82c99","keyword":"<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>","originalKeyword":"Mg2B2O5晶须"},{"id":"b99b825b-4541-4be5-afd1-db082dc3ceac","keyword":"镁基复合材料","originalKeyword":"镁基复合材料"},{"id":"5abb483b-9f4c-4843-8794-d4ce8e28b7d2","keyword":"界面","originalKeyword":"界面"}],"language":"zh","publisherId":"xyjsclygc201306026","title":"CuO涂覆<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>增强镁基复合材料界面结构研究","volume":"42","year":"2013"},{"abstractinfo":"有关Ni-P-SiC复合镀层耐蚀性的研究不多.为此,在<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>增强AZ91D镁基复合材料表面化学镀Ni-P-SiC层.采用扫描电镜(SEM)、电子探针(EPMA)、电化学方法研究了镀液中纳米SiC含量对镀层表面形貌、成分、耐蚀性、结合力的影响.结果表明:纳米SiC颗粒的加入细化了镀层晶粒,造成了镀层疏松,随着镀液中SiC浓度的增加,复合镀层的耐蚀性逐渐降低,但对基体仍有保护作用,SiC浓度为<span style=\"color:red\">2</span>g/L时耐蚀性较佳,且镀层与基体结合良好.","authors":[{"authorName":"曹海莲","id":"04811c25-59ec-43a5-98d0-07abd6317136","originalAuthorName":"曹海莲"},{"authorName":"王晓民","id":"e2cec482-5d40-4a0d-b5af-55c50c6afa5e","originalAuthorName":"王晓民"},{"authorName":"南辉","id":"a3f52c7a-9373-490b-8957-53c818346ec8","originalAuthorName":"南辉"},{"authorName":"邱彦星","id":"72b24e3a-183e-4794-aa09-9fddc1eae782","originalAuthorName":"邱彦星"},{"authorName":"王繁茂","id":"becd8d8e-ddeb-4a7f-87ae-c69440332ee3","originalAuthorName":"王繁茂"},{"authorName":"杨鑫","id":"babcb81c-bb41-4b07-8094-1d1bca78842d","originalAuthorName":"杨鑫"},{"authorName":"陈国顺","id":"549a8eed-d62b-49f3-a5ac-080b0431f6ae","originalAuthorName":"陈国顺"}],"doi":"","fpage":"27","id":"879a4ba7-5758-410b-8a27-cdde0220c93c","issue":"4","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"d432471b-711f-4624-9b78-f772de79118b","keyword":"化学镀","originalKeyword":"化学镀"},{"id":"2a6f52f3-728e-419c-8630-72436348ab1b","keyword":"镁基复合材料","originalKeyword":"镁基复合材料"},{"id":"11da9f66-b9fd-498e-a066-59636b9d203c","keyword":"Ni-P-SiC复合镀层","originalKeyword":"Ni-P-SiC复合镀层"},{"id":"1c51db00-2dc4-4ff6-89f4-d0c6879ce584","keyword":"纳米SiC","originalKeyword":"纳米SiC"},{"id":"86ea2d00-447e-4e46-b8b0-8665612938ab","keyword":"耐蚀性","originalKeyword":"耐蚀性"}],"language":"zh","publisherId":"clbh201504008","title":"<span style=\"color:red\">Mg2B2O5</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>增强AZ91D镁基复合材料表面Ni-P-SiC化学镀层的耐蚀性与SiC含量的关系","volume":"48","year":"2015"},{"abstractinfo":"以六水硝酸镁、硼酸、甘氨酸、尿素为原料,运用溶液燃烧法合成了<span style=\"color:red\">Mg2B2O5</span>亚微米棒.利用XRD,SEM,TPG-DTA表征手段对产物及产物前驱体进行表征.讨论了不同温度、燃烧剂、<span style=\"color:red\">Mg</span>∶<span style=\"color:red\">B</span>比例和煅烧时间对产物的物相、形貌的影响.确定合成<span style=\"color:red\">Mg2B2O5</span>亚微米棒的最佳工艺条件为甘氨酸做燃烧剂、<span style=\"color:red\">Mg</span>∶<span style=\"color:red\">B</span>=1:1、在900℃煅烧4h,得到的产物呈棒状,直径分布在200 ～400 nm之间,长径比分布在3～6之间.","authors":[{"authorName":"贾涵月","id":"2bcf915d-60df-4ff3-8be0-c15e61713709","originalAuthorName":"贾涵月"},{"authorName":"霍慧琴","id":"9714c28b-92f7-4e40-b675-2786d17ef2ad","originalAuthorName":"霍慧琴"},{"authorName":"闫玉芳","id":"e662f66b-79ab-4ba7-8b7f-929e608b9136","originalAuthorName":"闫玉芳"},{"authorName":"李晓芳","id":"b16f08ae-8d29-428f-a392-d2026397b6aa","originalAuthorName":"李晓芳"},{"authorName":"田苗苗","id":"54debf0d-b131-4063-9eba-4657780f7afa","originalAuthorName":"田苗苗"},{"authorName":"储刚","id":"cbf5fb49-86a5-4917-b842-a49943eb4911","originalAuthorName":"储刚"}],"doi":"","fpage":"2321","id":"bc4400a1-fe19-49ba-9ed0-e20f934097e9","issue":"8","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"1ff6c819-902a-4edf-9aff-c480a28e59b4","keyword":"溶液燃烧法","originalKeyword":"溶液燃烧法"},{"id":"c75dc2f7-c826-42b0-adb0-7b45486d9d9b","keyword":"<span style=\"color:red\">Mg2B2O5</span>亚微米棒","originalKeyword":"Mg2B2O5亚微米棒"},{"id":"24ffed0f-0e87-4e75-9b8e-c8700926232b","keyword":"甘氨酸","originalKeyword":"甘氨酸"}],"language":"zh","publisherId":"rgjtxb98201508050","title":"溶液燃烧法制备<span style=\"color:red\">Mg2B2O5</span>亚微米棒","volume":"44","year":"2015"},{"abstractinfo":"在变形温度为250 ～400℃,应变速率<span style=\"color:red\">5</span>×10-<span style=\"color:red\">5</span>～0.5 s-1范围内,研究了均匀化热处理态<span style=\"color:red\">Mg2B2O5</span>/AZ63<span style=\"color:red\">B</span>镁基复合材料的热压缩变形行为,并利用双曲线正弦函数建立了其本构方程.结果表明:复合材料的峰值应力及其对应的应变均随温度的降低及应变速率的增加而增大;计算峰值应力与实验值的比较表明双曲正弦函数可以准确描述复合材料的本构关系;复合材料的应力指数n和激活能Q分别为5.5和221 kJ/mol,其变形机制为晶格扩散控制的位错攀移机制.热挤压试验表明:经过均匀化热处理,复合材料的最大及稳态挤压力与铸态相比分别下降了92 kN和80 kN.","authors":[{"authorName":"朱云鹏","id":"8cc1d3db-928b-4f70-9586-aa81282f52e5","originalAuthorName":"朱云鹏"},{"authorName":"解品","id":"de4567f7-c8e7-43cd-88c9-5c6240049480","originalAuthorName":"解品"},{"authorName":"张瑞","id":"42558abc-94f3-485d-9aa7-31ddcd386d0f","originalAuthorName":"张瑞"},{"authorName":"金培鹏","id":"23c81a11-0927-4ba2-a4be-1e0c6dfe84fb","originalAuthorName":"金培鹏"},{"authorName":"徐仕翀","id":"262939da-d1d0-4e95-bef2-a7250a094d80","originalAuthorName":"徐仕翀"}],"doi":"","fpage":"47","id":"cb676f9d-b4aa-4e08-ba8a-30c6be7eadfa","issue":"10","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"3358fb95-2570-4d85-87ee-da9653e2ed24","keyword":"镁基复合材料","originalKeyword":"镁基复合材料"},{"id":"ee5a93d3-df7e-4d5a-a341-525702a7a90e","keyword":"热变形","originalKeyword":"热变形"},{"id":"03c2d719-3a80-45d9-a217-8fd080719645","keyword":"均匀化热处理","originalKeyword":"均匀化热处理"},{"id":"d437ba71-8a00-4125-9752-f9344f38de22","keyword":"本构关系","originalKeyword":"本构关系"}],"language":"zh","publisherId":"jsrclxb201610009","title":"搅拌铸造工艺制备<span style=\"color:red\">Mg2B2O5</span>/AZ63<span style=\"color:red\">B</span>镁基复合材料的热变形行为","volume":"37","year":"2016"},{"abstractinfo":"采用X射线衍射仪、X射线光电子能谱仪、扫描电子显微镜和透射电子显微镜对萃取<span style=\"color:red\">Mg2B2O5</span>w的物相、表面元素化学状态变化及<span style=\"color:red\">Mg2B2O5</span>w/AZ91D复合材料界面反应产物进行了研究.结果表明:<span style=\"color:red\">Mg2B2O5</span>w/AZ91D界面处存在厚度不均匀的MgO和MgB<span style=\"color:red\">2</span>相界面层;MgO的形成主要与复合材料制备过程中<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>表面上的吸附氧有关,而界面产物MgB<span style=\"color:red\">2</span>则应来源于<span style=\"color:red\">Mg2B2O5</span>w分解产物<span style=\"color:red\">B2O</span>3与基体中<span style=\"color:red\">Mg</span>的反应;<span style=\"color:red\">Mg2B2O5</span>w、MgO和MgB<span style=\"color:red\">2</span>之间通常没有确定的晶体学位相关系,但在特定<span style=\"color:red\">Mg2B2O5</span>w表面观察到(202)<span style=\"color:red\">Mg2B2O5</span>w//(002)MgO,[010]<span style=\"color:red\">Mg2B2O5</span>//[110]MgO和(002)MgO//(0001)MgB<span style=\"color:red\">2</span>,[110]MgO//[2110]MgB<span style=\"color:red\">2</span>取向关系.","authors":[{"authorName":"陈善华","id":"ed2c10b2-3a5d-4f42-947b-f630b2793364","originalAuthorName":"陈善华"},{"authorName":"何晓明","id":"c8b80c63-211e-434a-857b-33ad8f95b61b","originalAuthorName":"何晓明"},{"authorName":"金培鹏","id":"11a2e5d8-641b-490b-b5d1-b20394614781","originalAuthorName":"金培鹏"},{"authorName":"","id":"7ffcba80-3a72-44e0-a9c4-831082ebb06e","originalAuthorName":""}],"doi":"","fpage":"16","id":"82d7bb36-d89c-4698-898a-d8d23afc431e","issue":"2","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"e6b1e6cb-4b74-419d-9cbe-980fb05bf00b","keyword":"<span style=\"color:red\">Mg2B2O5</span>w","originalKeyword":"Mg2B2O5w"},{"id":"e683780f-d219-4e73-85a2-6b0d782cac09","keyword":"镁基复合材料","originalKeyword":"镁基复合材料"},{"id":"ab3f586b-fd30-444b-b5f2-44aa37ae9a7a","keyword":"界面","originalKeyword":"界面"},{"id":"ba6fac8f-809a-4d9a-8d51-851de9fade72","keyword":"形成机理","originalKeyword":"形成机理"}],"language":"zh","publisherId":"jsrclxb201102004","title":"<span style=\"color:red\">Mg2B2O5</span>w/AZ91D镁基复合材料的界面结构及其形成机理","volume":"32","year":"2011"},{"abstractinfo":"本文采用9Al<SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">O</span><SUB>3</SUB>·<span style=\"color:red\">2B</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">O</span><SUB>3</SUB><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>补强了PZT95／<span style=\"color:red\">5</span>型铁电相变陶瓷材料，研究了<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>添加量与材料的电性能和力学性能之间的关系，实验结果表明：（1）复合材料的最佳烧结温度随着添加含量的增加而降低．（<span style=\"color:red\">2</span>）适量的<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>添加对材料的特殊电性能无明显影响，而材料的力学性能有较明显的改善，例如含0．3wt％<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>的材料，其抗折强度比基料提高了42．24％．（3）品<span style=\"color:red\">须</span>的拔出，桥接对材料的增韧补强具有重要意义.","authors":[{"authorName":"李晓晖","id":"c76ca263-8648-441a-a3ad-206203ef9fba","originalAuthorName":"李晓晖"},{"authorName":"林盛卫","id":"523607d6-f884-410f-9b27-42a9bd64e4f0","originalAuthorName":"林盛卫"},{"authorName":"瞿翠凤","id":"6e4f8dab-9b92-4a02-be81-9f5e2dfec5f1","originalAuthorName":"瞿翠凤"},{"authorName":"姚春华","id":"6f67d7e1-b8e2-43d9-b62a-dde707c038bd","originalAuthorName":"姚春华"},{"authorName":"金绮华","id":"7e1b4b42-a5f9-450d-b557-a53993906f80","originalAuthorName":"金绮华"}],"categoryName":"|","doi":"","fpage":"315","id":"ed038e37-3613-4687-8bd0-0dfece1c4043","issue":"3","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"03aba96a-f1a8-4e9f-9b31-304275d51d1e","keyword":"<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>","originalKeyword":"晶须"},{"id":"28e3b64a-93e6-481a-8cc6-3f9bcdf6497e","keyword":" reinforce","originalKeyword":" reinforce"},{"id":"4df03313-6ef7-4ffb-902e-09a8f4beaeeb","keyword":" PZT95/<span style=\"color:red\">5</span>","originalKeyword":" PZT95/5"},{"id":"9d62fa81-a47e-4ae2-bc7c-8e473b6ea4d4","keyword":" mechanical properties","originalKeyword":" mechanical properties"},{"id":"4eba0903-bf34-40e5-9fe6-f45e17d19c1f","keyword":" electric properties","originalKeyword":" electric properties"}],"language":"zh","publisherId":"1000-324X_1997_3_19","title":"9Al<SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">O</span><SUB>3</SUB>·<span style=\"color:red\">2B</span><SUB><span style=\"color:red\">2</span></SUB><span style=\"color:red\">O</span><SUB>3</SUB><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>补强PZT95/<span style=\"color:red\">5</span>型铁电相变陶瓷材料的研究","volume":"12","year":"1997"},{"abstractinfo":"以MgCl<span style=\"color:red\">2</span>为原料,NaOH为沉淀剂,研究了它们的浓度配比、反应温度、<span style=\"color:red\">晶</span>化温度、<span style=\"color:red\">晶</span>化时间、<span style=\"color:red\">晶</span>化方式等因素对形成<span style=\"color:red\">Mg</span>(OH)<span style=\"color:red\">2</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>的影响. 结果表明,当n(MgCl<span style=\"color:red\">2</span>): n(NaOH)=1.20: 1.92、混合温度Tm=86 ℃、<span style=\"color:red\">晶</span>化温度Tc=100 ℃、<span style=\"color:red\">晶</span>化时间Time=5.5 h时,可以得到发育不完全的初级<span style=\"color:red\">Mg</span>(OH)<span style=\"color:red\">2</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>. 若改用水热法<span style=\"color:red\">晶</span>化,可得到发育较好的<span style=\"color:red\">Mg</span>(OH)<span style=\"color:red\">2</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>. 在此基础上,若在NaOH溶液中加入一定量的有机溶剂OR(NaOH浓度不变)时,即可得到发育更完善的<span style=\"color:red\">Mg</span>(OH)<span style=\"color:red\">2</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>. 电子显微镜照片显示,粒子呈<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>形状,粒度分布均匀,分散性好,晶形好,纯度高. 并对<span style=\"color:red\">晶</span>须生长机理进行了初步分析.","authors":[{"authorName":"吴健松","id":"1f0bb896-6f73-4c0f-a563-0a91064e3280","originalAuthorName":"吴健松"},{"authorName":"肖应凯","id":"5dee3f71-a53d-4926-9930-157b6bcc960a","originalAuthorName":"肖应凯"},{"authorName":"张丽","id":"e173ea07-d31d-4667-a0d0-be9563763b44","originalAuthorName":"张丽"},{"authorName":"匡文华","id":"90c9a732-b548-4121-838f-e752017c33a0","originalAuthorName":"匡文华"},{"authorName":"梁海群","id":"c20a1cbe-6de3-4f32-a71a-03f4bc9e766e","originalAuthorName":"梁海群"},{"authorName":"吴康娣","id":"6271d68e-1952-42af-a2b3-d1307a879229","originalAuthorName":"吴康娣"}],"doi":"10.3969/j.issn.1000-0518.2008.05.006","fpage":"529","id":"4b3c7541-dbd4-4aeb-a934-01aa9337082b","issue":"5","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"2775795c-d08c-4b57-825d-7bb4eeab5964","keyword":"<span style=\"color:red\">Mg</span>(OH)<span style=\"color:red\">2</span>","originalKeyword":"Mg(OH)2"},{"id":"d99d7d94-c3ae-4f24-8342-aa06244bfbc2","keyword":"<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>","originalKeyword":"晶须"},{"id":"c83b674d-5c18-4481-8ac1-36ba2add1c4f","keyword":"水热法","originalKeyword":"水热法"},{"id":"db4aa80e-0b15-4ffd-9791-f5d017690785","keyword":"功能材料","originalKeyword":"功能材料"}],"language":"zh","publisherId":"yyhx200805006","title":"<span style=\"color:red\">Mg</span>(OH)<span style=\"color:red\">2</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>的制备","volume":"25","year":"2008"},{"abstractinfo":"六钛酸钾<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>是一种连锁风洞结构的具有优良物理机械性能和稳定化学性能等特点的新型材料。目前KDC法合成六钛酸钾<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>所需的煅烧温度高，且<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>长径比较小，而采用V<span style=\"color:red\">2O5</span>为添加剂的改进KDC法可以降低其煅烧温度，提高<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>长径比，使长径比〉20。实验通过TG—DSC曲线说明V<span style=\"color:red\">2O5</span>的加入可以降低其煅烧温度，通过XRD确定了六钛酸钾<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>的合适煅烧温度、煅烧时间和钒酸盐的加入量，通过SEM说明<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>的长径比、形貌等。结果表明，当煅烧温度为800℃、煅烧时间为<span style=\"color:red\">5</span>h、V<span style=\"color:red\">2O5</span>的加入量为<span style=\"color:red\">2</span>％时，合成的六钛酸钾<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>平均长径比可达到22，且晶体结晶性好，形貌均匀。","authors":[{"authorName":"牛飞","id":"c3604dbf-aae1-4978-8ed5-52f3f1fd1ff6","originalAuthorName":"牛飞"},{"authorName":"刘自力","id":"51a6da3d-f151-4f62-b3b6-95b63bf8efdb","originalAuthorName":"刘自力"},{"authorName":"张健杰","id":"0ac7395b-b290-424e-a10c-9122d813ba40","originalAuthorName":"张健杰"},{"authorName":"向超","id":"6018f053-7452-4c25-9d11-2207777e0c8a","originalAuthorName":"向超"},{"authorName":"徐阳阳","id":"7342217b-1079-468f-8622-5ab655fa2c78","originalAuthorName":"徐阳阳"}],"doi":"","fpage":"1700","id":"3843a2f8-9c85-4a05-8ee4-d6e6c1f05881","issue":"13","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"968882a6-a3b4-4d3b-9f5a-df3ce74128a1","keyword":"六钛酸钾<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>","originalKeyword":"六钛酸钾晶须"},{"id":"35a3607c-1b9a-4066-919d-cce15b258591","keyword":"改进KDC法","originalKeyword":"改进KDC法"},{"id":"5800e45e-1b07-45be-af7e-a7ebd05a7bff","keyword":"煅烧","originalKeyword":"煅烧"},{"id":"26489376-60fa-419d-af3c-e87e22779ac3","keyword":"V<span style=\"color:red\">2O5</span>","originalKeyword":"V2O5"},{"id":"9403ac43-b67e-4565-9821-a63ae92024da","keyword":"长径比","originalKeyword":"长径比"}],"language":"zh","publisherId":"gncl201213010","title":"V<span style=\"color:red\">2O5</span>促进六钛酸钾<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>的合成","volume":"43","year":"2012"},{"abstractinfo":"以苦卤为原料,先在体系中加入Na<span style=\"color:red\">2</span>CO3-NaHCO3缓冲溶液,再以Na<span style=\"color:red\">2</span>CO3为沉淀剂,采用液相沉淀法制备了直<span style=\"color:red\">晶</span>率好、分散性好的碱式碳酸镁<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>(<span style=\"color:red\">Mg2</span> (OH)<span style=\"color:red\">2</span>CO3·3H<span style=\"color:red\">2O</span>).通过元素分析、SEM及XRD测试等手段分别表征了产品的纯度、形貌特征及属性.结果表明,碱式碳酸镁<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>分散性好、晶形好、粒度分布均匀、<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>质量好.当反应温度T=32℃,反应时间t=69 h时可获得晶形好、表面光滑的碱式碳酸镁<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>.","authors":[{"authorName":"吴健松","id":"546f5494-cd49-4e7d-8577-6af747a6ef9e","originalAuthorName":"吴健松"},{"authorName":"梁海群","id":"f79b4ce8-a49d-41a8-a716-97e156a532d9","originalAuthorName":"梁海群"},{"authorName":"黄雪清","id":"e1600488-86bd-4044-a9e8-abcf825716bc","originalAuthorName":"黄雪清"}],"doi":"","fpage":"1713","id":"37d87271-0b5b-475a-95c1-02472aa5fc68","issue":"6","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"ddc0a01f-c233-4508-8eec-09a94814cf7c","keyword":"碱式碳酸镁","originalKeyword":"碱式碳酸镁"},{"id":"85554b69-9281-4401-8d61-055a53681a78","keyword":"<span style=\"color:red\">晶</span><span style=\"color:red\">须</span>","originalKeyword":"晶须"},{"id":"ec72ffac-4bfb-4055-9e98-5c042659fdc0","keyword":"苦卤","originalKeyword":"苦卤"},{"id":"2e286de4-4009-455e-aa99-d68afdec071d","keyword":"增韧补强剂","originalKeyword":"增韧补强剂"},{"id":"fb5ffef4-570e-4cef-9669-0fe53a0b81cc","keyword":"阻燃剂","originalKeyword":"阻燃剂"}],"language":"zh","publisherId":"rgjtxb98201506050","title":"徐闻盐场苦卤制备<span style=\"color:red\">Mg2</span>(OH)<span style=\"color:red\">2</span>CO3·3H<span style=\"color:red\">2O</span><span style=\"color:red\">晶</span><span style=\"color:red\">须</span>","volume":"44","year":"2015"}],"totalpage":11271,"totalrecord":112708}