{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用一步溶剂热法合成纤锌矿结构CuInS2(W-CIS)纳米粉体,并对其生长形成机理进行了研究.利用XRD、FE-SEM及EDS对W-CIS纳米晶的结构和形貌以及元素组成进行分析,研究了溶剂热合成过程中的铜源、硫源、反应温度及反应时间对CuInS2纳米粉体物相及形貌的影响.结果表明:以CuCl2·2H2O或Cu(CH3COO)2·H2O、InCl3·4H2O和硫脲为原料,聚乙二醇400、乙二胺为溶剂于200℃下反应2h可以成功合成出结晶性良好的CuInS2纳米片,直径约为300 nm,厚度大约为10～20 nm.通过研究发现,乙二胺对形成纤锌矿结构CuInS2起着关键的作用,并且该粉体对亚甲基蓝的降解率可达75.04％.","authors":[{"authorName":"邹正光","id":"d96661f6-270c-473a-b0ba-c19596951f7d","originalAuthorName":"邹正光"},{"authorName":"<span style=\"color:red\">高</span><span style=\"color:red\">耀</span>","id":"150d9b79-ee2c-4daf-88e8-1352a0f73684","originalAuthorName":"高耀"},{"authorName":"龙飞","id":"6dbf5dc0-d8e7-4eb3-95a1-a28d1cdf2afd","originalAuthorName":"龙飞"},{"authorName":"张劲","id":"f83cba78-dc16-4d36-8443-06d65df5a8e1","originalAuthorName":"张劲"}],"doi":"","fpage":"2164","id":"40246a0e-0580-4a11-8725-31a284d215a7","issue":"8","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"5ea2c596-3565-4961-8d39-70676cb9f15a","keyword":"溶剂热法","originalKeyword":"溶剂热法"},{"id":"7e0df561-0718-4cd6-aaa9-25029659bef7","keyword":"纤锌矿","originalKeyword":"纤锌矿"},{"id":"b4ba0a10-ec13-417f-aba1-da1490d55677","keyword":"CuInS2纳米晶","originalKeyword":"CuInS2纳米晶"},{"id":"c72dc7f4-9f47-4f6f-9e81-b611a8db3937","keyword":"亚甲基蓝","originalKeyword":"亚甲基蓝"},{"id":"bd4e7d08-14a6-4a60-9188-0ee2f0845d94","keyword":"降解率","originalKeyword":"降解率"}],"language":"zh","publisherId":"rgjtxb98201508025","title":"纤锌矿CuInS2纳米晶的合成及其机理研究","volume":"44","year":"2015"},{"abstractinfo":"采用常压下两步溶剂热法合成了In2Se3/CuSe复合粉,并以其为原料,通过喷涂成膜后快速热处理制备了CuInSe2(CIS)薄膜.利用XRD、FE-SEM、EDS对In2Se3/CuSe复合粉的晶体结构和形貌进行分析表征,研究了溶剂热合成过程中的反应温度、表面活性剂对In2Se3/CuSe复合粉体物相及形貌的影响.结果表明:以InCl3·4H2O、Se粉为原料,聚乙二醇-400、水合肼、醋酸为溶剂于120℃下反应30 min可以成功合成出结晶性良好的纯相In2Se3纳米球,直径分布在50 ～ 100 nm之间;以In2Se3纳米粉作为中间产物,分散于乙二醇溶剂中,加入Se源溶液(水合肼溶解Se粉)及CuCl2· 2H2O,90℃下反应30 min可获得In2Se3/CuSe复合粉,其中CuSe呈不规则团聚状均匀分布在In2Se3纳米球的周围,且当加入0.2 g CTAB时获得的In2Se3/CuSe复合粉分散性较好.采用FE-SEM、EDS、XRF和Raman光谱对预置膜和快速热处理后获得的CIS薄膜的形貌和成分进行表征.结果表明:将In2Se3/CuSe复合粉制备成“墨水”后涂覆在镀Mo玻璃基板上,快速升温至550℃可成功获得致密的CIS薄膜.","authors":[{"authorName":"梁凤基","id":"26944d97-f54a-4f3b-a634-f3780f8c0b12","originalAuthorName":"梁凤基"},{"authorName":"龙飞","id":"b6453052-652c-4b21-9369-cfe68e55a402","originalAuthorName":"龙飞"},{"authorName":"莫淑一","id":"bd6a9e78-253c-4434-a0f2-957b4cc49987","originalAuthorName":"莫淑一"},{"authorName":"<span style=\"color:red\">高</span><span style=\"color:red\">耀</span>","id":"7b9df8d4-eda7-4ce3-9aac-3faccf6726c7","originalAuthorName":"高耀"},{"authorName":"邹正光","id":"a49dbeec-e3a8-4033-96bd-b8d9a119f2b6","originalAuthorName":"邹正光"}],"doi":"","fpage":"1705","id":"4d62b841-c764-42ef-bfb3-768ff8b5979c","issue":"7","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"ec393b36-2f3f-4371-9d19-d193dfdcc18b","keyword":"溶剂热","originalKeyword":"溶剂热"},{"id":"0a54871a-1805-474e-83ca-193cf20990af","keyword":"In2Se3/CuSe复合粉","originalKeyword":"In2Se3/CuSe复合粉"},{"id":"c9d94279-365c-48df-8544-69ee1933460d","keyword":"CIS薄膜","originalKeyword":"CIS薄膜"}],"language":"zh","publisherId":"rgjtxb98201407020","title":"溶剂热法合成In2Se3/CuSe复合粉及CulnSe2薄膜的制备","volume":"43","year":"2014"},{"abstractinfo":"选取<span style=\"color:red\">耀</span>州窑瓷胎样品25个, 唐三彩的胎3个, 作坊匣钵料样品1个, <span style=\"color:red\">耀</span>州博物馆附近粘土矿样品4个.用中子活化分析测量样品中29种元素的含量, 从这29种元素中挑选出8种指纹元素, 将指纹元素的含量进行散布分析.结果表明, 出自不同窑口的古<span style=\"color:red\">耀</span>州瓷的胎, 有着长期稳定的、集中的原料产地.<span style=\"color:red\">耀</span>州窑唐三彩的胎料产地和<span style=\"color:red\">耀</span>州瓷胎的原料产地相同.","authors":[{"authorName":"赵维娟","id":"87399813-6333-40d5-8862-e91f3b5eef3e","originalAuthorName":"赵维娟"},{"authorName":"李融武","id":"1b03932d-04df-4c1c-8b1c-f766b5ef1e02","originalAuthorName":"李融武"},{"authorName":"郭敏","id":"0216bca7-6007-4981-b207-9df18e977a41","originalAuthorName":"郭敏"},{"authorName":"<span style=\"color:red\">高</span>正<span style=\"color:red\">耀</span>","id":"5bba8c45-0a23-4659-83fe-09a421da85cb","originalAuthorName":"高正耀"},{"authorName":"李国霞","id":"896c2d21-d3ec-479b-9e6b-e0695a746540","originalAuthorName":"李国霞"},{"authorName":"谢建忠","id":"d7d8b73a-c790-43c7-bde5-f3b4a6d88f65","originalAuthorName":"谢建忠"},{"authorName":"冯松林","id":"fb102442-468e-4bd2-8c59-e4fc7ca3a9ec","originalAuthorName":"冯松林"},{"authorName":"范东宇","id":"4b852ccf-5f2d-4e49-bbe0-34062fc7873b","originalAuthorName":"范东宇"},{"authorName":"张颖","id":"43489065-a945-4433-83a5-f0528162c86c","originalAuthorName":"张颖"},{"authorName":"柴之芳","id":"e9634485-6704-4c72-b271-b1e5ec43051f","originalAuthorName":"柴之芳"},{"authorName":"禚振西","id":"81881df4-70f0-4020-9c42-c25229d5d6e1","originalAuthorName":"禚振西"}],"doi":"10.3969/j.issn.1007-4627.2004.03.015","fpage":"253","id":"1b04eafa-b1a8-47d2-b883-d3bb750bf58f","issue":"3","journal":{"abbrevTitle":"YZHWLPL","coverImgSrc":"journal/img/cover/YZHWLPL.jpg","id":"78","issnPpub":"1007-4627","publisherId":"YZHWLPL","title":"原子核物理评论   "},"keywords":[{"id":"b16c87a3-abb3-4f6f-b591-f24d0883bdeb","keyword":"古<span style=\"color:red\">耀</span>州瓷胎","originalKeyword":"古耀州瓷胎"},{"id":"311313ee-5899-4d29-8792-86fdbba45c66","keyword":"原料产地","originalKeyword":"原料产地"},{"id":"b527c9b6-fd82-4bbb-b728-03f3f2ea21a6","keyword":"中子活化分析","originalKeyword":"中子活化分析"},{"id":"d8e5f8e9-33fa-4552-947b-c974e50cdaa6","keyword":"指纹元素","originalKeyword":"指纹元素"},{"id":"3e2b59e9-8953-464b-ad17-a8b120af1e38","keyword":"散布分析","originalKeyword":"散布分析"}],"language":"zh","publisherId":"yzhwlpl200403015","title":"用指纹元素散布分析研究古<span style=\"color:red\">耀</span>州瓷胎的起源","volume":"21","year":"2004"},{"abstractinfo":"","authors":[],"doi":"","fpage":"","id":"8172436b-b074-4c0f-89d4-d12a00d74437","issue":"6","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"2765bfdf-bedb-41ae-baa5-4d1676b70f5e","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"cldb200106001","title":"徐祖<span style=\"color:red\">耀</span>院士简介","volume":"15","year":"2001"},{"abstractinfo":"","authors":[],"doi":"","fpage":"66","id":"6a2f0b53-ff85-45cd-a11e-74ecbdbd1186","issue":"2","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"f3e715ce-cb49-4bbd-8b72-1106c27d11ef","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jsrclxb200102017","title":"中国科学院院士徐祖<span style=\"color:red\">耀</span>","volume":"22","year":"2001"},{"abstractinfo":"一些合金固溶化(或淬水)后在预贝氏体(孕育)期内等温淬水(或时效),既保持高温时形成的晶体缺陷,又产生新的晶体缺陷.母相中由于溶质原子扩散而在缺陷处发生偏聚,则形成贫/富溶质微区,即类拐点(spinodal-like)分解.当贫溶质微区成分作为Ms,其温度等于或高于淬火(或时效)温度时,贝氏体将以马氏体样切变形核,故贝氏体是在溶质原子扩散控制下切变形核.在TEM温台试验中未发现台阶生长机制,界面上巨型台阶是贝氏体增宽(厚)速度差异所致.","authors":[{"authorName":"康沫狂","id":"d2cf8bbd-9644-4fa9-90f2-92e8b7fd468f","originalAuthorName":"康沫狂"},{"authorName":"朱明","id":"3e36643f-d8cc-4442-8bf4-52e605a7f209","originalAuthorName":"朱明"}],"doi":"10.3969/j.issn.1009-6264.2005.02.001","fpage":"1","id":"60f8a7ab-f1d5-4076-8cd3-acaf2cddcf6b","issue":"2","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"0f1522ab-9f07-404e-a27a-7843b1df3d13","keyword":"预贝氏体期","originalKeyword":"预贝氏体期"},{"id":"5c375e1b-f83e-4df4-a3e0-bbf9c7de279b","keyword":"扩散偏聚","originalKeyword":"扩散偏聚"},{"id":"1c225de7-ac25-47a4-806d-484bf9d27da8","keyword":"贫/富溶质微区","originalKeyword":"贫/富溶质微区"},{"id":"a0082930-00a4-4b9d-a154-c730e03cdb22","keyword":"巨型台阶","originalKeyword":"巨型台阶"},{"id":"258840be-abf7-48e4-8008-738aa7b3ffdc","keyword":"类拐点分解","originalKeyword":"类拐点分解"}],"language":"zh","publisherId":"jsrclxb200502001","title":"关于贝氏体形核和台阶机制的讨论--与徐祖<span style=\"color:red\">耀</span>院士等商榷","volume":"26","year":"2005"},{"abstractinfo":"改变常规镀锌钝化液成膜剂和pH值调整剂,研制出了一种新型<span style=\"color:red\">高</span>耐蚀性钝化工艺.此工艺形成的钝化膜铬含量:Cr(Ⅲ) 0.10 mg/dm2 Cr(Ⅳ) 2.277 mg/dm2 膜重 10.8 mg/dm2.在钝化膜形成后即使未干燥也有较高的抗摩擦性能,同时该膜也具有优异的耐酸碱性能,耐中性盐雾试验可达200 h不出现白锈.","authors":[{"authorName":"刘立炳","id":"6f39ce0a-32c8-4c07-83fd-1d41ca1d33de","originalAuthorName":"刘立炳"},{"authorName":"孙贺民","id":"6e955ca2-f25f-42c9-b50b-a10346d8d73b","originalAuthorName":"孙贺民"},{"authorName":"赵常就","id":"ce60c7fb-f3c5-4443-ad47-ebdeecafe34a","originalAuthorName":"赵常就"},{"authorName":"陈范才","id":"09557497-9030-47c0-9b1f-f8c3e6522a25","originalAuthorName":"陈范才"}],"doi":"10.3969/j.issn.1001-1560.1999.05.006","fpage":"10","id":"1c23cca2-a79b-4fe7-afe4-36967d43cfc6","issue":"5","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"3d1a4044-ff78-4c4d-973d-b1a87c9f5a06","keyword":"镀锌","originalKeyword":"镀锌"},{"id":"9d4b7f9a-2865-4012-8249-aff12b754ea5","keyword":"钝化","originalKeyword":"钝化"},{"id":"c0250205-4b68-4147-ba99-12652fdeb02f","keyword":"耐腐蚀性","originalKeyword":"耐腐蚀性"}],"language":"zh","publisherId":"clbh199905006","title":"<span style=\"color:red\">高</span>耐蚀镀锌钝化","volume":"32","year":"1999"},{"abstractinfo":"介绍了<span style=\"color:red\">高</span>铬<span style=\"color:red\">高</span>钴耐热钢成分设计的理论,研究了耐热钢的微观组织、热处理工艺和力学性能;根据裂纹产生的机制,通过实验的方法建立了恰当的热处理工艺,有效地防止了淬火裂纹的产生.研究表明,通过科学的成分设计和热处理的<span style=\"color:red\">高</span>铬<span style=\"color:red\">高</span>钴耐热钢具有良好的综合力学性能.","authors":[{"authorName":"郭存宝","id":"25e5eeec-0064-4274-b043-4b39bc1d752a","originalAuthorName":"郭存宝"},{"authorName":"龙思远","id":"d80a87e2-90b4-4609-b029-62ec588a2e13","originalAuthorName":"龙思远"},{"authorName":"廖慧敏","id":"b1b0df7f-b01b-40a4-9064-4e66458b284d","originalAuthorName":"廖慧敏"}],"doi":"","fpage":"423","id":"c8a3e764-a7f1-4913-b6d8-c929c225585a","issue":"z1","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"82810b10-af73-459c-b409-41356af934bb","keyword":"耐热钢","originalKeyword":"耐热钢"},{"id":"8ac141bb-5575-48ea-a535-f1a6e5f87911","keyword":"强化理论","originalKeyword":"强化理论"},{"id":"7ed2a4ef-7ff0-4559-b3dd-40be80c98b22","keyword":"DV-Xa分子轨道法","originalKeyword":"DV-Xa分子轨道法"},{"id":"ad505c41-f4b8-461d-af29-5a3b7fbe24f4","keyword":"热处理工艺","originalKeyword":"热处理工艺"}],"language":"zh","publisherId":"cldb2008z1129","title":"<span style=\"color:red\">高</span>铬<span style=\"color:red\">高</span>钴耐热钢的研究","volume":"22","year":"2008"},{"abstractinfo":"本文介绍了新型矿物添加材料赛<span style=\"color:red\">高</span>岭(Metakolin)的物理性能,化学成分,采用ASTM C39,ASTM C1202,稳态迁移等方法着重研究了赛<span style=\"color:red\">高</span>岭混凝土的抗压强度和抗氯离子性能,并与硅粉混凝土及对比波特兰水泥混凝土的有关性能作了比较,探讨了赛<span style=\"color:red\">高</span>岭作为硅粉替代材料生产<span style=\"color:red\">高</span>功能混凝土的可能性.","authors":[{"authorName":"蒋林华","id":"dd749bf4-6ec1-434d-8ebc-1acb0be0b7d4","originalAuthorName":"蒋林华"}],"doi":"10.3969/j.issn.1001-1625.2001.05.011","fpage":"51","id":"0d3fb318-d7bf-498b-a4ed-923c8549c9aa","issue":"5","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"f91221d9-da38-4299-a79c-ad5d348463fb","keyword":"赛<span style=\"color:red\">高</span>岭","originalKeyword":"赛高岭"},{"id":"24ccce66-2bba-47d1-bd5b-06c25a9810bc","keyword":"硅粉","originalKeyword":"硅粉"},{"id":"aa5bb8eb-5846-405e-bf9a-b5dfa40c4e30","keyword":"混凝土","originalKeyword":"混凝土"},{"id":"7656cc44-ccf7-419b-89a2-cb8e3b98d53a","keyword":"性能","originalKeyword":"性能"}],"language":"zh","publisherId":"gsytb200105011","title":"赛<span style=\"color:red\">高</span>岭混凝土研究","volume":"20","year":"2001"},{"abstractinfo":"<span style=\"color:red\">高</span>纯钴主要应用于磁记录材料、磁传感器材料、光电材料等高技术领域.其制备方法有萃取法、离子交换法、电解法、真空熔炼法等.萃取法和离子交换法能够制备<span style=\"color:red\">高</span>纯盐, 这是制备<span style=\"color:red\">高</span>纯钴的重要环节.<span style=\"color:red\">高</span>纯钴盐通过沉淀、氢还原或电解能获得<span style=\"color:red\">高</span>纯金属原料, 该过程也将金属进一步提纯.真空熔炼法能够进一步提纯金属, 并得到性能优异的金属锭.采用几种方法结合的工艺路线可以制备出品质优良的<span style=\"color:red\">高</span>纯材料.","authors":[{"authorName":"陈蓉","id":"98ce9af8-9406-4938-922c-18ecde6bed5f","originalAuthorName":"陈蓉"},{"authorName":"王力军","id":"cf76c8fe-17ca-4520-8621-e2c05b9b174c","originalAuthorName":"王力军"},{"authorName":"罗远辉","id":"1b53adc4-cbda-42b6-aca0-68a6dd0e2d44","originalAuthorName":"罗远辉"},{"authorName":"张力","id":"fbfb43b4-a869-40d9-99bb-c9c878849c28","originalAuthorName":"张力"},{"authorName":"陈松","id":"833018c9-94d0-4ca8-8e3f-85f6c3836d61","originalAuthorName":"陈松"},{"authorName":"韩林","id":"c2971562-454c-4a36-b2a9-61821e47fc32","originalAuthorName":"韩林"}],"doi":"10.3969/j.issn.0258-7076.2005.05.043","fpage":"797","id":"3956c55f-58ec-4703-afd1-9a523af04a52","issue":"5","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"69952c2c-6965-4ad8-92c7-450421ec9087","keyword":"<span style=\"color:red\">高</span>纯钴","originalKeyword":"高纯钴"},{"id":"d31fc244-f68b-4e76-b2e7-70069c919ea3","keyword":"萃取","originalKeyword":"萃取"},{"id":"4ac104a9-eb8c-469f-b537-493a100251c4","keyword":"离子交换","originalKeyword":"离子交换"},{"id":"194ef3cf-12c1-424b-b15d-9bc6aa1c49a9","keyword":"电解","originalKeyword":"电解"},{"id":"7e1c90f2-8949-452f-be43-5aa40155e141","keyword":"真空熔炼","originalKeyword":"真空熔炼"}],"language":"zh","publisherId":"xyjs200505043","title":"<span style=\"color:red\">高</span>纯钴制备技术","volume":"29","year":"2005"}],"totalpage":2229,"totalrecord":22282}