{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":4,"startPagecode":1},"records":[{"abstractinfo":"增韧环氧树脂是环氧树脂领域的研究热点,本文就环氧树脂增韧研究进行了概述,介绍了近年来环氧树脂增韧方法及相应的增韧机理研究进展,力求为环氧树脂在增韧领域的进一步研究提供新的思路和方法,以进一步扩展环氧树脂的应用领域.","authors":[{"authorName":"史孝群","id":"c43d6cab-5ef1-4565-9573-567b3f7c6c2f","originalAuthorName":"史孝群"},{"authorName":"肖久梅","id":"6933fd63-163e-448f-a6de-ec04f0239293","originalAuthorName":"肖久梅"},{"authorName":"<span style=\"color:red\">龚</span><span style=\"color:red\">春</span><span style=\"color:red\">秀</span>","id":"77c35493-1ade-41ac-96cb-04cf664b6c6e","originalAuthorName":"龚春秀"},{"authorName":"马文江","id":"e0610a5c-5e7c-40f5-bc7a-b9e2e8a1fdb9","originalAuthorName":"马文江"},{"authorName":"刘建林","id":"9d546f75-9d78-4c1f-866b-5e83b48df1f4","originalAuthorName":"刘建林"}],"doi":"10.3969/j.issn.1009-9239.2002.01.011","fpage":"31","id":"a97fc26e-7ab5-401d-8828-1ea14dbc5cf4","issue":"1","journal":{"abbrevTitle":"JYCL","coverImgSrc":"journal/img/cover/JYCL.jpg","id":"50","issnPpub":"1009-9239","publisherId":"JYCL","title":"绝缘材料"},"keywords":[{"id":"61ff75c9-1300-4082-b780-1f529fe8a5d3","keyword":"环氧树脂","originalKeyword":"环氧树脂"},{"id":"0ed76ed2-d91c-49a9-b80b-d41076b76576","keyword":"增韧","originalKeyword":"增韧"},{"id":"7ae95bf4-12db-4506-8c03-5584e483629f","keyword":"增韧机理","originalKeyword":"增韧机理"}],"language":"zh","publisherId":"jycltx200201011","title":"环氧树脂增韧研究进展","volume":"35","year":"2002"},{"abstractinfo":"采用Chiralpak IC手性柱(250 mm×4.6 mm,5 μm),建立了正相高效液相色谱测定板蓝根中表告依<span style=\"color:red\">春</span>(R-告依<span style=\"color:red\">春</span>)和告依<span style=\"color:red\">春</span>(S-告依<span style=\"color:red\">春</span>)含量的方法.考察了流动相组成、流速和柱温对分离度的影响.经优化后的实验条件:以正己烷-异丙醇(体积比为90∶10)为流动相,流速为0.8 mL/min;检测波长为245 nm,柱温为20 ℃.在此优化条件下,表告依<span style=\"color:red\">春</span>和告依春分离度为3.4,检出限为2.0 mg/L,在0.02～2.0 g/L 范围内有良好的线性关系,平均回收率为101% ,相对标准偏差(RSD)小于3.0%(n=6).本方法可将具有抗病毒活性的表告依<span style=\"color:red\">春</span>与其对映体告依<span style=\"color:red\">春</span>基线分离并测定,专属性强,能有效控制板蓝根的质量.","authors":[{"authorName":"聂黎行","id":"fee7f0b1-4bfd-4c4e-9d65-d7f03c2a918a","originalAuthorName":"聂黎行"},{"authorName":"王钢力","id":"ee281225-e77f-4477-a486-a098ca91b1db","originalAuthorName":"王钢力"},{"authorName":"戴忠","id":"813e1426-d061-4e41-9723-d75cfa16968e","originalAuthorName":"戴忠"},{"authorName":"林瑞超","id":"3034f33a-eaf2-4665-8751-f5ef70c65379","originalAuthorName":"林瑞超"}],"doi":"10.3724/SP.J.1123.2010.01001","fpage":"1001","id":"32355b8f-ccce-4726-b210-eaacc0917986","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"5c41c71f-d053-43ba-8aa9-32ad96d3cca4","keyword":"手性高效液相色谱法","originalKeyword":"手性高效液相色谱法"},{"id":"e26a591e-56ec-4bb4-acfd-5d5f7ad919ea","keyword":"表告依<span style=\"color:red\">春</span>(R-告依<span style=\"color:red\">春</span>)","originalKeyword":"表告依春(R-告依春)"},{"id":"1e32ab35-876b-46d9-9898-47fb5c40d701","keyword":"告依<span style=\"color:red\">春</span>(S-告依<span style=\"color:red\">春</span>)","originalKeyword":"告依春(S-告依春)"},{"id":"8c1b4600-8fac-47f6-98f6-6670e2a0daa9","keyword":"板蓝根","originalKeyword":"板蓝根"}],"language":"zh","publisherId":"sp201010018","title":"手性高效液相色谱法测定板蓝根中表告依<span style=\"color:red\">春</span>和告依<span style=\"color:red\">春</span>含量","volume":"28","year":"2010"},{"abstractinfo":"利用铱催化高碘酸钾氧化丽<span style=\"color:red\">春</span>红G(PG)的褪色反应,建立了测定痕量铱的催化动力学光度法.在硫酸介质和90℃加热15min的条件下,于500nm波长处,采用固定时间法测定丽<span style=\"color:red\">春</span>红G吸收值的降低.Ir(Ⅳ)的浓度在0～1.0μg/25mL范围内与催化反应的速率有良好的线性关系,检出限为1 81 ×10 mg/mL.对0.3μg/25mLIr(Ⅳ)测定的相对标准偏差为1.61%(n=11).体系至少稳定3.5h.考察了40多种共存离子的影响,大多数常见离子不干扰,方法有较好的选择性.催化反应对Ir(Ⅳ)和丽<span style=\"color:red\">春</span>红G均为一级反应,催化反应的表观活化能为103.66kJ/mol.用于冶金产品及岩矿中铱的测定,结果与推荐值十分吻合.","authors":[{"authorName":"侯能邦","id":"92c62fdf-fec8-4163-aad2-9ed54b7fdce6","originalAuthorName":"侯能邦"},{"authorName":"李祖碧","id":"c4dacfbe-4824-4cbe-a844-91a76be4f69c","originalAuthorName":"李祖碧"},{"authorName":"李崇宁","id":"f7a10f8c-895c-486c-ad99-2b32db2c7164","originalAuthorName":"李崇宁"},{"authorName":"王加林","id":"6d15967f-b1aa-492c-9003-5900696277f5","originalAuthorName":"王加林"},{"authorName":"曹秋娥","id":"b89522cc-6338-40b9-bb28-a8fc73f09d40","originalAuthorName":"曹秋娥"}],"doi":"10.3969/j.issn.1000-7571.2002.05.006","fpage":"17","id":"cf8ee9a7-e782-4fcb-866c-e15d9126e60f","issue":"5","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"3c381e65-e813-4912-b9c8-15299a341a75","keyword":"铱","originalKeyword":"铱"},{"id":"90683ee6-f835-43a8-b573-bc0be1641329","keyword":"丽<span style=\"color:red\">春</span>红G","originalKeyword":"丽春红G"},{"id":"a2a57fdf-fa6d-4d5d-bc97-967b1b2de292","keyword":"高碘酸钾","originalKeyword":"高碘酸钾"},{"id":"4ffcfe3c-3af4-41cd-ae8f-447d4f037585","keyword":"催化光度法","originalKeyword":"催化光度法"}],"language":"zh","publisherId":"yjfx200205006","title":"高碘酸钾氧化丽<span style=\"color:red\">春</span>红G催化光度法测定铱","volume":"22","year":"2002"},{"abstractinfo":"在90 ℃水浴中,Co2+ 能催化铋酸钠氧化丽<span style=\"color:red\">春</span>红S褪色,据此建立了一种褪色光度法测定Co2+ 的新方法.Co2+在0～50 μg/mL范围内遵守比尔定律,表观摩尔吸光系数为1.814×103 L/(mol*cm),最大吸收波长为520 nm,该方法检出限为0.538 μg/mL.该方法用于测定锡-钴枪黑色合金镀液中钴的含量,结果令人满意.","authors":[{"authorName":"郭振良","id":"584bf7f2-7e7f-4127-ade6-2c272d72dfbf","originalAuthorName":"郭振良"},{"authorName":"唐清华","id":"9ce2a809-b843-4434-8e7c-dac0f58527cb","originalAuthorName":"唐清华"},{"authorName":"牟起娜","id":"d37d8b39-f7ec-454c-a7d0-cf3e62dd6762","originalAuthorName":"牟起娜"},{"authorName":"孙言志","id":"7c0484e8-9cab-4b29-a48b-4bcb2c838cd8","originalAuthorName":"孙言志"}],"doi":"10.3969/j.issn.1004-227X.2005.12.018","fpage":"63","id":"8c6b0946-37e5-47d0-aff4-bf52e1cf4d1a","issue":"12","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"f6c28cfe-17af-49c2-b37f-6d1108f657b6","keyword":"丽<span style=\"color:red\">春</span>红S","originalKeyword":"丽春红S"},{"id":"cde44370-4a27-46a1-9f05-62ccb3d33206","keyword":"褪色光度法","originalKeyword":"褪色光度法"},{"id":"e7ed13de-3a0a-4b14-b563-e2203460d95f","keyword":"合金镀液","originalKeyword":"合金镀液"},{"id":"6cccbb22-6b70-42fd-9eb3-d3701b2868e9","keyword":"钴","originalKeyword":"钴"}],"language":"zh","publisherId":"ddyts200512018","title":"丽<span style=\"color:red\">春</span>红S褪色光度法测定锡-钴合金镀液中的钴","volume":"24","year":"2005"},{"abstractinfo":"基于在盐酸介质中,La(Ⅲ)催化过氧化氢氧化丽<span style=\"color:red\">春</span>红(3-羟基-4-(2-磺基-4-[4-苯磺基偶氮]偶氮苯)-2,7-萘二磺酸钠)的褪色反应,建立了一个灵敏度高的测定痕量La(Ⅲ)的催化动力学光度分析法.讨论了酸度、试剂用量、温度、干扰离子等因素的影响;研究了反应的最佳条件;测定了一些动力学参数.催化反应的表观活化能为66.63 kJ/mol.该方法测定La(Ⅲ)的线性范围为0.08～1.6 μg/mL,检出限为0.045 μg/mL.不需要预先分离,可将本方法用于沙子样品中痕量镧的测定,回收率为96.0%～111.5%.","authors":[{"authorName":"柳玉英","id":"d9ec6bd0-d964-4e32-8771-27a252778c36","originalAuthorName":"柳玉英"},{"authorName":"张少全","id":"2b0fcf73-acc9-4fea-8b44-e5a50abeaf85","originalAuthorName":"张少全"}],"doi":"10.3969/j.issn.1000-7571.2007.12.017","fpage":"67","id":"e07dfa5a-d08b-4575-bb1f-6a72fddac954","issue":"12","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"9c1ba52e-d166-412f-b761-4d857c395e9c","keyword":"动力学光度法","originalKeyword":"动力学光度法"},{"id":"ef492496-134d-4429-9178-04a73e0cc88b","keyword":"丽<span style=\"color:red\">春</span>红","originalKeyword":"丽春红"},{"id":"b896c3e7-0783-4577-adb9-3d560b75ea51","keyword":"镧","originalKeyword":"镧"},{"id":"e334331e-4000-434a-8d11-a4d75c544c6c","keyword":"过氧化氢","originalKeyword":"过氧化氢"}],"language":"zh","publisherId":"yjfx200712017","title":"镧(Ⅲ)催化过氧化氢氧化丽<span style=\"color:red\">春</span>红褪色光度法测定痕量镧","volume":"27","year":"2007"},{"abstractinfo":"","authors":[{"authorName":"薛福连","id":"a2751726-3729-490d-abee-964d2ca01af1","originalAuthorName":"薛福连"}],"doi":"10.3969/j.issn.1000-6826.2007.06.024","fpage":"52","id":"97981143-0c6a-49d3-95ff-2db4f5f5f3ec","issue":"6","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"f6268305-5be4-4189-976f-2bd0bb56f0dd","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj200706024","title":"\"金属王国\"中的后起之<span style=\"color:red\">秀</span>——钽","volume":"","year":"2007"},{"abstractinfo":"","authors":[{"authorName":"吴钰重","id":"9c027aa4-b103-451d-8e97-5f473eac2352","originalAuthorName":"吴钰重"}],"doi":"10.3969/j.issn.1000-6826.2015.05.01","fpage":"1","id":"0506a7f0-4c97-4d66-a669-f34c1c16bd2f","issue":"5","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"d9b0bd3a-6769-4f19-8833-73a919a0d3ad","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj201505001","title":"冯<span style=\"color:red\">春</span>：勤恳为师路，执着科研心","volume":"","year":"2015"},{"abstractinfo":"","authors":[],"doi":"","fpage":"30","id":"4e09436c-3eee-4b48-bb73-ee2a705bb4dc","issue":"5","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"b4a6851b-0179-4c6e-8a35-71c97028a68c","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj200105019","title":"全不锈钢微波炉一枝独<span style=\"color:red\">秀</span>","volume":"","year":"2001"},{"abstractinfo":"","authors":[{"authorName":"万晓枫","id":"7ff1ca6f-f37c-4a15-bdf4-f80cfb35ea05","originalAuthorName":"万晓枫"}],"doi":"10.3969/j.issn.1000-6826.2012.05.002","fpage":"3","id":"5e975dfc-623a-4fc0-8e16-acf1a3ad8f9c","issue":"5","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"c82a7a4b-c554-4ad6-b0b2-dd34590ec12c","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj201205002","title":"轻量化与绿色应用的有色金属工业<span style=\"color:red\">秀</span>","volume":"","year":"2012"},{"abstractinfo":"2004年上半年的钯市场为基金所主宰,价格出人意料地突破了300美元/盎司阻力线,收在18个月的高点.基本面虽然没有实质性的支撑,但未来需求的增长潜力大大鼓励了基金的热情.预计下半年的投机活力将有所减弱,基金有撤出商品市场的迹象.但价格处于历史低点、中长期需求看好的钯市场仍有吸引力,因此下半年的钯价仍将在投机的掌控之中.预计价格将在200美元/盎司处有强支撑,上行强阻在31 0～330美元/盎司区间;如果突破该价位,下一个阻力位将在370美元/盎司附近.","authors":[{"authorName":"靳湘云","id":"e350353d-3410-4148-bc78-c56e8c98c1b4","originalAuthorName":"靳湘云"}],"doi":"10.3969/j.issn.1674-3962.2004.08.005","fpage":"19","id":"71d445aa-a10f-45fb-8d62-c4c599bde8fd","issue":"8","journal":{"abbrevTitle":"ZGCLJZ","coverImgSrc":"journal/img/cover/中国材料进展.jpg","id":"80","issnPpub":"1674-3962","publisherId":"ZGCLJZ","title":"中国材料进展"},"keywords":[{"id":"bdc8b742-cce7-460a-b320-d1da28b4cf92","keyword":"钯市场","originalKeyword":"钯市场"},{"id":"f5636990-a8be-4bc4-9beb-ef07ccdb7de8","keyword":"半年","originalKeyword":"半年"},{"id":"81118ffe-6b3f-4337-836f-94830aa05765","keyword":"回顾","originalKeyword":"回顾"},{"id":"d491766d-30e0-4637-a07b-6055c51c4dc5","keyword":"展望","originalKeyword":"展望"}],"language":"zh","publisherId":"zgcljz200408005","title":"枯木逢<span style=\"color:red\">春</span>渐渐进--钯市场2004年上半年回顾与下半年展望","volume":"23","year":"2004"}],"totalpage":4,"totalrecord":37}