{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以Ag粉,Pb粉,Sn粉,Sb粉和Te粉为原料,采用固相合成方法合成了Ag0.5+xSb0.2+xPb6 Sn2 Te10(x=-0.05,0.05,0.1,0.2).经过混料、合成、碎料等,采用热压烧结法将Ag0.5+xSb0.2+xPb6 Sn2 Te10合金粉末烧结成块体材料.运用XRD、SEM方法对材料的物相成分、晶体结构和表面形貌进行了表征.用直接电流法测其电导率；在样品的两端加温场度差,在温度差△T=1～4℃时测其赛贝克系数.","authors":[{"authorName":"王松","id":"36875d1d-129c-424a-a42f-cc40af4e6f02","originalAuthorName":"王松"},{"authorName":"霍凤萍","id":"24cf5d9e-f563-45ee-967b-6d7859e86b4b","originalAuthorName":"霍凤萍"},{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"4551f669-1ba0-4524-9684-5c7bbecd5c46","originalAuthorName":"徐桂英"},{"authorName":"吴荣归","id":"9e9c7ac7-9d30-42a8-9b97-510035726b47","originalAuthorName":"吴荣归"}],"doi":"10.3969/j.issn.1001-4381.2010.z2.082","fpage":"297","id":"1e7bec38-057d-4755-891b-80d3bee0d4be","issue":"z2","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"7a297b2a-7f36-4d7e-a0f4-3a0baf7688e9","keyword":"热压制备","originalKeyword":"热压制备"},{"id":"113e55b7-8780-4a1c-b50a-c29bfc311aab","keyword":"热电性能","originalKeyword":"热电性能"},{"id":"4e9aedba-34f5-4198-aaa2-0bb0a34bcd45","keyword":"Ag0.5+xSb0.2+xPb6 Sn2 Te10","originalKeyword":"Ag0.5+xSb0.2+xPb6 Sn2 Te10"}],"language":"zh","publisherId":"clgc2010z2082","title":"Ag0.5+xSb0.2+xPb6Sn2Te10的热压制备与热电性能","volume":"","year":"2010"},{"abstractinfo":"以Bi粉、Te粉、Se粉、SbI3粉、Gd粉为原料,用高压烧结法制备了Gd掺杂的n型Bi2Te2.7Se0.3热电材料,对制备的样品分别在573、603、633 K真空退火36 h.用粉末XRD和FE-SEM研究了样品的物相及显微形貌;在298～473K范围内测定了样品的热电性能.建立了Bi2Te3基材料的禁带宽度与压力和体积的近似关系式,利用此关系式较好解释了高压烧结样品在退火前后热电性能的变化特性.研究结果表明制备的样品在退火前后均为纳米结构.高压烧结和Gd掺杂使样品晶胞尺寸变大,禁带宽度减小.退火使高压烧结样品的电导率提高,塞贝克系数增大,热导率降低.样品于633 K退火36h后具有较好的热电性能,在423 K时其ZT达到最大值为0.74.","authors":[{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"8753d202-fa1a-4411-9501-7824bd6f927c","originalAuthorName":"徐桂英"},{"authorName":"邹平","id":"1c97b97e-0180-4dc3-8ab7-2d0988a0a42f","originalAuthorName":"邹平"},{"authorName":"王松","id":"5e4c595b-2bf0-4fd1-9627-60b903efc31e","originalAuthorName":"王松"},{"authorName":"张艳华","id":"8c307099-ab98-41e8-b7e5-8e731b78a7e0","originalAuthorName":"张艳华"}],"doi":"","fpage":"950","id":"1f0b5a1d-371f-4359-8d46-89d11825eb0b","issue":"4","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"ee1fadc4-c959-4372-96c5-d1ec6748cc02","keyword":"n型Bi2Te2.7Se0.3热电材料","originalKeyword":"n型Bi2Te2.7Se0.3热电材料"},{"id":"d4016e35-ac18-46c2-801d-a920f0b97fcc","keyword":"高压烧结","originalKeyword":"高压烧结"},{"id":"4ea1e218-c265-4d05-9381-85f5f5aa609c","keyword":"退火","originalKeyword":"退火"},{"id":"d460031c-e179-4fa0-8a24-174808a34043","keyword":"热电性能","originalKeyword":"热电性能"}],"language":"zh","publisherId":"xyjsclygc201504035","title":"退火对高压烧结Gd掺杂Bi2Te2.7Se0.3纳米晶热电性能的影响","volume":"44","year":"2015"},{"abstractinfo":"以获得理想的磷化膜为目的,研究了强酸酸洗除锈对磷化膜性能的影响,总结了强酸酸洗存在的问题,提出了相应的弥补方法.","authors":[{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"919cb801-81d3-4b26-8d92-76b88426c72a","originalAuthorName":"徐桂英"},{"authorName":"周晓霜","id":"437d812d-60cc-4784-9bae-23279f92fac6","originalAuthorName":"周晓霜"}],"doi":"10.3969/j.issn.1001-1560.2003.03.025","fpage":"64","id":"2ffee91b-aa85-41ce-b442-3b47ec7a422e","issue":"3","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"a1618eb3-bca9-4de9-9270-a364b284bc2c","keyword":"磷化","originalKeyword":"磷化"},{"id":"ef044672-a551-4a49-b85f-badc4e6d17c8","keyword":"酸洗","originalKeyword":"酸洗"},{"id":"d6c59735-2d16-4ab4-b760-73e79346b429","keyword":"磷化膜","originalKeyword":"磷化膜"}],"language":"zh","publisherId":"clbh200303025","title":"强酸酸洗对磷化膜质量的影响","volume":"36","year":"2003"},{"abstractinfo":"对用于高炉炉身下部的不烧高密Al2 O3-C质耐火材料在不同体积比的CO与CO2混合气氛中的抗氧化性能进行了热力学分析和全面大量的实验.发现此种材料具有较好的抗氧化性能.以热力学分析和实验结果为基础,说明了其氧化机制,建立了不烧高密Al2 O3-C质耐火材料的氧化动力学模型.","authors":[{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"9a4694ea-bc9b-47f6-a34a-75d52a208634","originalAuthorName":"徐桂英"},{"authorName":"杜鹤<span style=\"color:red\">桂</span>","id":"0ac84d14-d194-4647-a21d-519de29a76ac","originalAuthorName":"杜鹤桂"},{"authorName":"程乃良","id":"efef6490-487d-40d7-afd9-dd8cb0edac99","originalAuthorName":"程乃良"},{"authorName":"崔泽南","id":"ef14b251-72ea-4aaf-a12d-edb8b7fd0457","originalAuthorName":"崔泽南"}],"doi":"","fpage":"59","id":"3a34ae37-aa98-490e-abae-b5d4e862e97f","issue":"8","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"2588f65f-ea6d-4be9-a08c-356ea339a33e","keyword":"高炉","originalKeyword":"高炉"},{"id":"2730493e-0169-4c7a-8a80-61fb0f381852","keyword":"不烧高密Al2O3-C砖","originalKeyword":"不烧高密Al2O3-C砖"},{"id":"218ff7e7-c631-49d8-815c-b2385e49fbf4","keyword":"内衬耐火材料","originalKeyword":"内衬耐火材料"},{"id":"bb4fc3bb-4db6-4e27-bd5c-088b45784e67","keyword":"氧化性能","originalKeyword":"氧化性能"}],"language":"zh","publisherId":"gt200108017","title":"不烧高密Al2 O3-C砖在不同气氛中的抗氧化性能","volume":"36","year":"2001"},{"abstractinfo":"对高炉炉身下部用不烧Al2O3-C质耐火材料在水蒸气环境下的抗氧化性能进行了热力学分析和氧化性能实验。总结出其氧化规律，建立了不烧Al2O3-C质耐火材料的氧化动力学模型。此外，还对氧化前后试样的抗折强度进行了测定和比较。","authors":[{"authorName":"崔泽南","id":"5b5ba0a9-a015-4860-827c-6cc85a08c419","originalAuthorName":"崔泽南"},{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"7bcda852-3f90-4313-86e8-e8e48e8a5613","originalAuthorName":"徐桂英"},{"authorName":"杜鹤<span style=\"color:red\">桂</span>","id":"fde4a66b-70e7-4e9e-bc7f-7d6df91f702d","originalAuthorName":"杜鹤桂"},{"authorName":"程乃良","id":"f0c1900e-0faf-4bf7-804a-8fd084e00d60","originalAuthorName":"程乃良"}],"doi":"","fpage":"71","id":"3b4503d8-32f2-4284-8229-3652759146e9","issue":"3","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"b427a779-fbce-4f95-93a5-f11c2818a82e","keyword":"高炉","originalKeyword":"高炉"},{"id":"9ac8877e-5766-4225-9e54-846e0c730b6b","keyword":"不烧Al2O3-C砖","originalKeyword":"不烧Al2O3-C砖"},{"id":"df277d38-b127-43f1-8784-90fb1f6d6e72","keyword":"耐火材料","originalKeyword":"耐火材料"},{"id":"10e0faa0-b186-46d4-a851-5b05a6b493dc","keyword":"氧化性能","originalKeyword":"氧化性能"}],"language":"zh","publisherId":"gtyjxb200103017","title":"高炉用不烧Al2O3-C质耐火材料在水蒸气中的抗氧化性能","volume":"13","year":"2001"},{"abstractinfo":"采用碳热还原法和不同的添加剂在温度为９７０～１１２０℃、压力为０．１ＭＰａ的Ｎ２条件下，在石墨电阻炉内首次制备出Ｎｂ<EM>Ｃ<SUB>ｘ</SUB></EM>（<EM>ｘ</EM>＝０．９８）－Ｃ三维网状纤维．三维网状纤维的直径为１２～３８ｍ，网的环长为０．２２～２．２μｍ，网孔径为７０～７０１μｍ．本文详细研究了制备的工艺条件及相应的网状纤维的形貌．","authors":[{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"9a2e8a8d-9a38-4188-9eac-23c24a65e749","originalAuthorName":"徐桂英"},{"authorName":"李建保","id":"e54698ce-c864-4936-89ca-5ba731a41416","originalAuthorName":"李建保"},{"authorName":"黄勇","id":"74b52863-a37a-47da-9a1d-ba66c550fdf2","originalAuthorName":"黄勇"},{"authorName":"谢志鹏","id":"da93fb1f-6532-449f-9b79-73702928f04e","originalAuthorName":"谢志鹏"}],"categoryName":"|","doi":"","fpage":"818","id":"5104cd2f-3841-443e-aeac-deebb26eba20","issue":"5","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"dcfc16ca-0816-49ca-a357-b7f8e415bdc5","keyword":"Nb<EM>C<SUB>x</SUB></EM>－C三维网状纤维","originalKeyword":"Nb<EM>C<SUB>x</SUB></EM>－C三维网状纤维"},{"id":"7846b89e-8924-47a9-82ff-d507a73342de","keyword":" Nb<EM>C</EM><SUB><EM>x</EM></SUB>-C netted fibers","originalKeyword":" Nb<EM>C</EM><SUB><EM>x</EM></SUB>-C netted fibers"},{"id":"96620a0a-f880-4c42-b1d8-058816efb0f2","keyword":" processing condition","originalKeyword":" processing condition"}],"language":"zh","publisherId":"1000-324X_1999_5_12","title":"NbC<SUB><EM>x</EM></SUB>-C三维网状纤维的制备","volume":"14","year":"1999"},{"abstractinfo":"以Pb粉,Te粉和PBi_2粉为原料,采用固相合成方法合成了掺杂PBi_2(0.03,0.05,0.1,0.3at%)N型PbTe合金,XRD分析表明,合金具有NaCl型面心立方结构.采用热压烧结法将PhTe合金粉末烧结成块体材料,运用XRD,SEM方法对材料的物相组成和形貌进行了表征,表明热压烧结后材料仍保持NaCl型面心立方结构,出现偏析现象,分为富Te相和富Pb相,其中富Pb相呈现片状.通过材料热电性能参数的测试,研究了20MPa下不同热压烧结温度,不同含量PhI_2掺杂对材料热电性能的影响,结果表明合理热压烧结温度对材料的热电性能提高起到关键作用,当PBi_2含量为0.1at%时,PbTe合金在350℃具有最高的功率因子2.48mW/(m·K~2).","authors":[{"authorName":"吴荣归","id":"f34ca6de-6150-4819-932c-33dff7a302e2","originalAuthorName":"吴荣归"},{"authorName":"李兴","id":"9f8ed987-5c22-4f29-b84c-f65f2ca34eb8","originalAuthorName":"李兴"},{"authorName":"张艳华","id":"04db04fd-9c69-43c2-a58d-54383395d68b","originalAuthorName":"张艳华"},{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"2ff89691-5c87-46d3-b855-0cc956ad5013","originalAuthorName":"徐桂英"}],"doi":"","fpage":"271","id":"6729ccae-6a92-4322-b841-f6892d19d172","issue":"2","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"5cc0055f-ac30-4c7f-8aa9-8603792584c8","keyword":"PbTe","originalKeyword":"PbTe"},{"id":"612bd1dd-7d35-426a-af53-58e89abbddf5","keyword":"PBI_2掺杂","originalKeyword":"PBI_2掺杂"},{"id":"d0fd1b27-a2cc-4a8a-b47d-73e527374126","keyword":"热压","originalKeyword":"热压"},{"id":"b8a09a98-b725-4630-ac00-2b051bb58af1","keyword":"热电性能","originalKeyword":"热电性能"}],"language":"zh","publisherId":"clkxygc201002026","title":"PbTe基合金的热压制备与热电性能","volume":"28","year":"2010"},{"abstractinfo":"分别以SbCl3和不同的硒源(SeO2、Se粉)为原料,采用水合肼(N2H4.H2O)为还原剂,用水热法在150℃下反应24 h后合成Sb2Se3纳米粉末.通过X射线粉末衍射(XRD)、透射电镜(TEM)、场发射电子扫描电镜(FESEM)以及高分辨透射电镜等分析方法对产物的物相成分和形貌等进行表征.结果表明,产物的结构为正交晶系的Sb2Se3纳米晶体,其微观形貌为一维纳米线结构.采用不同硒源合成产物的微观形貌基本相似,其中以SeO2作为硒源水热合成的Sb2Se3纳米线比以Se粉作为硒源合成的纳米线要更加窄而薄,而且纳米线尺寸比较均匀一致.纳米线晶体沿[001]方向生长,这与Sb2Se3独特的晶体结构有着密切的联系.","authors":[{"authorName":"张艳华","id":"80142a10-c4f9-462a-bab8-3a92221e46bf","originalAuthorName":"张艳华"},{"authorName":"韩菲","id":"f5ac70f1-87ff-47d3-9cd5-a7a4e7a8c9d8","originalAuthorName":"韩菲"},{"authorName":"王泽","id":"137756f5-18bb-4679-8a89-f31a6e290a60","originalAuthorName":"王泽"},{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"bb1137b9-70cd-4427-951b-90ff62883909","originalAuthorName":"徐桂英"}],"doi":"","fpage":"1820","id":"790f31e5-9852-49fe-b93d-e6f74d9b3578","issue":"10","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"2552e3d3-8ba9-48e9-819e-3e8f58fef352","keyword":"水热合成","originalKeyword":"水热合成"},{"id":"68be8044-08b1-4fa4-ad58-ecce19c33746","keyword":"Sb2Se3","originalKeyword":"Sb2Se3"},{"id":"7ad9b6dc-2ebd-4797-96f1-a567daddabf4","keyword":"纳米线","originalKeyword":"纳米线"}],"language":"zh","publisherId":"xyjsclygc201010029","title":"Sb2Se3纳米线的水热合成和表征","volume":"39","year":"2010"},{"abstractinfo":"讨论了热电材料研究与发展的最新方向,阐述了单体和梯度热电材料的基本理论和正在进行的研究热点及其所遵循的基本原则.","authors":[{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"fbe5d4a7-049e-4a5c-b2a3-496524191647","originalAuthorName":"徐桂英"},{"authorName":"葛昌纯","id":"d0f7e07d-654a-4147-8731-6db031c69833","originalAuthorName":"葛昌纯"}],"doi":"","fpage":"38","id":"7a2a7f83-d13a-4a5b-8575-1a2457ae7a8c","issue":"11","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"8eeecbb7-8b68-4364-a398-4362609c7980","keyword":"热电材料","originalKeyword":"热电材料"},{"id":"fd6b71c4-00ed-4702-91fe-03c3cf65322b","keyword":"研究","originalKeyword":"研究"},{"id":"69bdad99-b1f4-4ee8-a627-f38440a34cd2","keyword":"发展","originalKeyword":"发展"},{"id":"6d4f707f-f2af-4d7c-bbdc-e63dcab9c728","keyword":"方向","originalKeyword":"方向"}],"language":"zh","publisherId":"cldb200011015","title":"热电材料的研究和发展方向","volume":"14","year":"2000"},{"abstractinfo":"不烧Al2O3-C质耐火材料是针对高炉炉身下部的工作条件开发的一类新型耐火材料，水蒸气氧化是该部位内衬材料蚀损的主要原因之一.对该种耐火材料在水蒸气环境下的抗氧化性能进行了热力学分析，并进行了一系列的等温氧化性能实验.实验结果表明：该种铝碳耐火材料在高温下有保护型氧化的特征,其氧化后的抗折强度有所提高，在水蒸气中具有较好的抗氧化性能.此外，根据其氧化规律建立了不烧Al2O3-C质耐火材料的氧化动力学模型.","authors":[{"authorName":"程乃良","id":"442f9e11-58dd-45d3-8df6-9c16e97ef238","originalAuthorName":"程乃良"},{"authorName":"<span style=\"color:red\">徐</span><span style=\"color:red\">桂</span><span style=\"color:red\">英</span>","id":"579970e9-8f5e-439d-9bb7-f6975947797f","originalAuthorName":"徐桂英"},{"authorName":"杜鹤<span style=\"color:red\">桂</span>","id":"2903fe6b-76cb-4ea8-83d5-63ce17bf42d0","originalAuthorName":"杜鹤桂"},{"authorName":"崔泽南","id":"6e417492-7c36-479a-b8f4-513d930b17e9","originalAuthorName":"崔泽南"}],"doi":"10.3969/j.issn.1005-0299.2000.04.007","fpage":"30","id":"7b3d4d2c-abc7-457e-86ec-dccc08f2af6a","issue":"4","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"b751d82d-d1a8-44dc-8deb-a41a5564e121","keyword":"高炉","originalKeyword":"高炉"},{"id":"3cd594a3-68f1-4f73-8857-7ccd015a4986","keyword":"不烧Al2O3-C砖","originalKeyword":"不烧Al2O3-C砖"},{"id":"140f08b1-9630-4a5f-abf9-fd7178a5661d","keyword":"水蒸气","originalKeyword":"水蒸气"},{"id":"8f602d99-84b9-4dda-bcce-0a1cfd51cf9d","keyword":"氧化性能","originalKeyword":"氧化性能"}],"language":"zh","publisherId":"clkxygy200004007","title":"不烧Al2O3-C质耐火材料在水蒸汽中的抗氧化性能","volume":"8","year":"2000"}],"totalpage":33,"totalrecord":330}