{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"合成了14个未见文献报道的O-甲基-α-羟基烃基膦酸酯单金属盐,通过IR、1H NMR和元素分析测试技术确证了它们的结构,并测定了它们的<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>.生物测试结果表明,该类化合物对小麦和黄瓜具有不同程度的<span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>,其中化合物Ⅰ k在10μg/g剂量下对黄瓜子根显示了较高的促进<span style=\"color:red\">活性</span>.","authors":[{"authorName":"廖桂红","id":"1cde78b3-31bf-45eb-89a7-03ee21f88f07","originalAuthorName":"廖桂红"},{"authorName":"贺红武","id":"18c5d829-cd9e-4062-87e1-2b7d767c8153","originalAuthorName":"贺红武"}],"doi":"10.3969/j.issn.1000-0518.2005.09.002","fpage":"933","id":"0aa06b69-a65b-44f7-a2bb-b88df98a88ca","issue":"9","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"3a22becb-28d4-4f21-98a6-a9cccdc92ce0","keyword":"α-羟基烷基膦酸酯单金属盐","originalKeyword":"α-羟基烷基膦酸酯单金属盐"},{"id":"dfe80f18-376e-4317-8ace-aa6468f64a0c","keyword":"合成","originalKeyword":"合成"},{"id":"ff235587-3aa8-4c9d-ab85-c71e03120ab6","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","originalKeyword":"植物生长调节活性"}],"language":"zh","publisherId":"yyhx200509002","title":"O-甲基-α-羟基烃基膦酸酯单金属盐的合成及<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","volume":"22","year":"2005"},{"abstractinfo":"通过4-氨基苯氧丙酸乙酯与相应的取代芳香醛类化合物进行缩合反应得到了11个未见报道的α-{[4-(取代苯基亚甲基)亚氨基]苯氧基}丙酸乙酯类目标化合物,用UV、IR、1H NMR和元素分析测试技术对其进行了表征.探讨了芳环上取代基对反应收率的影响,结果发现具有吸电子取代基的对硝基苯甲醛给出93%的最高反应产率;而有供电子取代基的对甲基苯甲醛给出54%的最低反应产率.初步生物<span style=\"color:red\">活性</span>测试证明,此类席夫碱化合物具有一定的<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>;化合物6b和6f具有52%和55%的促黄瓜子叶生根<span style=\"color:red\">活性</span>,化合物6j具有75%的黄瓜子叶生根抑制<span style=\"color:red\">活性</span>;化合物6h具有53%的<span style=\"color:red\">生长</span>素<span style=\"color:red\">活性</span>;化合物6b具有51%的细胞分裂素<span style=\"color:red\">活性</span>.","authors":[{"authorName":"刘国华","id":"fd3881ef-2123-4451-ab40-c4bc0a386b3a","originalAuthorName":"刘国华"},{"authorName":"余焓","id":"04cb624f-4184-4434-9832-ff7282f40ae2","originalAuthorName":"余焓"},{"authorName":"姚美","id":"f1bbae70-62c2-40e4-8553-3b8ce62b7b33","originalAuthorName":"姚美"},{"authorName":"方海斌","id":"7d894b98-b26b-4c94-a28a-62d717671964","originalAuthorName":"方海斌"}],"doi":"10.3969/j.issn.1000-0518.2007.02.008","fpage":"152","id":"97fbbeb1-7950-476e-a991-7e1fdac37291","issue":"2","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"4f7d2b09-8b17-4051-8939-7ea150181701","keyword":"席夫碱","originalKeyword":"席夫碱"},{"id":"d8f03f44-b0f8-4f56-9166-bc3c134f01f5","keyword":"苯氧丙酸酯","originalKeyword":"苯氧丙酸酯"},{"id":"c48c2aa3-9f0d-469e-88e5-1b7551fbd769","keyword":"合成","originalKeyword":"合成"},{"id":"a85f8db1-a1bf-4e50-8fe4-ab0a84c960f9","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","originalKeyword":"植物生长调节活性"}],"language":"zh","publisherId":"yyhx200702008","title":"α-{[4-(取代苯基亚甲基)亚氨基]苯氧基}丙酸乙酯的合成及<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","volume":"24","year":"2007"},{"abstractinfo":"合成了9种新的3-(2-氯-4-三氟甲基苯氧基)-N-杂环基苯甲酰胺(4),通过红外光谱、核磁共振氢谱、质谱和元素分析对该系列化合物进行了结构确认. 该类化合物对小麦和黄瓜具有不同程度的<span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>,其中化合物4e在10 μg/g剂量下对黄瓜<span style=\"color:red\">生长</span>显示了较高的促进<span style=\"color:red\">活性</span>.","authors":[{"authorName":"彭浩","id":"0a14a45d-d880-4ff6-b219-7e1a4004e44a","originalAuthorName":"彭浩"},{"authorName":"宁丽红","id":"03bb45d1-703d-4716-a8c6-68d2302b408e","originalAuthorName":"宁丽红"},{"authorName":"涂海洋","id":"ccf01984-db68-4653-8474-507127495b57","originalAuthorName":"涂海洋"},{"authorName":"贺红武","id":"81a59a6d-ce0f-4cc0-bb71-2f1557206d28","originalAuthorName":"贺红武"}],"doi":"10.3969/j.issn.1000-0518.2003.07.007","fpage":"643","id":"4d3d5eef-c050-4717-9314-23aadb063e3a","issue":"7","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"5188829a-f590-4845-af85-79776f321969","keyword":"苯甲酰胺","originalKeyword":"苯甲酰胺"},{"id":"60cf23c9-d01b-44f1-8d1c-979e7bd801b0","keyword":"二苯醚","originalKeyword":"二苯醚"},{"id":"b3ce34a4-7877-4ec0-964d-4b5bcaf0a086","keyword":"合成","originalKeyword":"合成"},{"id":"f19350dd-bd48-443e-9539-099fe3931159","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","originalKeyword":"植物生长调节活性"}],"language":"zh","publisherId":"yyhx200307007","title":"3-(2-氯-4-三氟甲基苯氧基)-N-杂环基苯甲酰胺的合成与<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","volume":"20","year":"2003"},{"abstractinfo":"以芴、水杨醛和氨基芳基硫脲为原料合成了一系列新型芴三偶氮基水杨醛缩氨基芳基硫脲衍生物,其结构经IR、~1H NMR、MS和元素分析测试技术确证.经平皿油菜生根实验表明,该类化合物在低浓度下对油菜生根显示促进作用,高浓度下促进作用小或显示抑制作用,对油菜生根的<span style=\"color:red\">调节</span>作用与硫脲的苯取代基上的取代基性质有关.","authors":[{"authorName":"冯驸","id":"29bfb31e-e9e5-4b22-9577-f2c7dd595383","originalAuthorName":"冯驸"},{"authorName":"胡卫兵","id":"e013b6a8-9941-4fab-ab1c-9dc1c591c93a","originalAuthorName":"胡卫兵"},{"authorName":"刘红霞","id":"c5fd7462-82ef-46fe-b4e0-b68d4ca71969","originalAuthorName":"刘红霞"},{"authorName":"聂响亮","id":"e3216e68-b902-497d-bae6-a333f80a2fe3","originalAuthorName":"聂响亮"},{"authorName":"余爱农","id":"c86c4ad3-a712-472c-b230-17c8e8bc6ac7","originalAuthorName":"余爱农"}],"doi":"10.3724/SP.J.1095.2010.90090","fpage":"169","id":"faafd3f3-0f90-498f-90f0-49af06378d23","issue":"2","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"ddfee7fd-b461-4c42-a32b-a87bfbcf924a","keyword":"三氨基芴","originalKeyword":"三氨基芴"},{"id":"82f403dd-c88e-4eea-a565-0ec3842b0ef0","keyword":"水杨醛","originalKeyword":"水杨醛"},{"id":"f9204426-2e79-4ab0-9d63-47a8dce34b93","keyword":"三偶氮基水杨醛缩氨基芳基硫脲衍生物","originalKeyword":"三偶氮基水杨醛缩氨基芳基硫脲衍生物"},{"id":"3f290b47-8c99-41dc-9e03-7d8c23427c6e","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","originalKeyword":"植物生长调节活性"},{"id":"c7cb81b9-291d-4a7b-acbd-0e34e85d6450","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"yyhx201002010","title":"芴三偶氮基水杨醛缩氨基芳基硫脲合成及其<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>作用","volume":"27","year":"2010"},{"abstractinfo":"合成了14个具有6-氯-3-吡啶甲基取代的硫脲,其结构经IR、1H NMR、元素分析确证. 初步杀虫及<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>测试表明,所有化合物对黄瓜芽、水稻芽和根的<span style=\"color:red\">生长</span>有很好的促进作用,其中化合物D13对家蝇的校正死亡率达96%.","authors":[{"authorName":"阎争亮","id":"698023b1-024f-4545-a35e-d32ad3cc825e","originalAuthorName":"阎争亮"},{"authorName":"司宗兴","id":"66d649b9-7d6d-4d7e-b1b2-1de8c98c161b","originalAuthorName":"司宗兴"}],"doi":"10.3969/j.issn.1000-0518.2001.08.015","fpage":"651","id":"48a9cea9-0c9e-494c-b416-d476b656971d","issue":"8","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"879f9fb7-f143-4340-8903-e509e2e51e2c","keyword":"氯-氯甲基吡啶","originalKeyword":"氯-氯甲基吡啶"},{"id":"22a9b2e8-40e1-4242-b4ad-40e988e8e232","keyword":"硫脲","originalKeyword":"硫脲"},{"id":"99026a8d-c211-41fa-a494-6ecaefff6c14","keyword":"杀虫","originalKeyword":"杀虫"},{"id":"c355e2fc-6646-4507-9d78-16c9d653ad14","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","originalKeyword":"植物生长调节活性"}],"language":"zh","publisherId":"yyhx200108015","title":"6-氯-3-吡啶甲基取代硫脲化合物的合成与生物<span style=\"color:red\">活性</span>","volume":"18","year":"2001"},{"abstractinfo":"在25℃,V(CF3COOH):V(CH3COOH)=1:9的反应介质中1-萘甲醚被Cl-氯化,O2及催化量的NO+BF-4为氧化剂,合成了8种标题化合物6a～6h,产率为43.2%～56.5%,采用元素分析、IR、1H NMR和MS测试技术确证了它们的结构.初步考察了目标化合物的<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>,大多数化合物显示出较好的<span style=\"color:red\">生长</span>素类的激素作用,质量浓度为0.1 g/L时,化合物6f对小麦牙鞘的抑制率为-20.3%,促进率为2.58%,而化合物6h则分别为-15.3%和2.04%.比较了目标化合物6a～6h与萘氧乙酸及相应的α-羟基膦酸酯的<span style=\"color:red\">植物</span><span style=\"color:red\">调节</span><span style=\"color:red\">活性</span>,目标化合物6a～6h在质量浓度为0.1 g/L时,对小麦牙鞘的抑制率较相应的α-羟基膦酸酯高出2.3%～4.5%,促进率高出0.24%～0.58%.比较了氯原子引入萘环后目标化合物生物<span style=\"color:red\">活性</span>的变化,氯原子的引入有利于提高母体化合物的<span style=\"color:red\">植物</span><span style=\"color:red\">调节</span><span style=\"color:red\">活性</span>.","authors":[{"authorName":"刘绪峰","id":"0c0335c8-9e5b-4376-b327-83d969670573","originalAuthorName":"刘绪峰"},{"authorName":"王运","id":"ceb2d2bc-7ef9-4ec1-9657-b21b725d7ff4","originalAuthorName":"王运"},{"authorName":"程珍贤","id":"cebfbd2c-39b7-4f94-8843-7f683fdfec90","originalAuthorName":"程珍贤"},{"authorName":"贺红武","id":"1747c872-9027-4b6a-bb4e-f503fbb2e445","originalAuthorName":"贺红武"}],"doi":"10.3969/j.issn.1000-0518.2005.01.009","fpage":"40","id":"2cf6596d-9132-4f0a-b897-646aad2e2871","issue":"1","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"6a5a8fc5-e7fa-46ba-922a-a8e73b41bf1a","keyword":"膦酸酯","originalKeyword":"膦酸酯"},{"id":"a3d4c7ad-590a-4f0a-ae21-c57a2defabca","keyword":"氯萘酚","originalKeyword":"氯萘酚"},{"id":"bb70738e-3d3c-4327-b8c8-f40b1df5ef1f","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","originalKeyword":"植物生长调节活性"}],"language":"zh","publisherId":"yyhx200501009","title":"α-(4-氯-1-萘氧基乙酰氧基)烃基膦酸酯的合成与植调<span style=\"color:red\">活性</span>","volume":"22","year":"2005"},{"abstractinfo":"首次合成了二茂铁基-1,3,4-三唑Schiff碱衍生物(5a ～5e),利用IR、1 H NMR和HRMS等手段对其进行了结构表征.用黄瓜子叶生根法以及小麦芽鞘法,分别测试化合物的细胞分裂素<span style=\"color:red\">活性</span>和<span style=\"color:red\">生长</span>素<span style=\"color:red\">活性</span>.结果表明,在10 mg/L浓度下,有4个化合物的子叶生根促进作用为46.9％～73.6％,比对参照物的细胞分裂<span style=\"color:red\">活性</span>更高,但<span style=\"color:red\">生长</span>素<span style=\"color:red\">活性</span>不明显,化合物5c仅提高25％;化合物的除草<span style=\"color:red\">活性</span>在68％～72％之间.以石墨烯修饰的玻碳电极为工作电极,在Britton-Robison缓冲溶液中,研究了目标化合物电化学行为.结果表明,在pH值为2或3的溶液中,合成目标化合物具有良好的氧化还原可逆性,氧化峰电流对数(lg Ipc)与扫描速度对数(lgv)、浓度对数(lg c)均呈现良好线性关系,目标化合物(5a～5d)的电子转移过程均受吸附-扩散混合控制,该类化合物的循环伏安法最低检出限为10-5 moL/L.","authors":[{"authorName":"朱长安","id":"da25dc21-f8cc-4121-9a60-b9b329a93dc7","originalAuthorName":"朱长安"},{"authorName":"武飞宇","id":"a3558149-314d-4e30-8950-9cd5794728dc","originalAuthorName":"武飞宇"},{"authorName":"王雪","id":"5ffd7193-472a-44fd-a088-890a9ff7f98c","originalAuthorName":"王雪"},{"authorName":"高丽娜","id":"e3d6e010-dadc-40b4-9506-4f8dda32c4c8","originalAuthorName":"高丽娜"},{"authorName":"翁前锋","id":"173758d6-eb30-46a3-b8c4-dd298e5a7cfb","originalAuthorName":"翁前锋"},{"authorName":"石丽","id":"078d2f84-45ad-4b31-84b9-cb8a26f178d6","originalAuthorName":"石丽"},{"authorName":"张成路","id":"e520e33f-c31b-4ca8-9734-2576b8c781fa","originalAuthorName":"张成路"}],"doi":"10.3724/SP.J.1095.2014.30294","fpage":"455","id":"9b04433d-70c2-4748-ad56-1479c07d2b02","issue":"4","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"026e9af8-ae76-4ee4-9a71-c7c3cfb934e3","keyword":"二茂铁基均三唑","originalKeyword":"二茂铁基均三唑"},{"id":"81dfd943-0d09-4518-ae50-cc971911e440","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","originalKeyword":"植物生长调节活性"},{"id":"c219e170-55f0-45b3-b766-c31f1c52f1b4","keyword":"除草<span style=\"color:red\">活性</span>","originalKeyword":"除草活性"},{"id":"97843da3-4d6e-4030-b19f-2000db255b60","keyword":"循环伏安法","originalKeyword":"循环伏安法"}],"language":"zh","publisherId":"yyhx201404014","title":"二茂铁基1,3,4-三唑席夫碱衍生物合成及生物<span style=\"color:red\">活性</span>和电化学性质","volume":"31","year":"2014"},{"abstractinfo":"用聚乙二醇400为相转移催化剂,由3,5-二甲基苯酚和氯乙酸合成了3,5-二甲基苯氧基乙酸(DMBC),用水热法将它与氯化铜合成了配合物Cu(DMBC)2(H2O)2,通过元素分析、红外光谱对其进行了表征；采用X射线单晶衍射法测定了其晶体和分子结构.其晶体属单斜晶系,P21/c空间群.晶胞参数:a=1.526(2) nm,b=0.7092(11) num,c=1.0942(17) nm,β=104.567(15)°,V=1.146(3) nm3,Z=2,F(000) =478.在分子中,Cu(Ⅱ)分别与2个配体的羧基氧原子和2个水分子配位,中心离子构成稍微变形的平面四边形配位构型.分之间通过氢键和π-π相互作用自组装成稳定的二维层状超分子.利用Gauss03程序,在B3LYP/6-31G水平上对标题化合物进行了量化计算,给出了配合物分子中各原子的净电荷布居,计算结果与测定结果吻合.测试了该配合物对油菜籽发芽<span style=\"color:red\">生长</span>促进<span style=\"color:red\">活性</span>和抑菌作用.CCDC:909139","authors":[{"authorName":"张有明","id":"ec4d5893-3aa1-4674-ba29-dd4a4b6d716a","originalAuthorName":"张有明"},{"authorName":"谢永强","id":"5a0fab64-0b9c-43b0-b91d-db002e356781","originalAuthorName":"谢永强"},{"authorName":"姚虹","id":"0d5130d0-f4da-41e7-b3f3-97e9dcbf9a5c","originalAuthorName":"姚虹"},{"authorName":"耿志远","id":"5fed01bd-08e0-4ad6-8942-d4f7e9c891f1","originalAuthorName":"耿志远"},{"authorName":"刘江龙","id":"8f43d930-ea9a-4a17-af8c-9d3357f11868","originalAuthorName":"刘江龙"},{"authorName":"贺晓旋","id":"19ad70b2-d4d8-4fb6-9152-f46291be8e80","originalAuthorName":"贺晓旋"},{"authorName":"魏太保","id":"99beadb8-e0b7-46ba-8aab-6cd1995af881","originalAuthorName":"魏太保"}],"doi":"10.3724/SP.J.1095.2013.20512","fpage":"1010","id":"6f4a1e64-056d-47c4-9bdd-b03be5cde4cc","issue":"9","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"5a82c87d-8234-482f-b9c0-1c0203eb8e8d","keyword":"二甲基芳氧乙酸","originalKeyword":"二甲基芳氧乙酸"},{"id":"c39252cf-016f-4dcd-a536-2d8178592f68","keyword":"Cu(Ⅱ)配合物","originalKeyword":"Cu(Ⅱ)配合物"},{"id":"c372e50d-b770-4146-bbbd-8af7b756105d","keyword":"晶体结构","originalKeyword":"晶体结构"},{"id":"470bcb13-213c-4900-98e8-c93c36bc0976","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span><span style=\"color:red\">活性</span>","originalKeyword":"植物生长调节活性"},{"id":"1909bc87-7c45-47a9-82cf-9e294368d72b","keyword":"抑菌<span style=\"color:red\">活性</span>","originalKeyword":"抑菌活性"},{"id":"108f213f-6a59-47be-a6cf-5b0257a25594","keyword":"量化计算","originalKeyword":"量化计算"}],"language":"zh","publisherId":"yyhx201309006","title":"Cu(DMBC)2(H2O)2(DMBC:3,5-二甲基苯氧基乙酸)配合物层状超分子的水热合成、结构及生物<span style=\"color:red\">活性</span>","volume":"30","year":"2013"},{"abstractinfo":"建立了同时测定果蔬中11种外源<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂的超高效液相色谱-串联质谱方法.果蔬样品经酸性乙腈-乙酸铵溶液,超声波辅助提取, ProElut NH2填料净化后直接进样分析,采用正负离子多反应监测( MRM)模式,外标法定量.结果表明,在优化后的提取方法、色谱和质谱条件下,11种外源<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂在0.003—10 mg·L-1范围内线性关系良好,相关系数( R2 )大于0.999,检出限为0.001—0.01 mg·kg-1 ,平均回收率范围为78.4%—100.1%,相对标准偏差(RSD)范围为2.5%—6.6%.该方法快速简便、灵敏度高、净化效果好,适合果蔬中外源<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂的快速测定.","authors":[{"authorName":"林涛","id":"81155c81-6cd3-4c9b-96b8-0ead22b37a0c","originalAuthorName":"林涛"},{"authorName":"黎其万","id":"9df70eb7-76a7-4f04-a1cc-0c35366395fe","originalAuthorName":"黎其万"},{"authorName":"刘宏程","id":"0135afba-a9ad-4999-8e70-67e7d1cc9090","originalAuthorName":"刘宏程"},{"authorName":"樊建麟","id":"dd9d9e90-a5f8-4099-91eb-009e3bd7c334","originalAuthorName":"樊建麟"},{"authorName":"杨东顺","id":"5ac81bef-6201-41b0-ae87-2fd7c4200128","originalAuthorName":"杨东顺"},{"authorName":"李彦刚","id":"337d7ddc-d826-4855-ac76-32cdc6138dcb","originalAuthorName":"李彦刚"}],"doi":"10.7524/j.issn.0254-6108.2016.01.2015090703","fpage":"57","id":"8df2153e-ae9c-473f-8aa4-f2178e8ed189","issue":"1","journal":{"abbrevTitle":"HJHX","coverImgSrc":"journal/img/cover/HJHX.jpg","id":"43","issnPpub":"0254-6108","publisherId":"HJHX","title":"环境化学   "},"keywords":[{"id":"01f9a478-6351-4207-b625-e51478bcbab4","keyword":"水果","originalKeyword":"水果"},{"id":"d3cfee03-c669-4745-b8be-293fdc90d14b","keyword":"蔬菜","originalKeyword":"蔬菜"},{"id":"58959a16-e555-4124-987a-496a68adff08","keyword":"外源<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂","originalKeyword":"外源植物生长调节剂"},{"id":"6f77908a-6f35-4e6f-8ecb-9cd28abab224","keyword":"提取","originalKeyword":"提取"},{"id":"779da2d4-3f13-4270-919a-9abbec57a165","keyword":"测定","originalKeyword":"测定"}],"language":"zh","publisherId":"hjhx201601008","title":"果蔬中外源<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂的快速提取和测定","volume":"35","year":"2016"},{"abstractinfo":"建立了用于测定瓜果中多效唑、氯吡脲、异戊烯腺嘌呤和6-苄氨基嘌呤等4种<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂残留量的高效液相色谱-串联质谱分析方法.样品用乙腈提取,经阳离子交换固相萃取柱净化后,用Agilent XDB-C18色谱柱分离,以5 mmol/L乙酸铵溶液和含0.1％(体积分数)甲酸的乙腈溶液为流动相进行梯度洗脱.质谱采用电喷雾正离子(ESI+)模式电离,多反应监测(MRM)模式检测,基质匹配标准溶液外标法定量.4种<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂在各自的范围内线性很好,相关系数均大于0.999.选取了黄瓜和苹果作为代表性基质进行添加回收试验,定量限(信噪比大于l0)在0.04 ～1.35 μg/kg之间,检出限(信噪比大于3)在0.01～0.41 μg/kg之间,在3个添加水平下回收率范围为81.0％～93.3％,相对标准偏差(RSDs)为3.5％ ～ 9.5％.该方法的灵敏度、准确度和精密度均符合农药残留测定的技术要求,适用于瓜果中这4种<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂残留量的检测.","authors":[{"authorName":"牟艳莉","id":"9d0d7566-1fe7-42d2-ade2-f7fc120ce163","originalAuthorName":"牟艳莉"},{"authorName":"郭德华","id":"5d2da785-c532-46ab-802c-73b24f5d3c8c","originalAuthorName":"郭德华"},{"authorName":"丁卓平","id":"1398e39a-8411-40f5-a6ab-81c336c7ed31","originalAuthorName":"丁卓平"}],"doi":"10.3724/SP.J.1123.2013.06003","fpage":"1016","id":"44b69947-2392-40e7-b2fd-ad8fd4cb7fac","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"5fa3cf04-5063-4e4c-8bde-a077c06a7b74","keyword":"固相萃取","originalKeyword":"固相萃取"},{"id":"f6247d91-72dc-4a00-a9ff-e77059a39947","keyword":"高效液相色谱-串联质谱","originalKeyword":"高效液相色谱-串联质谱"},{"id":"e14fce01-4df1-4a8f-a15b-0bbd86a43417","keyword":"<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂","originalKeyword":"植物生长调节剂"},{"id":"98363874-0bd6-46fa-bd19-f6d5374d7fba","keyword":"瓜果","originalKeyword":"瓜果"},{"id":"8eef14b3-9467-408d-a786-9d02198028c4","keyword":"残留","originalKeyword":"残留"}],"language":"zh","publisherId":"sp201310016","title":"高效液相色谱-串联质谱法检测瓜果中的4种<span style=\"color:red\">植物</span><span style=\"color:red\">生长调节</span>剂的残留量","volume":"31","year":"2013"}],"totalpage":2644,"totalrecord":26438}