{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用SEM，EPMA和热震方法，研究了CeO2添加剂对等离子喷涂ZrO2涂层抗热震性的影响。结果表明：当CeO2由0增加到9.0%(质量分数,下同)时，涂层的抗热震起裂次数和失效次数分别由32次和46次增加到76次和105次；继续增加CeO2，涂层的抗热震性能急剧下降。ZrO2+9.0%CeO2涂层在热循环中形成的网状微裂纹，不仅可降低涂层中的应力，也可提高涂层开裂的临界温差，从而可改善其抗热震性能。","authors":[{"authorName":"唐建成","id":"86c2a777-fcf0-41b6-9620-9cd2a2859e51","originalAuthorName":"唐建成"},{"authorName":"<span style=\"color:red\">邵</span><span style=\"color:red\">德</span><span style=\"color:red\">春</span>","id":"3a69c63e-c410-4f2c-a125-7904f760819b","originalAuthorName":"邵德春"},{"authorName":"郭面焕","id":"c944e2fe-c942-480f-b5b2-3ef91b675d17","originalAuthorName":"郭面焕"},{"authorName":"黄伯云","id":"00520a39-e076-47a4-bf65-be1b77faaea9","originalAuthorName":"黄伯云"},{"authorName":"周科朝","id":"0b1af545-c465-4e49-ac84-6a149413d5ce","originalAuthorName":"周科朝"}],"doi":"","fpage":"69","id":"de901fcd-908d-43f5-9a92-5e8d83b7dc46","issue":"1","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"17e8ed5d-54ae-42d5-9abf-e5e8c8623ba0","keyword":"CeO2添加剂","originalKeyword":"CeO2添加剂"},{"id":"eab40a1b-2d0a-4c7e-bb4f-7b29e60a4672","keyword":"抗热震性","originalKeyword":"抗热震性"},{"id":"1b631efb-fc43-46c1-bf89-67cc65892987","keyword":"微裂纹","originalKeyword":"微裂纹"},{"id":"fb4c047e-55f4-4075-83be-31ba671df110","keyword":"等离子喷涂","originalKeyword":"等离子喷涂"},{"id":"89080957-2005-4404-a0c8-3d545ecf0332","keyword":"ZrO2","originalKeyword":"ZrO2"}],"language":"zh","publisherId":"xyjsclygc200101018","title":"CeO2添加剂对等离子喷涂ZrO2涂层抗热震性的影响","volume":"30","year":"2001"},{"abstractinfo":"采用等离子喷涂方法制备Al2O3陶瓷涂层,研究了稀土对涂层组织及耐蚀性的影响.结果表明,在喷涂粉末中添加适当的稀土硅铁合金不仅可以改变涂层显微组织、减少和消除层状结构,而且显著提高了涂层的耐蚀性.","authors":[{"authorName":"李淑华","id":"80027b16-a06e-4981-adb7-47b7ff003395","originalAuthorName":"李淑华"},{"authorName":"刘建敏","id":"6f374ba3-c75d-4a3e-b4f4-c8ae43dbcfe3","originalAuthorName":"刘建敏"},{"authorName":"<span style=\"color:red\">邵</span><span style=\"color:red\">德</span><span style=\"color:red\">春</span>","id":"a163b52a-b9ed-4ca8-9fb3-4526a79e1b49","originalAuthorName":"邵德春"}],"doi":"10.3969/j.issn.1004-0277.1999.03.011","fpage":"37","id":"0ea0abe7-a2af-4c30-9df7-4ec1835734b7","issue":"3","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"3b7d37e5-a533-474c-8ecd-dc5d73927a7d","keyword":"等离子喷涂","originalKeyword":"等离子喷涂"},{"id":"2a42dfaf-ca24-434a-948d-ce30b24970bc","keyword":"氧化铝","originalKeyword":"氧化铝"},{"id":"990793d7-ba8b-441a-9d39-5600dfe2a2e8","keyword":"稀土","originalKeyword":"稀土"},{"id":"52c51e9b-059a-4a36-aae0-1fea59b3fac0","keyword":"抗腐蚀性","originalKeyword":"抗腐蚀性"}],"language":"zh","publisherId":"xitu199903011","title":"稀土对Al2O3陶瓷涂层组织及性能的影响","volume":"20","year":"1999"},{"abstractinfo":"采用Chiralpak IC手性柱(250 mm×4.6 mm,5 μm),建立了正相高效液相色谱测定板蓝根中表告依<span style=\"color:red\">春</span>(R-告依<span style=\"color:red\">春</span>)和告依<span style=\"color:red\">春</span>(S-告依<span style=\"color:red\">春</span>)含量的方法.考察了流动相组成、流速和柱温对分离度的影响.经优化后的实验条件:以正己烷-异丙醇(体积比为90∶10)为流动相,流速为0.8 mL/min;检测波长为245 nm,柱温为20 ℃.在此优化条件下,表告依<span style=\"color:red\">春</span>和告依春分离度为3.4,检出限为2.0 mg/L,在0.02～2.0 g/L 范围内有良好的线性关系,平均回收率为101% ,相对标准偏差(RSD)小于3.0%(n=6).本方法可将具有抗病毒活性的表告依<span style=\"color:red\">春</span>与其对映体告依<span style=\"color:red\">春</span>基线分离并测定,专属性强,能有效控制板蓝根的质量.","authors":[{"authorName":"聂黎行","id":"fee7f0b1-4bfd-4c4e-9d65-d7f03c2a918a","originalAuthorName":"聂黎行"},{"authorName":"王钢力","id":"ee281225-e77f-4477-a486-a098ca91b1db","originalAuthorName":"王钢力"},{"authorName":"戴忠","id":"813e1426-d061-4e41-9723-d75cfa16968e","originalAuthorName":"戴忠"},{"authorName":"林瑞超","id":"3034f33a-eaf2-4665-8751-f5ef70c65379","originalAuthorName":"林瑞超"}],"doi":"10.3724/SP.J.1123.2010.01001","fpage":"1001","id":"32355b8f-ccce-4726-b210-eaacc0917986","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"5c41c71f-d053-43ba-8aa9-32ad96d3cca4","keyword":"手性高效液相色谱法","originalKeyword":"手性高效液相色谱法"},{"id":"e26a591e-56ec-4bb4-acfd-5d5f7ad919ea","keyword":"表告依<span style=\"color:red\">春</span>(R-告依<span style=\"color:red\">春</span>)","originalKeyword":"表告依春(R-告依春)"},{"id":"1e32ab35-876b-46d9-9898-47fb5c40d701","keyword":"告依<span style=\"color:red\">春</span>(S-告依<span style=\"color:red\">春</span>)","originalKeyword":"告依春(S-告依春)"},{"id":"8c1b4600-8fac-47f6-98f6-6670e2a0daa9","keyword":"板蓝根","originalKeyword":"板蓝根"}],"language":"zh","publisherId":"sp201010018","title":"手性高效液相色谱法测定板蓝根中表告依<span style=\"color:red\">春</span>和告依<span style=\"color:red\">春</span>含量","volume":"28","year":"2010"},{"abstractinfo":"2012年2月22日是两院院士<span style=\"color:red\">邵</span>象华先生百岁华诞的大喜日子,2月21日上午,中国钢研科技集团有限公司为<span style=\"color:red\">邵</span>象华院士百岁华诞举办了隆重的座谈会。","authors":[],"doi":"","fpage":"16","id":"b91bfe95-42b7-41e4-8ed9-e5773f29f027","issue":"3","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"d2105c24-f208-4b24-8b19-bf467d2b0a85","keyword":"＂庆祝<span style=\"color:red\">邵</span>象华院士百岁华诞座谈会＂","originalKeyword":"＂庆祝邵象华院士百岁华诞座谈会＂"},{"id":"df4761b4-1374-4fcd-8cf4-327714600128","keyword":"钢铁工业","originalKeyword":"钢铁工业"},{"id":"8a2fcb21-b70e-4106-96cc-c707c039244c","keyword":"科技工作者","originalKeyword":"科技工作者"},{"id":"f5805ea9-8437-439d-84c2-6d0f81500ac2","keyword":"学术作风","originalKeyword":"学术作风"}],"language":"zh","publisherId":"gtyjxb201203004","title":"“庆祝<span style=\"color:red\">邵</span>象华院士百岁华诞座谈会”隆重召开","volume":"24","year":"2012"},{"abstractinfo":"2012年2月22日是两院院士<span style=\"color:red\">邵</span>象华先生百岁华诞的大喜日子,2月21日上午,中国钢研科技集团有限公司为<span style=\"color:red\">邵</span>象华院士百岁华诞举办了隆重的座谈会。座谈会会场一幅以长城和中国钢铁工业为背景的巨型彩色喷绘画卷蕴喻了<span style=\"color:red\">邵</span>象华院士的成长经历和学术贡献。座谈会高朋满座,群贤毕集。中国材料界学术泰斗,国家最高科学技术奖获得者师昌绪院士、中国工程院名誉院长徐匡迪院士、中国科学院副院长李静海院士、","authors":[],"doi":"","fpage":"75","id":"90f1fcfb-cc62-4b18-b287-ba2d3d459b74","issue":"3","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"e830a8e9-3b92-458b-8ecc-4192704ffee5","keyword":"师昌绪院士","originalKeyword":"师昌绪院士"},{"id":"cf99cc15-ae16-4654-a7c2-007b2e85fa03","keyword":"国家最高科学技术奖","originalKeyword":"国家最高科学技术奖"},{"id":"820407b1-47c6-4c07-b8b3-ebce8bc4934f","keyword":"中国工程院","originalKeyword":"中国工程院"},{"id":"17200f26-910f-4bce-af83-beea7ccf79a0","keyword":"学术贡献","originalKeyword":"学术贡献"},{"id":"6982139f-7d3d-4126-b3af-06e5e7ef8525","keyword":"钢铁工业","originalKeyword":"钢铁工业"},{"id":"7416ace7-3590-450e-95df-94de60ab2d99","keyword":"中国科学院","originalKeyword":"中国科学院"},{"id":"c3552b08-e8da-4b85-965f-db3b43777054","keyword":"成长经历","originalKeyword":"成长经历"},{"id":"8c26f9db-5cc3-445f-8333-6f6089c2b1ca","keyword":"副院长","originalKeyword":"副院长"}],"language":"zh","publisherId":"gt201203017","title":"“庆祝<span style=\"color:red\">邵</span>象华院士百岁华诞座谈会”隆重召开","volume":"47","year":"2012"},{"abstractinfo":"对<span style=\"color:red\">德</span>马克连铸机存在的问题进行分析,并针对存在问题进行技术改造,收到较好的效果,使铸坯质量和产量得到明显的提高.","authors":[{"authorName":"姜振强","id":"09c1d70f-8c55-47ae-ba0f-c0e77f57b958","originalAuthorName":"姜振强"},{"authorName":"郭广文","id":"a17f5c61-3ee8-48b8-a907-1897fc12daaf","originalAuthorName":"郭广文"},{"authorName":"陈树林","id":"6d5932f7-228e-47bd-8e6d-5b42150a9407","originalAuthorName":"陈树林"}],"doi":"10.3969/j.issn.1005-4006.2003.05.005","fpage":"12","id":"5777ebc2-0764-44e5-8805-c7c4c71980c2","issue":"5","journal":{"abbrevTitle":"LZ","coverImgSrc":"journal/img/cover/LZ.jpg","id":"52","issnPpub":"1005-4006","publisherId":"LZ","title":"连铸"},"keywords":[{"id":"21ad4ab9-9ba1-467e-b781-12be7452c174","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"lz200305005","title":"<span style=\"color:red\">德</span>马克连铸机系统改造","volume":"","year":"2003"},{"abstractinfo":"利用铱催化高碘酸钾氧化丽<span style=\"color:red\">春</span>红G(PG)的褪色反应,建立了测定痕量铱的催化动力学光度法.在硫酸介质和90℃加热15min的条件下,于500nm波长处,采用固定时间法测定丽<span style=\"color:red\">春</span>红G吸收值的降低.Ir(Ⅳ)的浓度在0～1.0μg/25mL范围内与催化反应的速率有良好的线性关系,检出限为1 81 ×10 mg/mL.对0.3μg/25mLIr(Ⅳ)测定的相对标准偏差为1.61%(n=11).体系至少稳定3.5h.考察了40多种共存离子的影响,大多数常见离子不干扰,方法有较好的选择性.催化反应对Ir(Ⅳ)和丽<span style=\"color:red\">春</span>红G均为一级反应,催化反应的表观活化能为103.66kJ/mol.用于冶金产品及岩矿中铱的测定,结果与推荐值十分吻合.","authors":[{"authorName":"侯能邦","id":"92c62fdf-fec8-4163-aad2-9ed54b7fdce6","originalAuthorName":"侯能邦"},{"authorName":"李祖碧","id":"c4dacfbe-4824-4cbe-a844-91a76be4f69c","originalAuthorName":"李祖碧"},{"authorName":"李崇宁","id":"f7a10f8c-895c-486c-ad99-2b32db2c7164","originalAuthorName":"李崇宁"},{"authorName":"王加林","id":"6d15967f-b1aa-492c-9003-5900696277f5","originalAuthorName":"王加林"},{"authorName":"曹秋娥","id":"b89522cc-6338-40b9-bb28-a8fc73f09d40","originalAuthorName":"曹秋娥"}],"doi":"10.3969/j.issn.1000-7571.2002.05.006","fpage":"17","id":"cf8ee9a7-e782-4fcb-866c-e15d9126e60f","issue":"5","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"3c381e65-e813-4912-b9c8-15299a341a75","keyword":"铱","originalKeyword":"铱"},{"id":"90683ee6-f835-43a8-b573-bc0be1641329","keyword":"丽<span style=\"color:red\">春</span>红G","originalKeyword":"丽春红G"},{"id":"a2a57fdf-fa6d-4d5d-bc97-967b1b2de292","keyword":"高碘酸钾","originalKeyword":"高碘酸钾"},{"id":"4ffcfe3c-3af4-41cd-ae8f-447d4f037585","keyword":"催化光度法","originalKeyword":"催化光度法"}],"language":"zh","publisherId":"yjfx200205006","title":"高碘酸钾氧化丽<span style=\"color:red\">春</span>红G催化光度法测定铱","volume":"22","year":"2002"},{"abstractinfo":"介绍了贝纳<span style=\"color:red\">德</span>效应,胆甾相液晶织构等概念,实验制备出胆甾相液晶平面态样品,用偏光显微镜观察温度场致织构变化,观察到液晶盒在清亮点温度附近出现特殊花纹图案,类似于贝纳<span style=\"color:red\">德</span>效应或者是温度场致方格栅效应.实验现象说明了温度场使液晶分子产生对流,在偏光显微镜下观察双折射干涉,指向矢分布有周期性变化,形成了微观的贝纳<span style=\"color:red\">德</span>花纹.实验现象对于胆甾相液晶基础研究具有一定意义.","authors":[{"authorName":"杨磊","id":"5013b502-d604-4221-9af6-8bbbd1960581","originalAuthorName":"杨磊"},{"authorName":"刘洋","id":"202a3a36-249d-468b-b8da-59e126411cd9","originalAuthorName":"刘洋"},{"authorName":"郑永磊","id":"b3d0d06e-5f02-457a-8669-2d895d24bcfb","originalAuthorName":"郑永磊"},{"authorName":"高攀","id":"d0eac134-2d43-4079-aead-c0198398411b","originalAuthorName":"高攀"},{"authorName":"范志新","id":"c705feda-75b8-4a3e-b8ce-75b233083e88","originalAuthorName":"范志新"}],"doi":"10.3788/YJYXS20122703.0288","fpage":"288","id":"33e8f1ec-a2c9-492e-91eb-0329df32f5d9","issue":"3","journal":{"abbrevTitle":"YJYXS","coverImgSrc":"journal/img/cover/YJYXS.jpg","id":"72","issnPpub":"1007-2780","publisherId":"YJYXS","title":"液晶与显示   "},"keywords":[{"id":"abe8f909-b3b4-46da-8e99-5ae5f2101e23","keyword":"胆甾相液晶","originalKeyword":"胆甾相液晶"},{"id":"3f874625-c7c5-48c7-ab2a-44cf168fb99b","keyword":"平面织构","originalKeyword":"平面织构"},{"id":"c5070beb-0731-49fc-b2c8-2db59f17bc70","keyword":"方格栅效应","originalKeyword":"方格栅效应"},{"id":"0dea2f30-25a1-44cc-b3df-f8245b693b31","keyword":"贝纳<span style=\"color:red\">德</span>效应","originalKeyword":"贝纳德效应"},{"id":"43b474c5-b82e-49a8-8bbe-9a835c9ce411","keyword":"偏光显微镜","originalKeyword":"偏光显微镜"}],"language":"zh","publisherId":"yjyxs201203002","title":"胆甾相液晶盒贝纳<span style=\"color:red\">德</span>效应实验","volume":"27","year":"2012"},{"abstractinfo":"在90 ℃水浴中,Co2+ 能催化铋酸钠氧化丽<span style=\"color:red\">春</span>红S褪色,据此建立了一种褪色光度法测定Co2+ 的新方法.Co2+在0～50 μg/mL范围内遵守比尔定律,表观摩尔吸光系数为1.814×103 L/(mol*cm),最大吸收波长为520 nm,该方法检出限为0.538 μg/mL.该方法用于测定锡-钴枪黑色合金镀液中钴的含量,结果令人满意.","authors":[{"authorName":"郭振良","id":"584bf7f2-7e7f-4127-ade6-2c272d72dfbf","originalAuthorName":"郭振良"},{"authorName":"唐清华","id":"9ce2a809-b843-4434-8e7c-dac0f58527cb","originalAuthorName":"唐清华"},{"authorName":"牟起娜","id":"d37d8b39-f7ec-454c-a7d0-cf3e62dd6762","originalAuthorName":"牟起娜"},{"authorName":"孙言志","id":"7c0484e8-9cab-4b29-a48b-4bcb2c838cd8","originalAuthorName":"孙言志"}],"doi":"10.3969/j.issn.1004-227X.2005.12.018","fpage":"63","id":"8c6b0946-37e5-47d0-aff4-bf52e1cf4d1a","issue":"12","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"f6c28cfe-17af-49c2-b37f-6d1108f657b6","keyword":"丽<span style=\"color:red\">春</span>红S","originalKeyword":"丽春红S"},{"id":"cde44370-4a27-46a1-9f05-62ccb3d33206","keyword":"褪色光度法","originalKeyword":"褪色光度法"},{"id":"e7ed13de-3a0a-4b14-b563-e2203460d95f","keyword":"合金镀液","originalKeyword":"合金镀液"},{"id":"6cccbb22-6b70-42fd-9eb3-d3701b2868e9","keyword":"钴","originalKeyword":"钴"}],"language":"zh","publisherId":"ddyts200512018","title":"丽<span style=\"color:red\">春</span>红S褪色光度法测定锡-钴合金镀液中的钴","volume":"24","year":"2005"},{"abstractinfo":"建立了一快速、简单地测定阿<span style=\"color:red\">德</span>福韦酯及其降解产物阿<span style=\"color:red\">德</span>福韦单特戊酸甲基酯、阿<span style=\"color:red\">德</span>福韦的反相高效液相色谱方法.以Inertsil CN-3化学键合硅胶为固定相,以乙腈-25 mmol/L磷酸盐缓冲液(pH 4.0)(体积比为33∶67)为流动相,流速1.0 mL/min,检测波长260 nm.阿<span style=\"color:red\">德</span>福韦酯、阿<span style=\"color:red\">德</span>福韦的质量浓度分别为1.861～181.7 mg/L和2.018～197.2 mg/L时与峰面积呈良好的线性关系(r分别为0.9999和0.9998);阿<span style=\"color:red\">德</span>福韦酯及阿<span style=\"color:red\">德</span>福韦平均加样回收率分别为99.5% ～101.0%和99.1% ～99.6% ,相对标准偏差(RSD)均低于1.0% ,阿<span style=\"color:red\">德</span>福韦的最小检测量(以信噪比为3计)为1 ng.该方法能同时测定阿<span style=\"color:red\">德</span>福韦酯及其降解产物,可用于阿<span style=\"color:red\">德</span>福韦酯降解产物的检测.","authors":[{"authorName":"蒋晔","id":"d81c9556-101e-44ae-8f7d-708558882cea","originalAuthorName":"蒋晔"},{"authorName":"徐智儒","id":"9eef3ed2-ee80-4552-ab3a-268dbcbc9fd9","originalAuthorName":"徐智儒"},{"authorName":"张晓青","id":"a608aa9c-6cca-4251-8a2a-f07c34a05c73","originalAuthorName":"张晓青"}],"doi":"10.3321/j.issn:1000-8713.2004.03.015","fpage":"248","id":"aae1beb3-7cee-4866-ac8c-fd12afe66285","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"b1838086-88c9-409b-a0bb-b040bd650e14","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"5511da67-0d84-4304-94fb-d76a67fc0b6b","keyword":"阿<span style=\"color:red\">德</span>福韦酯","originalKeyword":"阿德福韦酯"},{"id":"8b0de6ef-2781-4f9a-a028-670dc773b0c8","keyword":"降解产物","originalKeyword":"降解产物"}],"language":"zh","publisherId":"sp200403015","title":"反相高效液相色谱法测定阿<span style=\"color:red\">德</span>福韦酯及其降解产物","volume":"22","year":"2004"}],"totalpage":31,"totalrecord":303}