{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"用液相沉积法制备了壳层均匀、包裹致密的单分散P(St-co-AA)/Fe2O3亚微核壳粒子.用XRD、TEM和FESEM表征了该类粒子的物相、形貌及微观结构.结果表明用该法制备的核壳粒子,其壳层为Fe2O3晶粒,且均匀地包裹在乳胶粒子表面形成草莓状结构;改变FeCl3溶液的用量和重复包裹次数能方便地调节P(St-co-AA)/Fe2O3亚微核壳粒子的壳层厚度.可通过煅烧法用该核壳粒子来制备形状完整的单分散亚微中空磁球.","authors":[{"authorName":"<span style=\"color:red\">黄</span><span style=\"color:red\">中</span><span style=\"color:red\">梅</span>","id":"58ca2759-13e4-4cf1-834f-e47d6726c41b","originalAuthorName":"黄中梅"},{"authorName":"赵素玲","id":"832be98b-2550-4be1-934a-e7d10f651845","originalAuthorName":"赵素玲"}],"doi":"","fpage":"63","id":"77b43fd2-8769-4fca-a636-f66036ac8c77","issue":"10","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"a8686b7c-aef3-4826-abca-063c33b2087a","keyword":"核壳粒子","originalKeyword":"核壳粒子"},{"id":"86b4992c-5f2f-4216-b6ed-60b702a6b1ad","keyword":"亚微中空磁球","originalKeyword":"亚微中空磁球"},{"id":"9119020e-7d0e-4d3b-ac84-728a27806ca4","keyword":"聚(苯乙烯-共-丙烯酸)","originalKeyword":"聚(苯乙烯-共-丙烯酸)"},{"id":"80dded21-fc9c-44a8-85f5-44957b01196b","keyword":"Fe2O3","originalKeyword":"Fe2O3"}],"language":"zh","publisherId":"cldb201410016","title":"水解FeCl3制备单分散P(St-co-AA)/Fe2O3亚微核壳粒子","volume":"28","year":"2014"},{"abstractinfo":"结合空心纳微粒子的形成机理和结构可控性,阐述了空心纳微粒子的硬模板法和软模板法两大制备技术,重点综述了逐层自组装(LBL)法、表面化学反应与沉积法、微封装法等的研究进展.概述了空心纳微粒子的结构与性能的关系及其在材料科学、生物医学、催化剂等领域的应用现状及前景.","authors":[{"authorName":"<span style=\"color:red\">黄</span><span style=\"color:red\">中</span><span style=\"color:red\">梅</span>","id":"e74fc35c-5fc9-4c41-9560-c563b6d4017a","originalAuthorName":"黄中梅"},{"authorName":"官建国","id":"56c8b740-548f-4b53-a6ba-3a73dce21794","originalAuthorName":"官建国"},{"authorName":"甘治平","id":"b038cce9-85e0-4818-a945-01bad7991ddc","originalAuthorName":"甘治平"},{"authorName":"王振杰","id":"07dde63d-17cb-4a10-aab1-1636ec5c7952","originalAuthorName":"王振杰"}],"doi":"10.3321/j.issn:1000-324X.2005.06.001","fpage":"1281","id":"a620cb31-ab9d-4ef4-81f3-6cd7655e10e8","issue":"6","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"6cf196f0-b5eb-4bfb-86c0-93cf503ad762","keyword":"空心纳微粒子","originalKeyword":"空心纳微粒子"},{"id":"30c382d6-c01e-4e2d-982c-d8e901fec15f","keyword":"模板","originalKeyword":"模板"},{"id":"ccb6e5ba-29df-47ff-9fa8-838354a196ee","keyword":"逐层自组装法","originalKeyword":"逐层自组装法"},{"id":"3b7232a5-159f-486f-8b12-f072da454b56","keyword":"表面化学反应与沉积法","originalKeyword":"表面化学反应与沉积法"},{"id":"04e30f63-e5cc-45cc-8e6a-6de24fb84327","keyword":"微封装法","originalKeyword":"微封装法"}],"language":"zh","publisherId":"wjclxb200506001","title":"空心纳微粒子的模板法制备技术及应用","volume":"20","year":"2005"},{"abstractinfo":"<span style=\"color:red\">梅</span>钢铁水中磷含量偏高,冶炼低磷钢种有困难,通过对国内外降磷方法所采用的\"铁水炉外预脱磷\"、\"SRP法\"及\"转炉双渣法脱磷方法\"的比较分析,摸索出适合<span style=\"color:red\">梅</span>钢自身特点的方法--转炉同炉铁水脱磷炼钢工艺.通过在冶炼<span style=\"color:red\">中</span>采用前期造渣、中途倒渣的方法,将磷的质量分数降到≤0.01%,满足了生产低磷钢的要求.","authors":[{"authorName":"唐洪乐","id":"07f52dc6-c59e-4e0f-ae66-bd2d5c1bf385","originalAuthorName":"唐洪乐"},{"authorName":"汪洪峰","id":"ab27baba-5cb3-4e6f-99f0-9b2e0e782999","originalAuthorName":"汪洪峰"},{"authorName":"孙晓辉","id":"d53d7143-3298-436e-82b0-761567afc07b","originalAuthorName":"孙晓辉"}],"doi":"","fpage":"34","id":"645485c4-c2c3-41ec-95d8-e6e43c02277e","issue":"10","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"cb44b437-92fd-4616-8608-bf22a05dc3b7","keyword":"TBM顶底复吹","originalKeyword":"TBM顶底复吹"},{"id":"6fc84803-f180-4728-963f-0588623349d2","keyword":"脱磷率","originalKeyword":"脱磷率"},{"id":"f6649a2c-ccf1-418a-abb5-33f487c5c47a","keyword":"<span style=\"color:red\">中</span>磷铁水","originalKeyword":"中磷铁水"},{"id":"78984ddf-c3a0-4b3f-bee7-e43eb57898d4","keyword":"低磷钢","originalKeyword":"低磷钢"}],"language":"zh","publisherId":"gt200810008","title":"<span style=\"color:red\">梅</span>钢<span style=\"color:red\">中</span>磷铁水低磷钢冶炼问题的探讨","volume":"43","year":"2008"},{"abstractinfo":"在<span style=\"color:red\">梅</span>钢2号连铸机生产过程<span style=\"color:red\">中</span>,漏钢事故经常发生,同时误报的次数较为频繁,严重影响板坯质量和铸机的高效化生产的情况.针对这种情况,<span style=\"color:red\">梅</span>钢自主研发了适合<span style=\"color:red\">梅</span>钢二号连铸机的漏钢预报系统.模型投用后完全避免了粘结漏钢,解决了困扰<span style=\"color:red\">梅</span>钢2号连铸机正常生产的难题,并且为公司节约巨额费用.","authors":[{"authorName":"田建良","id":"2912a4f1-07df-4193-8d9b-d7fbc4fe9c06","originalAuthorName":"田建良"},{"authorName":"陈开义","id":"4d3b73ea-cb43-472b-be7c-d2c7d5a2568d","originalAuthorName":"陈开义"},{"authorName":"江中块","id":"59cfa878-c55b-4755-855e-b1ded9b6eeea","originalAuthorName":"江中块"}],"doi":"","fpage":"15","id":"38ff962c-1726-4ac2-bd24-fbaf1325e382","issue":"3","journal":{"abbrevTitle":"LZ","coverImgSrc":"journal/img/cover/LZ.jpg","id":"52","issnPpub":"1005-4006","publisherId":"LZ","title":"连铸"},"keywords":[{"id":"b538988a-0a42-4076-8f61-67c873f52d89","keyword":"粘结漏钢","originalKeyword":"粘结漏钢"},{"id":"65bc285f-a178-4164-9021-d2f76792c9ba","keyword":"预报系统","originalKeyword":"预报系统"}],"language":"zh","publisherId":"lz201303005","title":"<span style=\"color:red\">梅</span>钢漏钢预报系统的开发与实践","volume":"","year":"2013"},{"abstractinfo":"内<span style=\"color:red\">梅</span>罗指数和地质累积指数广泛应用于土壤、沉积物等环境介质<span style=\"color:red\">中</span>的重金属污染评价,选择金矿开发区土壤<span style=\"color:red\">中</span>Hg、Pb、Cu、Cd、Zn 5种重金属,对比了两种方法的评价结果,统计分析各个样品的综合污染程度,区分不同方法评价的差异,并提出了形成差异的主要原因.","authors":[{"authorName":"张江华","id":"efdcea07-2be1-458c-84fa-699bd0b89294","originalAuthorName":"张江华"},{"authorName":"赵阿宁","id":"f32933ac-35f0-4353-bb73-a2565d8dc9f0","originalAuthorName":"赵阿宁"},{"authorName":"王仲复","id":"2eb27f25-2f04-4b75-b13c-247e0a22aa30","originalAuthorName":"王仲复"},{"authorName":"柯海玲","id":"eff0ac9e-55f0-4a2d-aaa8-a9bce01d5559","originalAuthorName":"柯海玲"},{"authorName":"陈华清","id":"9606329a-4136-415f-82a1-428cb06ab0aa","originalAuthorName":"陈华清"}],"doi":"10.3969/j.issn.1001-1277.2010.08.013","fpage":"43","id":"f1cf5aba-2710-4849-942d-04491613fc65","issue":"8","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"20be97ae-033d-4402-b919-c39b28722962","keyword":"重金属污染","originalKeyword":"重金属污染"},{"id":"52cc6e94-854b-48af-8151-eda00703471c","keyword":"内<span style=\"color:red\">梅</span>罗指数","originalKeyword":"内梅罗指数"},{"id":"263bc8c0-00c8-49c6-a191-5a15da4005d6","keyword":"地质累积指数","originalKeyword":"地质累积指数"},{"id":"d0f4efc7-5f17-4522-a02a-8272047b1e40","keyword":"小秦岭金矿带","originalKeyword":"小秦岭金矿带"}],"language":"zh","publisherId":"huangj201008013","title":"内<span style=\"color:red\">梅</span>罗指数和地质累积指数在土壤重金属评价<span style=\"color:red\">中</span>的差异探讨——以小秦岭金矿带为例","volume":"31","year":"2010"},{"abstractinfo":"发展了一种新的采用毛细管区带电泳分析柠檬<span style=\"color:red\">黄</span>铝色淀和日落<span style=\"color:red\">黄</span>铝色淀的方法。通过前处理步骤成功实现了铝色淀<span style=\"color:red\">中</span>铝基质与色素的分离。利用石英毛细管柱（48.50 cm（有效长度40.00 cm）×50μm），分别针对柠檬<span style=\"color:red\">黄</span>铝色淀和日落<span style=\"color:red\">黄</span>铝色淀进行了电泳条件的优化，并得到最优分离结果。所建立的定量分析方法的检出限对于柠檬<span style=\"color:red\">黄</span>铝色淀和日落<span style=\"color:red\">黄</span>铝色淀分别达0.26 mg / L 和0.27 mg / L，线性范围分别为0.53~1.3×102 mg / L 和0.54~1.4×102 mg / L，两种被分析物的测定重复性（RSD，n =6）分别为4.3％和5.7％，日间重复性（ RSD，n =6）分别为5.6％和6.0％。经过更深入研究后，该方法可以发展为食品<span style=\"color:red\">中</span>相应色淀的检测方法。","authors":[{"authorName":"张一丁","id":"a3cd5a59-625b-4a67-906e-a58d01f934b0","originalAuthorName":"张一丁"},{"authorName":"常翠兰","id":"bd234c61-9f75-42c4-9867-88ba02e2e682","originalAuthorName":"常翠兰"},{"authorName":"郭启雷","id":"ba21cc69-4e1c-4f84-93c8-2b377338be44","originalAuthorName":"郭启雷"},{"authorName":"曹红","id":"43e261aa-deea-48df-964a-30f28d775cb2","originalAuthorName":"曹红"},{"authorName":"白玉","id":"e16b1374-1276-4df1-a852-6303926fc681","originalAuthorName":"白玉"},{"authorName":"刘虎威","id":"a6637165-a99e-44d9-b78b-5485c5a9effb","originalAuthorName":"刘虎威"}],"doi":"10.3724/SP.J.1123.2013.11020","fpage":"438","id":"34bddd19-2587-4a94-9cd5-a466cb60472f","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"1dd3d34a-c643-427f-a637-fb3e56f9a722","keyword":"毛细管区带电泳","originalKeyword":"毛细管区带电泳"},{"id":"fccec8e0-4a52-4539-86a6-31f6e774afea","keyword":"柠檬<span style=\"color:red\">黄</span>","originalKeyword":"柠檬黄"},{"id":"e8e9f7cc-130d-4f7e-bf65-b2c7d231f885","keyword":"日落<span style=\"color:red\">黄</span>","originalKeyword":"日落黄"},{"id":"621766ff-feb5-4cc5-a66c-09c06f6f971d","keyword":"色淀","originalKeyword":"色淀"},{"id":"3a9685cb-c5ad-41ad-aa36-0abd952990ea","keyword":"食品","originalKeyword":"食品"}],"language":"zh","publisherId":"sp201404019","title":"食品<span style=\"color:red\">中</span>柠檬<span style=\"color:red\">黄</span>铝色淀和日落<span style=\"color:red\">黄</span>铝色淀的毛细管区带电泳分析","volume":"","year":"2014"},{"abstractinfo":"模拟土壤施用稀土定位试验结果表明:<span style=\"color:red\">黄</span>刚土<span style=\"color:red\">中</span>各组份吸附稀土的能力为:无定形FexOy、紧结有机物＞松结有机物＞MnOx＞晶形FexOy＞永久负电荷;进入<span style=\"color:red\">黄</span>刚土的外源轻稀土,主要累积于紧结有机态(29.90～49.72%)、无定形氧化铁吸附态(26.81～46.76%),而累积于松结有机态的轻稀土受外源稀土的加入量影响较小(24.93～28.72%).当外源稀土用量在0.684～2.735mg/kg*季时,大豆地上部稀土无明显增加,而用量达13.674mg/kg时,地上部明显增加.<span style=\"color:red\">黄</span>刚土外源稀土的最佳用量为0.684mg/kg,此时,大豆增产43.82±15.08%、油菜增产17.92±9.07%.","authors":[{"authorName":"荆国芳","id":"fc1b92c6-600d-4fcd-8e1e-fa3dc5a1c9f5","originalAuthorName":"荆国芳"},{"authorName":"钱晓晴","id":"f0c35fa0-cdb7-47b9-b5f0-473802d2c771","originalAuthorName":"钱晓晴"}],"doi":"10.3969/j.issn.1004-0277.2002.02.011","fpage":"38","id":"8b89503d-85fe-42d8-a31b-5ee41eed9fc4","issue":"2","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"d9808f7e-67c4-4266-9caf-60295c858dc6","keyword":"稀土","originalKeyword":"稀土"},{"id":"60f39a5b-d062-4283-92b6-49c319b6ff2e","keyword":"形态","originalKeyword":"形态"},{"id":"97b50517-dd4d-4380-b408-02394f1ee3bd","keyword":"生态效应","originalKeyword":"生态效应"}],"language":"zh","publisherId":"xitu200202011","title":"外源稀土在<span style=\"color:red\">黄</span>刚土<span style=\"color:red\">中</span>形态分布和生态效应研究","volume":"23","year":"2002"},{"abstractinfo":"建立了快速检测环境水样<span style=\"color:red\">中</span>的丁基<span style=\"color:red\">黄</span>原酸的离子色谱-紫外检测方法.以NaOH淋洗液等度淋洗,丁基<span style=\"color:red\">黄</span>原酸在IonPacAS16高效阴离子交换柱(HPAEC)上可以在8 min内完成分离,而常规共存离子无干扰.使用紫外检测法(UV)301nm波长进行测定,丁基<span style=\"color:red\">黄</span>原酸的检出限(500 μL进样,S/N=3)分别为0.1 μg·L-1,且均具有较宽的线性范围(0.5-1000 μg·L-1).5 μg· L-1丁基<span style=\"color:red\">黄</span>原酸标准溶液测定的相对标准偏差小于1％,而样品加标回收率在99.3％-104.8％之间.该方法检测丁基<span style=\"color:red\">黄</span>原酸无需复杂前处理、检测迅速、灵敏度高,适用于地表水中丁基<span style=\"color:red\">黄</span>原酸的分析.","authors":[{"authorName":"李仁勇","id":"13b1402d-1df2-4e6c-a17f-2e700ea36e4a","originalAuthorName":"李仁勇"}],"doi":"","fpage":"688","id":"daaa1004-a63d-40f2-9b71-6cd035e81b98","issue":"3","journal":{"abbrevTitle":"HJHX","coverImgSrc":"journal/img/cover/HJHX.jpg","id":"43","issnPpub":"0254-6108","publisherId":"HJHX","title":"环境化学   "},"keywords":[{"id":"b3f6ddc0-18e3-4e33-9f8e-e92486ae1ad9","keyword":"离子色谱","originalKeyword":"离子色谱"},{"id":"c624ec5e-dec7-4095-a80e-b46a3f78c254","keyword":"紫外检测","originalKeyword":"紫外检测"},{"id":"3ce5b231-c12a-4e54-9816-730ac8e3d6ff","keyword":"IonPac AS16","originalKeyword":"IonPac AS16"},{"id":"f5b071a8-2075-498b-ad3f-52842947a33a","keyword":"环境水样","originalKeyword":"环境水样"},{"id":"63064339-1cb3-4e1f-ba83-1e50a8e95e27","keyword":"丁基<span style=\"color:red\">黄</span>原酸","originalKeyword":"丁基黄原酸"}],"language":"zh","publisherId":"hjhx201703029","title":"离子色谱法串联紫外检测环境地表水样<span style=\"color:red\">中</span>丁基<span style=\"color:red\">黄</span>原酸","volume":"36","year":"2017"},{"abstractinfo":"低碳钢在双氧水系抛光液<span style=\"color:red\">中</span>化学抛光时,双氧水易分解,温度不易控制,而在硝酸系抛光液<span style=\"color:red\">中</span>化学抛光会产生<span style=\"color:red\">黄</span>烟且能耗较大.为此,研制了一种新型无<span style=\"color:red\">黄</span>烟低碳钢<span style=\"color:red\">中</span>温化学抛光液对Q235钢化学抛光,考察了化学抛光液组成及温度、时间对抛光质量的影响.结果表明:使用本工艺的化学抛光试样表面平整、粗糙度低,光亮度达3～4级;获得最佳抛光质量的化学抛光工艺为120～250 mL/L H3PO4,100～200 mL/L H3SO4,40～80 g/L NaNO3,10～40 g/L NaCl,20 g/L复合添加剂,55～65℃,2～5 min.","authors":[{"authorName":"朱其柱","id":"915a74d4-7101-4eaa-96b4-addf8a6415b6","originalAuthorName":"朱其柱"},{"authorName":"金光","id":"412b152f-2cb6-4d47-866a-03af54d7a13d","originalAuthorName":"金光"},{"authorName":"赵晖","id":"c3f3492c-b025-4df9-a83c-e7c38a1a7dca","originalAuthorName":"赵晖"}],"doi":"","fpage":"42","id":"d319e205-e66e-47bd-bdef-1925a14ab04a","issue":"9","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"6b2153e6-1e09-4d98-822e-67434c68e3f7","keyword":"化学抛光","originalKeyword":"化学抛光"},{"id":"c537e638-18f1-4a72-b258-d4574cbe0b0a","keyword":"Q235钢","originalKeyword":"Q235钢"},{"id":"2a88ac12-86b4-4293-b400-567886dd9646","keyword":"<span style=\"color:red\">中</span>温","originalKeyword":"中温"},{"id":"8dc9b550-70a9-471f-95ec-7d9c02e0b11b","keyword":"光亮度","originalKeyword":"光亮度"}],"language":"zh","publisherId":"clbh201009014","title":"Q235钢<span style=\"color:red\">中</span>温无<span style=\"color:red\">黄</span>烟化学抛光工艺","volume":"43","year":"2010"},{"abstractinfo":"以壳聚糖为吸附剂,戊二醛作为交联剂,采用反相悬浮交联法制备球状壳聚糖树脂,利用二硫化碳作为改性剂,在碱性条件下对壳聚糖树脂进行<span style=\"color:red\">黄</span>原酸化改性,制备成交联<span style=\"color:red\">黄</span>原酸化壳聚糖树脂(cross-linked xanthated chitosan resin,CXCR).对 CXCR进行红外表征,并研究了其对水溶液<span style=\"color:red\">中</span>棒曲霉素的吸附性能.结果表明,CXCR 在棒曲霉素初始浓度为8 mg/L,CXCR 用量为1 g/L,溶液 pH 值＝4,25℃下吸附16 h,吸附量可达6．53 mg/g,可有效地吸附水溶液<span style=\"color:red\">中</span>的棒曲霉素.CXCR 对棒曲霉素的吸附符合拟二级动力学模型；吸附热力学符合 Freundlich 吸附等温线模型.CXCR 有望作为一种新型的材料用于棒曲霉素的吸附,具有广阔的应用前景.","authors":[{"authorName":"刘心荷","id":"4cc4f365-7fcc-4f23-bd15-5f9d8ab6f41e","originalAuthorName":"刘心荷"},{"authorName":"李杨","id":"b6ff6fc6-9ac8-4eaf-b562-c30fa26a17fa","originalAuthorName":"李杨"},{"authorName":"孟祥红","id":"7d4f140e-18e8-4c6b-bfb4-bd66bff2f59a","originalAuthorName":"孟祥红"},{"authorName":"刘炳杰","id":"e6f1f754-c172-4062-9a45-646fc4d8c2ab","originalAuthorName":"刘炳杰"}],"doi":"10.3969/j.issn.1001-9731.2015.04.004","fpage":"4020","id":"9ec9e735-106b-47b3-bb55-a1068e6b742e","issue":"4","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"bdc9ac8f-35c9-4558-9751-28b409ca899d","keyword":"壳聚糖树脂","originalKeyword":"壳聚糖树脂"},{"id":"8f3fe566-5ce9-4eba-a921-1ad019f38477","keyword":"<span style=\"color:red\">黄</span>原酸化","originalKeyword":"黄原酸化"},{"id":"c2e87a30-c0bf-482e-8238-71ca9be66203","keyword":"改性","originalKeyword":"改性"},{"id":"94480ea7-0d46-475a-bc31-a2efcc036ed3","keyword":"棒曲霉素","originalKeyword":"棒曲霉素"},{"id":"fd3fd57a-303c-458e-9dcf-d3ef0353c0b3","keyword":"吸附","originalKeyword":"吸附"}],"language":"zh","publisherId":"gncl201504004","title":"交联<span style=\"color:red\">黄</span>原酸化壳聚糖树脂对水溶液<span style=\"color:red\">中</span>棒曲霉素的吸附","volume":"","year":"2015"}],"totalpage":9226,"totalrecord":92258}