{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"制备了不同结构的聚二甲基硅氧烷/聚砜复合膜,以<span style=\"color:red\">苯</span>/<span style=\"color:red\">水</span><span style=\"color:red\">物</span><span style=\"color:red\">系</span>考察了膜结构、操作条件等因素对复合膜渗透汽化分离性能的影响.实验结果表明,料液浓度升高、下游压力减低、操作温度升高、料液流量增大、活性层厚度变薄有利于渗透汽化的传质过程;聚砜基膜的传质阻力不可忽略,决定其传质阻力的主要因素为基膜的结构.","authors":[{"authorName":"陈镇","id":"c73b325f-5a5c-4577-bb58-e237d1e1abf6","originalAuthorName":"陈镇"},{"authorName":"刘家祺","id":"74d614ab-ac90-4b52-bc12-5e7ca24a2bb6","originalAuthorName":"刘家祺"},{"authorName":"李俊台","id":"1121b9c8-7c00-415c-ba51-75b6a3c52ba7","originalAuthorName":"李俊台"}],"doi":"10.3969/j.issn.1007-8924.2004.04.008","fpage":"32","id":"4c72355c-20e2-4491-a82b-41ca197de20b","issue":"4","journal":{"abbrevTitle":"MKXYJS","coverImgSrc":"journal/img/cover/MKXYJS.jpg","id":"54","issnPpub":"1007-8924","publisherId":"MKXYJS","title":"膜科学与技术   "},"keywords":[{"id":"3ad5ff00-dc44-44c8-92d2-17787d099bc7","keyword":"渗透汽化","originalKeyword":"渗透汽化"},{"id":"44bd11df-083c-480b-a2fe-77a8f8c6c477","keyword":"聚二甲基硅氧烷/聚砜(PDMS/PS)","originalKeyword":"聚二甲基硅氧烷/聚砜(PDMS/PS)"},{"id":"8b1fc48b-e905-4399-b3b8-3d5fa0aee52c","keyword":"复合膜","originalKeyword":"复合膜"},{"id":"8e7d1c7b-8b61-40e7-87e6-5be5d8dde710","keyword":"<span style=\"color:red\">苯</span>/<span style=\"color:red\">水</span><span style=\"color:red\">物</span><span style=\"color:red\">系</span>","originalKeyword":"苯/水物系"}],"language":"zh","publisherId":"mkxyjs200404008","title":"渗透汽化法回收水中挥发性有机<span style=\"color:red\">物</span>的影响因素分析","volume":"24","year":"2004"},{"abstractinfo":"介绍了<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的危害和来源,分析了国内外涂料中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>含量的安全限量标准,提出了控制涂料中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>含量的建议,为规范我国涂料生产和使用以及涂料中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>限量标准的制定和修订提供参考.","authors":[{"authorName":"戴继勇","id":"65d8c7ff-bdb5-4672-b66a-40792ee83b18","originalAuthorName":"戴继勇"},{"authorName":"陶学明","id":"45dd3580-3b22-4854-a176-03ced52f495b","originalAuthorName":"陶学明"},{"authorName":"张士胜","id":"cbd67e1f-9987-43e7-a14d-9daeb9c11ed2","originalAuthorName":"张士胜"},{"authorName":"郑玉艳","id":"f132ab04-39ac-49f4-a090-876ad1c88332","originalAuthorName":"郑玉艳"},{"authorName":"洪登华","id":"a84e5014-d472-450e-b55d-91dcd8ad0b30","originalAuthorName":"洪登华"}],"doi":"","fpage":"73","id":"521b9f69-fac1-44da-817c-fbe05b9d35bc","issue":"8","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"08dc6cb9-0006-450d-95bf-30491193eee7","keyword":"涂料","originalKeyword":"涂料"},{"id":"d4f80976-0c16-4eef-b8cc-cc154c3cd070","keyword":"油漆","originalKeyword":"油漆"},{"id":"fbcd13b2-53aa-4594-b0c3-8971687695f7","keyword":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","originalKeyword":"苯系物"},{"id":"083d5fa7-9250-4fd6-b990-9c7298a21d05","keyword":"安全限量","originalKeyword":"安全限量"},{"id":"c9c2e646-d3a4-4086-9e57-b250b882232f","keyword":"标准","originalKeyword":"标准"}],"language":"zh","publisherId":"ddyts201208019","title":"国内外油漆涂料中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>安全限量标准的研究","volume":"31","year":"2012"},{"abstractinfo":"含<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>废气严重危害人体健康.首先调研了常规处理含<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>废气所采用的方法,如吸收法、吸附法、热破坏法、冷凝法和膜分离法,概括了各方法的作用机理及特点;其次介绍了近年来开发的新技术,如生物法、光催化法和等离子体法;最后对比分析了各方法的优缺点,并提出含<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>废气处理技术日后的发展方向.","authors":[{"authorName":"闫柯乐","id":"10a1bb0e-f053-446d-9baf-a87c68722f8a","originalAuthorName":"闫柯乐"},{"authorName":"张红星","id":"ee7305ff-ed52-4cf3-8509-e5f5ddc010ff","originalAuthorName":"张红星"},{"authorName":"邹兵","id":"e95d8b63-7614-4132-97ff-447050167e7b","originalAuthorName":"邹兵"},{"authorName":"姜素霞","id":"5e89a154-4c8d-48b8-8fb4-30f406d9407e","originalAuthorName":"姜素霞"},{"authorName":"姜鸣","id":"d9810fbc-473b-4fb3-af41-90ddd0c19639","originalAuthorName":"姜鸣"}],"doi":"","fpage":"103","id":"3ed45b82-c6fa-4dea-be03-1ff17d26667e","issue":"1","journal":{"abbrevTitle":"HCCLLHYYY","coverImgSrc":"journal/img/cover/HCCLLHYYY.jpg","id":"42","issnPpub":"1671-5381","publisherId":"HCCLLHYYY","title":"合成材料老化与应用"},"keywords":[{"id":"fd6a4416-86b1-45ae-8c44-d93a8e4f4563","keyword":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","originalKeyword":"苯系物"},{"id":"0b1a1882-395b-4f9b-a07a-c8d9ad1e9435","keyword":"废气处理","originalKeyword":"废气处理"},{"id":"a14bbae5-e984-4139-a827-43a0147c4e63","keyword":"吸附法","originalKeyword":"吸附法"},{"id":"f7c7c2a2-8d38-4f60-86b9-bf24deeb5f54","keyword":"生物处理","originalKeyword":"生物处理"}],"language":"zh","publisherId":"hccllhyyy201601023","title":"含<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>废气处理技术研究进展","volume":"45","year":"2016"},{"abstractinfo":"采用错流纳滤工艺开展了饮用水中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span>污染<span style=\"color:red\">物</span>的去除效能和纳滤运行特性的研究,考察了纳滤膜对<span style=\"color:red\">苯</span>、乙苯、邻二甲苯和间二甲苯的截留效果,研究了操作压力、浓水流量、离子浓度、进水温度和<span style=\"color:red\">苯</span><span style=\"color:red\">系</span>污染<span style=\"color:red\">物</span>浓度等因素的影响.结果表明,随着操作压力和进水温度的升高,膜通量呈增加趋势;随浓水流量和离子浓度的升高,膜通量呈降低趋势;随着回收率、操作压力、离子浓度和进水温度的增加,纳滤膜的截留率均降低;随浓水流量和<span style=\"color:red\">苯</span><span style=\"color:red\">系</span>污染<span style=\"color:red\">物</span>浓度的增加,纳滤膜的截留率升高,在所有试验条件下,纳滤膜对4种<span style=\"color:red\">苯</span><span style=\"color:red\">系</span>污染<span style=\"color:red\">物</span>的截留率都介于86.56％～98.85％之间,出水中乙苯、邻二甲苯和间二甲苯含量均符合《生活饮用水卫生标准》(GB5749-2006);进水<span style=\"color:red\">苯</span>含量低于0.1 mg/L时,出水<span style=\"color:red\">苯</span>含量能满足国标要求.通过研究投资和运行成本,确定出经济运行参数为回收率90％、操作压力0.6 MPa和浓水流量30 L/min.","authors":[{"authorName":"赵伟业","id":"db4ed886-043e-4e64-a3e8-bb643d87488d","originalAuthorName":"赵伟业"},{"authorName":"李星","id":"ee8dd581-015d-4383-8131-914062672fd3","originalAuthorName":"李星"},{"authorName":"杨艳玲","id":"58fcdd5b-183c-4157-8a4f-03a945954d0c","originalAuthorName":"杨艳玲"},{"authorName":"朱学武","id":"5d5d1ea4-fabc-489d-80eb-34922848eec3","originalAuthorName":"朱学武"},{"authorName":"梁恒","id":"f88fd57b-1f86-4f2b-808f-a111e4e3517a","originalAuthorName":"梁恒"},{"authorName":"李圭白","id":"de4d25a6-d028-4226-a121-5d04d9e7bc58","originalAuthorName":"李圭白"},{"authorName":"刘永旺","id":"f36fe28b-2920-4362-af94-5faa96adb4a4","originalAuthorName":"刘永旺"},{"authorName":"谢柏明","id":"8c55c19f-dfb2-4ae1-becf-a2edf45a82cc","originalAuthorName":"谢柏明"}],"doi":"10.16159/j.cnki.issn1007-8924.2017.01.018","fpage":"114","id":"244701a1-255e-4dcb-9282-b573dd383bd5","issue":"1","journal":{"abbrevTitle":"MKXYJS","coverImgSrc":"journal/img/cover/MKXYJS.jpg","id":"54","issnPpub":"1007-8924","publisherId":"MKXYJS","title":"膜科学与技术   "},"keywords":[{"id":"f502eb64-41a8-479c-bf27-35fc022f4b1d","keyword":"饮用水","originalKeyword":"饮用水"},{"id":"28028707-0391-4abc-90a3-3f63394e00a9","keyword":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span>污染<span style=\"color:red\">物</span>","originalKeyword":"苯系污染物"},{"id":"a6cf2b73-a8f8-45d0-ae55-a8f0c4a0d0b4","keyword":"纳滤","originalKeyword":"纳滤"},{"id":"184a0aee-4c93-4638-97ae-e90713828437","keyword":"截留率","originalKeyword":"截留率"},{"id":"35f7d48c-0825-4763-af21-a9dbbf765dd0","keyword":"膜通量","originalKeyword":"膜通量"}],"language":"zh","publisherId":"mkxyjs201701018","title":"纳滤膜去除饮用水中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span>污染<span style=\"color:red\">物</span>效能试验研究","volume":"37","year":"2017"},{"abstractinfo":"建立了吹扫捕集气相色谱法测定水性涂料中8种<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的分析方法,对色谱条件、吹扫条件等进行了探讨,同时对分析参数如线性相关性、相对标准偏差、最低检出限及加标回收率进行了评价.结果表明:采用吹扫捕集气相色谱法,在2.5～ 50.0 μg/L范围内,8种<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的质量浓度和峰面积呈良好的线性关系；对加标浓度为5.0μg/L的涂料样品平行测定7次,其相对标准偏差为1.8％～4.3％；水性涂料样品的加标回收率在88.3％ ～ 107％之间；最低检出限在0.50～1.0 μg/L之间.","authors":[{"authorName":"张瑞平","id":"c3d4f655-0cb5-45eb-acd5-be3235e1646e","originalAuthorName":"张瑞平"},{"authorName":"胡江瑛","id":"fac4e367-7a77-4f54-baa3-592edcd6954e","originalAuthorName":"胡江瑛"},{"authorName":"方德明","id":"49f24c24-70ac-4743-9e74-ac33cc3e83fc","originalAuthorName":"方德明"}],"doi":"10.3969/j.issn.0253-4312.2012.10.017","fpage":"69","id":"d60d4701-3c58-435c-8542-3d4fc644efb6","issue":"10","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"b8b98253-e498-4061-b18f-4a693fa3983d","keyword":"吹扫捕集","originalKeyword":"吹扫捕集"},{"id":"fa6cc988-ee78-4957-bdd0-4fe1e45c48c2","keyword":"气相色谱","originalKeyword":"气相色谱"},{"id":"6dc7099c-70ba-497f-8b3b-d8f87b6b845a","keyword":"水性涂料","originalKeyword":"水性涂料"},{"id":"60e9f66e-5981-437b-abaf-6ee0c0bbfbd4","keyword":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","originalKeyword":"苯系物"}],"language":"zh","publisherId":"tlgy201210017","title":"吹扫捕集气相色谱法测定水性涂料中的<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","volume":"42","year":"2012"},{"abstractinfo":"针对离子迁移谱难分辨迁移率相近或相同的有机<span style=\"color:red\">物</span>,开展了气相色谱-紫外光电离-离子迁移谱联用技术的研究.通过测量不同色谱柱温和氮载气流量条件下<span style=\"color:red\">苯</span>的色谱和迁移谱,对实验参数进行了优化.并对<span style=\"color:red\">苯</span>、甲苯,以及邻、间、对一二甲苯等五种<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>混合<span style=\"color:red\">物</span>进行了测量,获得了混合样品的色谱保留时间、迁移谱离子迁移时间与离子信号强度的三维谱图.结果表明,同分异构体邻、间、对-二甲苯的迁移率非常接近,单一的紫外光电离-离子迁移谱无法对它们进行分辨,通过色谱-迁移谱技术的联用,则可以实现<span style=\"color:red\">苯</span>、甲苯,以及邻、间、对-二甲苯混合<span style=\"color:red\">物</span>的有效分辨.证明所建立的气相色谱-紫外光电离-离子迁移谱技术具有良好的分辨检测能力.","authors":[{"authorName":"邓巧玲","id":"a212b2fd-ab8b-4dc0-80fa-772e9c27bfe1","originalAuthorName":"邓巧玲"},{"authorName":"李虎","id":"11b43251-d4a8-4f33-ab8f-3dbb824fb199","originalAuthorName":"李虎"},{"authorName":"韩海燕","id":"631c1ec5-7925-4ad6-a808-14f9c40a6898","originalAuthorName":"韩海燕"},{"authorName":"沈成银","id":"cdc23662-eda9-4ef9-81c0-8c8e2486dc64","originalAuthorName":"沈成银"},{"authorName":"王鸿梅","id":"b8318dad-13c7-4681-a0c2-c86000e9df54","originalAuthorName":"王鸿梅"},{"authorName":"江海河","id":"be68868a-22e6-45e9-a4e7-515ec0ef87a9","originalAuthorName":"江海河"},{"authorName":"储焰南","id":"2c4ed7c5-b4ab-49a4-b41b-9e7bc8324384","originalAuthorName":"储焰南"}],"doi":"10.3969/j.issn.1007-5461.2011.01.003","fpage":"12","id":"36b19698-f798-4d4c-99ce-0427a4222e0f","issue":"1","journal":{"abbrevTitle":"LZDZXB","coverImgSrc":"journal/img/cover/LZDZXB.jpg","id":"53","issnPpub":"1007-5461","publisherId":"LZDZXB","title":"量子电子学报   "},"keywords":[{"id":"48dc6097-31da-4871-8d9b-d4750b2606f9","keyword":"光谱学","originalKeyword":"光谱学"},{"id":"bc6a01a0-f2f7-44de-b0da-582bf9737072","keyword":"气相色谱","originalKeyword":"气相色谱"},{"id":"93d51ba9-abc5-45fe-b470-adf39bbfa32b","keyword":"紫外光电离-离子迁移谱","originalKeyword":"紫外光电离-离子迁移谱"},{"id":"7dd1c720-42de-4bb4-8439-2942841e22ab","keyword":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","originalKeyword":"苯系物"},{"id":"7fa8cf65-a3de-4bbc-a29d-2b4d648a1f2a","keyword":"同分异构体","originalKeyword":"同分异构体"}],"language":"zh","publisherId":"lzdzxb201101003","title":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的色谱光电离迁移谱两维分辨检测方法研究","volume":"28","year":"2011"},{"abstractinfo":"利用激光电离技术进行大气压力下的环境<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的探测,是一种新的探测方法,它能快速、实时、在线测量环境中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的浓度,并且设备简单,不需要复杂的真空系统,其探测灵敏度小于5 ppb,时间分辨率为4 s.该方法尤其适合机动车道边附近的测量.文中介绍了系统结构和主要参数,报道了该仪器在不同的交通状况下,探测大气环境中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的一些结果,车流量大则污染严重,车流量小则污染轻.","authors":[{"authorName":"周留柱","id":"84f09c74-0c13-4ab1-a89f-b0494da43011","originalAuthorName":"周留柱"},{"authorName":"方黎","id":"aee90218-d144-4a77-9182-fbab92ea2b6e","originalAuthorName":"方黎"},{"authorName":"孔祥和","id":"7c267490-8db0-4d40-87b4-8535a8380506","originalAuthorName":"孔祥和"},{"authorName":"郑海洋","id":"808b25bf-0fe4-4760-a946-a83109ce5e71","originalAuthorName":"郑海洋"},{"authorName":"夏柱红","id":"7e70dc47-22dc-4ad8-9d20-cb8dc57ebc34","originalAuthorName":"夏柱红"},{"authorName":"顾学军","id":"d284466c-6d57-4530-8a9f-e63355994bd2","originalAuthorName":"顾学军"},{"authorName":"朱元","id":"66eef9e0-1e7c-46b1-8c90-f24c6225016f","originalAuthorName":"朱元"},{"authorName":"张为俊","id":"9555de53-8a7d-4f43-b2b3-1ece61452691","originalAuthorName":"张为俊"}],"doi":"10.3969/j.issn.1007-5461.2003.02.015","fpage":"203","id":"3b6cda0f-4a1c-4008-a72c-bda2ebd27975","issue":"2","journal":{"abbrevTitle":"LZDZXB","coverImgSrc":"journal/img/cover/LZDZXB.jpg","id":"53","issnPpub":"1007-5461","publisherId":"LZDZXB","title":"量子电子学报   "},"keywords":[{"id":"a68291ed-5b69-43b8-bd90-a8f04e1c5f23","keyword":"激光电离技术","originalKeyword":"激光电离技术"},{"id":"72435b3b-7bd7-46f5-8925-ea64560081de","keyword":"机动车尾气","originalKeyword":"机动车尾气"},{"id":"d348970a-f84c-4685-9ab0-6f9367f32597","keyword":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","originalKeyword":"苯系物"},{"id":"86d52185-25e2-4844-8025-23e61fdca5f1","keyword":"探测","originalKeyword":"探测"}],"language":"zh","publisherId":"lzdzxb200302015","title":"大气压力下激光电离技术探测环境痕量<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>实验研究","volume":"20","year":"2003"},{"abstractinfo":"以正丁基锂为引发剂,合成丁<span style=\"color:red\">苯</span>阴离子聚合<span style=\"color:red\">物</span>,通过对不同的反应温度、活性聚合<span style=\"color:red\">物</span>停留时间、极性添加剂及单体浓度的试验,分析其中大分子的含量.结果表明,反应温度、活性聚合<span style=\"color:red\">物</span>停留时间是形成大分子的主要因素.通过反应机理分析,大分子主要是由于活性聚合<span style=\"color:red\">物</span>热分解产生共轭双键的聚合<span style=\"color:red\">物</span>继续与未终止的活性<span style=\"color:red\">物</span>反应而成.","authors":[{"authorName":"蒋遥明","id":"80f6b628-831f-4504-9915-f9b2c46933f3","originalAuthorName":"蒋遥明"},{"authorName":"徐建波","id":"518433ab-2d32-450c-ab2e-80755cadc170","originalAuthorName":"徐建波"},{"authorName":"熊华富","id":"fb10eb68-0f86-492e-8bff-7af49556e016","originalAuthorName":"熊华富"},{"authorName":"刘先珍","id":"20b0d12e-7638-4674-a333-6e0da2aa71c8","originalAuthorName":"刘先珍"},{"authorName":"张爱民","id":"f58fe4fb-dc64-471e-92c5-fba318bb9d67","originalAuthorName":"张爱民"}],"doi":"","fpage":"184","id":"4c7bae5a-9303-4519-97d1-eb5feddebb30","issue":"1","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"68078512-8160-4e66-bf0b-1c4adf981ed4","keyword":"丁<span style=\"color:red\">苯</span>聚合<span style=\"color:red\">物</span>","originalKeyword":"丁苯聚合物"},{"id":"3c16ec58-e699-42ee-8df1-9fd9a64bbf70","keyword":"阴离子聚合","originalKeyword":"阴离子聚合"},{"id":"5350fd8f-c8c8-4157-ab3b-d3148ae8c2c3","keyword":"大分子","originalKeyword":"大分子"},{"id":"2c390223-7e27-4aeb-8151-91de35861f15","keyword":"活性聚合<span style=\"color:red\">物</span>","originalKeyword":"活性聚合物"}],"language":"zh","publisherId":"gfzclkxygc200501045","title":"丁<span style=\"color:red\">苯</span>锂<span style=\"color:red\">系</span>阴离子聚合<span style=\"color:red\">物</span>中大分子的成因研究","volume":"21","year":"2005"},{"abstractinfo":"建立了静态顶空萃取、气相色谱-质谱联用( HS-GC/MS)同时测定海水中常见的痕量13种<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>(BTEX)方法.对影响分析效果的主要条件:色谱柱类型、升温程序、顶空平衡温度、平衡时间以及气液体积比进行了详细的分析和优化.在优化条件下,该方法的线性相关系数大于0.999,线性范围为0.16～320μg/L,检出限(按信噪比为3计)为0.019～0.033μg/L;水样中3个加标水平(1.6、16和160 μg/L)的回收率为81.25％～103.73％,相对标准偏差(RSD,n=6)为0.3％～4.4％.将该方法应用于上海黄浦区海水样品中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的测定,结果令人满意.该方法分析时间为12 min.操作简单快捷,灵敏度高,环境友好,定性、定量准确、可靠.","authors":[{"authorName":"白红妍","id":"0909a8ed-0558-4858-a761-c3b5a1716735","originalAuthorName":"白红妍"},{"authorName":"韩彬","id":"e67f0493-a53b-4ab9-aed1-1e41ce0cf389","originalAuthorName":"韩彬"},{"authorName":"陈军辉","id":"dc5c9ac8-612b-4492-9bd3-510b088e1a8d","originalAuthorName":"陈军辉"},{"authorName":"郑立","id":"14f25d69-4e4d-4f4f-9a2f-5418e2ec04fe","originalAuthorName":"郑立"},{"authorName":"杨东方","id":"08248180-fbac-46d4-b267-732cfef46cb9","originalAuthorName":"杨东方"},{"authorName":"王小如","id":"b3fec854-ff93-43fd-a83d-9555d6d72e52","originalAuthorName":"王小如"}],"doi":"10.3724/SP.J.1123.2011.12042","fpage":"474","id":"b59ff9a0-e612-4e5f-a40a-68e6781f5676","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"275e9b31-a4de-4ad5-9b03-e573c05f2e1e","keyword":"静态顶空萃取","originalKeyword":"静态顶空萃取"},{"id":"71eab470-5b45-4d9c-9e4e-05906ad77b69","keyword":"气相色谱-质谱","originalKeyword":"气相色谱-质谱"},{"id":"b5b42ca2-2994-4524-b6a9-c5b5749b5778","keyword":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","originalKeyword":"苯系物"},{"id":"1e700231-acf1-432a-b62a-1325c5075d5b","keyword":"海水","originalKeyword":"海水"}],"language":"zh","publisherId":"sp201205009","title":"静态顶空气相色谱-质谱联用法快速测定海水中13种<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","volume":"30","year":"2012"},{"abstractinfo":"利用顶空固相微萃取(HS-SPME)与气相色谱-质谱(GC-MS)联用建立了测定海洋沉积<span style=\"color:red\">物</span>中的<span style=\"color:red\">苯</span>、甲苯、乙苯、对二甲苯、间二甲苯、邻二甲苯以及苯乙烯等7种常见<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的检测分析方法.对无机盐的加入、平衡时间、萃取温度、萃取时间、解吸温度和时间等多个固相微萃取条件以及色谱条件进行了优化,内标法定量.结果表明:在0.500 ～20.0 ng/g范围内7种<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的线性关系良好,相关系数在0.995 ～ 0.999之间;方法检出限为0.081 8～0.175 ng/g(干重);日内和日间重现性较好,相对标准偏差分别为1.2％ ～ 3.6％(n=5)和0.4％～6.3％(n=3);在每1.00 g海洋沉积<span style=\"color:red\">物</span>样品中2.0和15.0 ng加标水平下,平均加标回收率分别为61.7％ ～79.5％和77.1％～85.6％,相对标准偏差分别为5.4％～9.6％和3.9％～7.6％(n=5).该方法快速、灵敏、简便,准确度高,重现性好,适合海洋沉积<span style=\"color:red\">物</span>样品中<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>的痕量分析.","authors":[{"authorName":"吴金浩","id":"86199fe1-e3a8-486c-8da0-55a2a4682c93","originalAuthorName":"吴金浩"},{"authorName":"王召会","id":"55a2b0a8-9d36-4b64-a168-034f59fa6183","originalAuthorName":"王召会"},{"authorName":"王摆","id":"21fc6480-6a76-410f-b220-97e3233ced91","originalAuthorName":"王摆"},{"authorName":"周遵春","id":"be9d7d81-6a85-472c-822e-730b8a4b4ad4","originalAuthorName":"周遵春"},{"authorName":"王年斌","id":"9655b71d-5102-471a-8af3-9d0b8a3396e8","originalAuthorName":"王年斌"}],"doi":"10.3724/SP.J.1123.2013.07025","fpage":"1218","id":"474c90a6-fddc-4c1e-96b0-d6717a59607a","issue":"12","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"7de2a2e8-b6eb-43d9-802b-7fdc18c79314","keyword":"顶空固相微萃取","originalKeyword":"顶空固相微萃取"},{"id":"15d1e3e0-7f1d-4e99-bb4a-681926fa8886","keyword":"气相色谱-质谱","originalKeyword":"气相色谱-质谱"},{"id":"01da2ac9-223b-4ce9-878e-98d40687b1a2","keyword":"<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","originalKeyword":"苯系物"},{"id":"9fd7d57e-8e65-4eb8-bcaa-baa9ba246913","keyword":"海洋沉积<span style=\"color:red\">物</span>","originalKeyword":"海洋沉积物"}],"language":"zh","publisherId":"sp201312014","title":"顶空固相微萃取-气相色谱-质谱联用法测定海洋沉积<span style=\"color:red\">物</span>中的<span style=\"color:red\">苯</span><span style=\"color:red\">系</span><span style=\"color:red\">物</span>","volume":"31","year":"2013"}],"totalpage":5345,"totalrecord":53447}